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279results about How to "Effect on mechanical properties" patented technology

Preparation method of high-melting-point and high-entropy alloy spherical powder based on laser additive manufacturing

The invention discloses a preparation method of high-melting-point and high-entropy alloy spherical powder based on laser additive manufacturing. The preparation method comprises the steps: randomly selecting powder of five or more from high-melting-point metallic elements including tungsten, titanium, zirconium, hafnium, vanadium, niobium, tantalum and molybdenum, and mixing the powder according to a certain ratio; then, carrying out mechanical alloying by using a high-energy ball mill to obtain single-phase solid solution powder of a high-melting-point and high-entropy alloy; preparing a powder bar material by adopting the forming standard of a hot isostatic pressing process; and finally, preparing laser directly-formed powder by using an electrode induction melting gas atomization process. By using the single-phase solid solution powder of the high-melting-point and high-entropy alloy, formed by using the preparation method, a series of problems of different burnout rates of different elements due to relatively high difference as well as component microscopic segregation and negative eutectic and the like caused by various elements in the laser additive manufacturing and forming processes of the powder of the high-melting-point metallic elements can be solved, and the rapid and precise manufacture of high-temperature-resistant and wear-resistant parts special for the aerospace and hot end parts of high-performance turbine engines can be more effectively realized.
Owner:XI AN JIAOTONG UNIV

Compound medicament intravascular stent and preparation method thereof

The invention relates to a composite drug stent and a preparation method thereof. The stent includes a stent body and active drugs; wherein, the stent body is a perforated medical material with good biocompatibility, which can be made by optionally using stainless steel, cobalt-based alloy, titanium alloy, nickel-titanium alloy, or polylactic acid bio-polymer material; the active drugs include special endothelial progenitor cell antibody drug and anti-smooth muscle cell proliferation drug. The internal surface of the perforated stent body is fixedly provided with the special endothelial cell antibody drug, while the external surface of the perforated stent body is coated with the anti-smooth muscle cell proliferation drug. The preparation method includes as follows: (1) pretreating the surface of the stent body; (2) making holes; (3) post-treating the surface of the stent body; (4) dispensing medicines; (5) coating the external surface; (6) fixing the internal surface; (7) drying at low temperature. The preparation method can selectively absorb endothelial progenitor cells and facilitate in repairing endodermis, and can effectively inhibit the proliferation and migration of vascular smooth muscle cells, persistently and effectively reduce the newborn endangium, effectively prevent the stent from narrowing, and avoid the risk of tardive thrombosis.
Owner:LEPU MEDICAL TECH (BEIJING) CO LTD

Preparation method of self-lubricating ceramic cutting tool material comprising spherical nanometer silicon dioxide coated hexagonal boron nitride composite powder

The invention relates to a preparation method of self-lubricating ceramic cutting tool material comprising spherical nanometer silicon dioxide coated hexagonal boron nitride composite powder. The self-lubricating ceramic cutting tool material comprises the following raw material components in percentage by volume: 15-75% of TiC, 2-20% of h-BN@SiO2, 0.2-2.5% of MgO and the balance of Al2O3, wherein the h-BN@SiO2 is the spherical silicon dioxide coated hexagonal boron nitride composite powder which is obtained by dispersing h-BN powder in absolute ethyl alcohol and dropwise adding tