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65 results about "Lead selenide" patented technology

Lead selenide (PbSe), or lead(II) selenide, a selenide of lead, is a semiconductor material. It forms cubic crystals of the NaCl structure; it has a direct bandgap of 0.27 eV at room temperature. (Note that incorrectly identifies PbSe and other IV–VI semiconductors as indirect gap materials.) It is a grey crystalline solid material.

Device comprising doped nano-component and method of forming the device

A device comprising a doped semiconductor nano-component and a method of forming the device are disclosed. The nano-component is one of a nanotube, nanowire or a nanocrystal film, which may be doped by exposure to an organic amine-containing dopant. Illustrative examples are given for field effect transistors with channels comprising a lead selenide nanowire or nanocrystal film and methods of forming these devices.
Owner:GLOBALFOUNDRIES INC

Formation of photoconductive and photovoltaic films

The present application discloses a method and system of depositing a lead selenide film onto another material. The lead selenide film may used in a photoconductive application or a photovoltaic application. Furthermore, the applications may be responsive to infrared radiation at ambient temperature. In one embodiment, a method includes sputtering the lead selenide film, performing a sensitization process, and applying a passivation film. In one exemplary embodiment, a p-n junction is formed by directly adhering a lead selenide film to a silicon substrate.
Owner:ADVANCED INTEGRATION

Sulfur-group lead-compound thermoelectric material and preparation method thereof

The invention relates to a sulfur-group lead-compound thermoelectric material and a preparation method thereof. The chemical formula of the sulfur-group lead-compound thermoelectric material is Pb(1-x)Sb(2x / 3)Se, wherein the x is larger than 0 and is less than 0.09. According to the preparation method, a high-purity simple substance is used as a raw material; batching is carried out based on a stoichiometric ratio in the chemical formula; after vacuum packaging, high-temperature melting, and annealing heat treatment are carried out, grinding is carried out to obtain powder; vacuum hot pressing sintering and slow cooling are carried out to obtain a sheet type block material that is a lead selenide material based on target components. A controllable preparation method of forming a dislocation structure by introducing a Pb positive ion vacancy structure is designed; and because a high-density transgranular dislocation structure is introduced into the material, intermediate-frequency phonons can be scattered effectively, so that the lattic thermal conductivity, less than 0.4W / m-K, of the material, can be reduced substantially. According to the prepared novel high-performance thermoelectric material based on Pb(1-x)Sb(2x / 3)Se, the zT value reaches 1.6 on the condition of 900K, wherein the zT value is a highest value of the existing PbSe system terminal. Therefore, the sulfur-group lead-compound thermoelectric material is a novel thermoelectric material with great large-scale application potential.
Owner:TONGJI UNIV

Method of Treating Non-Refrigerated, Spectrally-Selective Lead Selenide Infrared Detectors

The invention relates to a method of processing non-refrigerated lead selenide infrared detectors, consisting in: 1) selecting the substrate and preparing same; 2) delineating and depositing multilayer interference filters; and 3) treating polycrystalline lead selenide infrared detectors on the interference filters, comprising the following steps, namely 3a) metal deposition, 3b) delineation of the metal deposit, 3c) delineation of the sensor, 3d) PbSe deposition by means of thermal evaporation, 3f) processing of sensor, 3g) thermal treatment in order to sensitise the active material, and 3h) deposition of a passivator layer on the active material. The inventive method is unique in that it can be used to treat differently-shaped non-refrigerated infrared detectors on the same substrate, including discrete elements, multielements, linear matrices, two-dimensional matrices, etc., with the responses of each being modified by design by the corresponding interference filter. The invention is suitable for low-cost infrared detectors that are used for process control, gas analyses, temperature measurements, military applications, etc.
Owner:MINIO DE DEFENSA

Process for preparing aqueous phase lead selenide nano material

A process for preparing water-phase nano-lead selenide features the reaction between lead acetate, selenourea and coating agent chosen from mercaptoacetic acid, mercaptopropionic acid, cysteine, thioglycerin, and mercaptoethanol at 60-180 deg.C for 15-90 min.
Owner:CHANGCHUN INST OF APPLIED CHEMISTRY - CHINESE ACAD OF SCI

Mode-locked optical fiber laser which takes lead selenide quantum dot as saturable absorber

ActiveCN107069413AStrong third-order nonlinear optical effectFast time responseActive medium shape and constructionMode locked fiber laserErbium doping
The invention discloses a mode-locked optical fiber laser which takes a lead selenide quantum dot as a saturable absorber. Passive mode-locked optical fiber lasers based on the saturable absorbers are applied widely and gradually, bust most of existing quantum dot saturable absorbers are blocky structures, the coupling efficiency is low and the saturable absorbers are difficult to be compatible with the otpical fiber laser. The mode-locked optical fiber laser comprises a pump source, a wavelength division multiplexer, a gain optical fiber, an output coupler, a filter, an optical fiber saturable absorber and a connection optical fiber. The optical fiber saturable absorber is composed of lead selenide quantum dot-doped glass optical fiber. The pump source is a semiconductor laser with multimode tail fibers. The gain optical fiber is a ytterbium-doped optical fiber, an erbium-doped optical fiber or a thulium-doped optical fiber. The connection optical fiber is a single-mode optical fiber. According to the mode-locked optical fiber laser, the saturable absorber has higher third-order non-linear optical effect and faster time response than those of the same-component blocky material and is compatible with the mode-locked optical fiber laser.
Owner:徐州新南湖科技有限公司

Quantum dot hybrid transparent polyimide fluorescent film and preparation method

The invention discloses a quantum dot hybrid transparent polyimide fluorescent film and a preparation method. The quantum dot hybrid transparent polyimide fluorescent film comprises 0.0001-2.0wt% of quantum dots, 85-99wt% of polyimide and 0-5wt% of additive. The quantum dots are one or more of carbon quantum dots, silicon quantum dots, germanium quantum dots, cadmium sulfide quantum dots, cadmiumselenide quantum dots, cadmium telluride quantum dots, zinc selenide quantum dots, lead sulfide quantum dots, lead selenide quantum dots, indium phosphide quantum dots and indium arsenide quantum dots. Polyimide is prepared by polymerization and imidization reaction of alicyclics, a fluorine-containing bifunctional (multifunctional) organic acid anhydride monomer and an organic amine monomer. Thequantum dot hybrid polyimide fluorescent film has high light transmittance, high quantum efficiency, low dielectric constant and loss and can be applied to the technical field of LED (light-emitting diode) luminescence and display.
Owner:ZHEJIANG FORST NEW MATERIAL RES INST CO LTD

Method for preparing lead selenide nanocrystals

The invention discloses a method for preparing lead selenide nanocrystals. The method comprises the following steps of: putting selenium powder in a container; removing the air from the container and filling the container with inert gas; adding alkylamine which has a long chain with a boiling point of over 180 DEG C into the container; fully stirring and heating the selenium powder and the ammonia to perform full reaction so as to form ligand; adding lead chloride into the alkylamine which has the long chain with the boiling point of over 180 DEG C, fully stirring the mixture, vacuuming the container and then heating the mixture of the lead chloride and ammonia to fully dissolve the lead chloride in the ammonia; and injecting the mixture of selenium powder into the mixture of lead chloride to perform reaction so as to obtain the lead selenide nanocrystalline particles.
Owner:LANZHOU UNIVERSITY

Method for preparing lead selenide polycrystalline film on basis of oxygen ion beam assisted deposition

The invention provides a method for preparing a lead selenide polycrystalline film on the basis of oxygen ion beam assisted deposition. In order to solve the problem of incapability of accurately controlling the oxygen doping amount and depth distribution in the PbSe film preparation process by physical vapor deposition-atmosphere annealing combination, oxygen ion assisted surface bombarding is performed by an ion beam assisted deposition technique in a static mixing mode after the film growth finishes, and the film is subjected to subsequent vacuum annealing to prepare the PbSe polycrystalline film with favorable and stable photosensitivity. The method can accurately control the oxygen ion injecting amount and depth distribution, and separates the oxygen doping from the polycrystallization process, thereby enhancing the degree of freedom of process optimization. The preliminary characterization of optical I-V characteristic, SEM (scanning electron microscope), XRD (X-ray diffraction) and the like on the prepared sample indicates that the PbSe polycrystalline prepared by the method has favorable photoelectric properties and surface characteristics.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Method to process polycrystalline lead selenide infrared detectors

Method to process polycrystalline lead selenide infrared detectors consisting in: 1) Substrate preparation; 2) Metal deposition; 3) Metal delineation; 4) Sensor delineation; 5) PbSe deposition by thermal evaporation in vacuum; 6) Specific thermal treatment for sensitizing the active material; 7) Deposition of a pasivating layer on the active material. The method is superior to other techniques because permits to process single element detectors, multielement detectors with different geometries such as: linear arrays, 2-dimensional arrays, detectors on interference filters, multicolor arrays and devices monolithically integrated with a ROIC. Applications include low cost infrared detectors for process control, gas analysis, defense, temperature measurement etc.
Owner:MINIO DE DEFENSA

Mode-locked fiber laser taking lead selenide quantum dot as gain medium

InactiveCN107147003AEnables radiation wavelength tuningLarge fluorescence emission cross sectionActive medium materialActive medium shape and constructionMode locked fiber laserAcousto-optic modulator
The invention discloses a mode-locked fiber laser taking a lead selenide quantum dot as a gain medium. An existing mode-locked fiber laser is limited by the grain medium, only can radiate a certain special wavelength and cannot radiate some special wavelengths, The mode-locked fiber laser comprises a grain fiber, a pumping source, a wavelength division multiplexer and a modulation unit, wherein the grain fiber employs glass fiber doped with the lead selenide quantum dot, the modulation unit employs an acoustic optical modulator or graphene, and the mass percent of the lead selenide quantum dot in the grain fiber accounts for 5.68%. The mode-locked fiber laser is achieved by employing two schemes, wherein a first scheme also comprises a high reflection unit and a low reflection unit, and a second scheme also comprises a pumping isolator and an output coupler. The lead selenide quantum dot is used as the gain medium of the laser, and the mode-locked fiber laser can radiate laser with the special wavelength being 1,700 nanometers by means of the characteristic of dependence of quantum dot irradiation wavelength on size and by combining the advantage of large emission cross section of the lead selenide quantum dot.
Owner:HANGZHOU DIANZI UNIV

Saturable absorption device, preparation method and optical fiber pulse laser

InactiveCN109842013AGood photoconductive effectResponsiveLaser detailsOptical fiber cableLead selenide
The embodiment of the invention discloses a saturable absorption device, a preparation method and an optical fiber pulse laser. The saturable absorption device comprises an optical element and a saturable absorption film, wherein the saturable absorption film is disposed in the optical transmission path of the optical element; and the saturable absorption film comprises lead selenide. The saturable absorption device provided by the embodiment of the invention utilizes the saturable absorption characteristics of lead selenide to compress the continuous laser into pulsed laser, which has the characteristics of good photoconductive effects and sensitive response, and can be stably generated Q-switched or mode-locked laser pulses when mounted in an optical fiber laser.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Lead salt film structure for infrared photoelectricity and preparation method thereof

The invention belongs to the field of photoelectronic devices, and particularly relates to a composite-structure lead salt film for infrared photoelectricity and a preparation method thereof. The leadsalt film comprises a base, a lead salt crystal grain layer prepared by a physical vapor deposition method, and small-crystal-grain lead salt prepared by a chemical method; the lead salt crystal grain layer covers the base, and gaps exist among lead salt crystal grains; the small-crystal-grain lead salt is embedded into the gaps; the lead salt film is lead sulfide or lead selenide; and the base is a quartz substrate or a sapphire substrate or a silicon wafer containing an oxide layer. The preparation method comprises a physical vapor deposition method and a chemical method. The composite structure lead salt film provided by the invention is more compact in structure and high in uniformity; as a photoelectric detector, the annealed composite structure lead salt film is low in noise, high in specific detection rate, short in time consumption of the preparation method and simple in process.
Owner:CHONGQING INST OF GREEN & INTELLIGENT TECH CHINESE ACADEMY OF SCI

Preparation method of lead selenide semiconductor film

The invention provides a preparation method of a lead selenide semiconductor film. The method mainly solves problems of loose film tissue and weak bonding strength with matrix of a film prepared by a traditional chemical method, and also solves problems of lack of photoelectric performance of the film prepared by a traditional chemical method and subsequent sensitization process required. The method employs a non-equilibrium radio frequency magnetron sputtering system and a lead selenide composite target material to prepare a coating; oxygen is introduced during a preparation process; and oxygen flow and sputtering power are adjusted to realize control on the film performance. The compact coating prepared by the invention has good combination performance between the film and the matrix, and good photoelectric response performances. The method is easily practical, uses simple and easily available raw materials and is easy to realize industrialized production.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Lead selenide coated lead telluride dendritic crystal composite and preparation method thereof

The invention provides a lead selenide coated lead telluride dendritic crystal composite and a preparation method thereof, and relates to a thermoelectric material. The lead selenide coated lead telluride dendritic crystal composite and the preparation method provided by the invention have the advantages that the preparation method is low in reaction temperature, simple in process and friendly to environment, and the synthesized powder is high in purity and good in morphology. The lead selenide coated lead telluride dendritic crystal composite is composed of lead telluride and lead selenide, wherein PbTe in a stoichiometric proportion is coated with PbSe in a stoichiometric proportion. The preparation method comprises the steps that Pb(CH3COO)2.3H2O, TeO2 and SeO2 are dissolved in a sodium hydroxide aqueous solution in the mol ratio of Pb: Te: Se=2: 1: 1; NaBH4 is added to the solution and mixed together to obtain a precursor solution; next, the precursor solution is transferred into a reaction kettle and preserved with heat for 18-22 h at a temperature ranging from 160 to 200 DEG C and then the reaction is stopped; after the reaction temperature is reduced to the room temperature, precipitate is separated out, washed until neutrality and dried at a constant temperature; finally, the lead selenide coated lead telluride dendritic crystal composite is obtained.
Owner:XIAMEN UNIV

Method for inhibiting quantum dot surface defect state based on crystal face control

InactiveCN111423869AEasy to fall offAddressing Insufficient PassivationMaterial nanotechnologyNanoopticsLead sulfidePhotochemistry
The invention discloses a method for inhibiting a quantum dot surface defect state based on crystal face control, and belongs to the technical field of preparation of compound semiconductor nano materials; the method includes heating the lead precursor solution to 40 DEG C to 70 DEG C, and then rapidly injecting a sulfur source or selenium source solution with the concentration of 0.6 mol / L to 0.8mol / L; slowly dropwise adding a sulfur source or selenium source solution with the concentration of 0.1 mol / L-0. 2mol / L; then adding a ligand, then adding an anti-solvent until the solution becomes turbid, then centrifuging, and precipitating to obtain lead sulfide quantum dots, lead selenide quantum dots, lead sulfide / lead selenide core-shell quantum dots or lead selenide / lead sulfide core-shellquantum dots which are wrapped by the ligand and have a body-centered tetragonal lattice structure, wherein the amount of substance of the lead precursor is greater than the sum of the amount of substance of the added sulfur source or selenium source, and the whole reaction is carried out under protective gas. The final product can effectively relieve the exposure condition of the {100} crystal face, avoids invasion of oxygen and moisture, has few surface defect states, and has good stability in air.
Owner:HUAZHONG UNIV OF SCI & TECH

Quantum dot photoelectric detector and preparation method thereof

The invention discloses a preparation method for a quantum dot photoelectric detector, and the preparation method comprises the following steps: preparing a precursor solution containing a cadmium selenide colloidal quantum dot; preparing a lead selenide colloidal quantum dot solution based on the precursor solution; removing impurities in the lead selenide colloidal quantum dot solution and performing separation to obtain a lead selenide colloidal quantum dot material; providing a substrate, and setting a plurality of spaced electrodes on the surface of the substrate; placing the lead selenide colloidal quantum dot material on the surface of the substrate to form a quantum dot photosensitive layer and electrically connecting the photosensitive layer to the electrode. The invention also provides the quantum dot photoelectric detector.
Owner:RESEARCH INSTITUTE OF TSINGHUA UNIVERSITY IN SHENZHEN

Lead selenide quantum dot/graphene composite material and preparation method thereof

The invention provides a lead selenide quantum dot / graphene composite material and a preparation method thereof. The composite material is prepared with graphene oxide sheets as a hard template through an ionic complexing method. Firstly, through the complexing and electrostatic effects between carboxylic groups in the graphene oxide and soluble lead salt, lead ions are immobilized on the surface of the graphene oxide, and then a less amount of an alkaline solution is dropwisely added slowly, wherein a certain interval is maintained between graphene oxide sheets through electrostatic repulsion between hydroxide ions and carboxylate ions. A selenium precursor solution is prepared under protective of nitrogen and then is added to the graphene oxide / lead ion complex to to be in a reflux reaction. A reduction agent is then added to reduce the graphene oxide sheets to prepare the lead selenide quantum dot / graphene composite material. The method is simple in operation, is convenient to operate and is repeatable. The composite material has high electron transportation performance of graphene, is high in Seebeck coefficient, and has excellent application prospect in the field of thermoelectricity.
Owner:TIANJIN RES INST FOR ADVANCED EQUIP TSINGHUA UNIV

PbSe quantum dot medium-long wave infrared photoelectric detector based on in-band transition, and manufacturing method thereof

PendingCN113421941AWide spectral control rangeHigh risk control valueFinal product manufactureSemiconductor devicesQuantum yieldParticle physics
The invention discloses a PbSe quantum dot medium-long wave infrared photoelectric detector based on in-band transition, and a manufacturing method thereof. PbSe nanometer colloid shows a good exciton structure, and energy exciton tuning ranges from 0.5 eV to 1 eV, which is a size function. When band-edge fluorescence is observed from 1.2 m to 24 m, the Stokes shift is small, and the sub-ns service life is close to the unified quantum yield. During 1.064 nm pumping, first exciton attenuation is consistent with radiation relaxation under low pumping intensity and Auger recombination under high pumping intensity. Optically induced absorption is observed at approximately the middle gap. Lead selenide (PbSe) quantum dots have the characteristics of wide infrared spectrum regulation and control range, high fluorescence quantum yield, solution processability and the like, and coating of a shell layer is one of strategies for effectively improving optical characteristics and chemical stability of the PbSe quantum dots and is a research direction for promoting application and development of the PbSe quantum dots. The PbSe core-shell quantum dots designed by the invention have very high application value in the fields of photoelectric detection, solar cells, lasers, photocatalysis and the like.
Owner:JIANGSU UNIV

Flexible antimony selenide solar cell and preparation method thereof

The invention provides a flexible antimony selenide solar cell and a preparation method thereof. According to the method, a lead selenide back contact layer is prepared on a back electrode through a low-temperature magnetron sputtering method, then subsequent preparation of an antimony selenide absorption layer, a buffer layer, a window layer and a top electrode is carried out, crystal growth of subsequently deposited antimony selenide is optimized through the lead selenide back contact layer, meanwhile, the contact barrier of a back contact interface is reduced, and the service life of the back contact interface is prolonged. And the preparation of the flexible, low-temperature and efficient antimony selenide thin film solar cell is realized. The invention provides a novel preparation method of the low-temperature flexible back contact layer, effectively optimizes the growth of the antimony selenide absorption layer, reduces the back contact potential barrier of the device, improves the performance of the device, and realizes the preparation of the flexible antimony selenide solar cell.
Owner:HEBEI UNIVERSITY

Method for preparing lead selenide film by using microwave plasma chemical vapor deposition technology

ActiveCN112017945ADo not change the composition of the elementsDoes not change material propertiesSemiconductor/solid-state device manufacturingChemical vapor deposition coatingEvaporation (deposition)Chemical physics
The invention belongs to the technical field of infrared detection, and relates to a method for preparing a lead selenide film by using a microwave plasma chemical vapor deposition technology. The method comprises the following steps: (1) growing a lead selenide film on a substrate by adopting a thermal evaporation technology; and (2) treating the lead selenide film by adopting the microwave plasma chemical vapor deposition technology. The microwave plasma treatment technology does not cause selenium element loss, and does not change element composition or material properties of raw materials,the crystallization degree is improved only through the sintering phenomenon, and the photoelectric property is enhanced.
Owner:CHONGQING INST OF GREEN & INTELLIGENT TECH CHINESE ACADEMY OF SCI +1
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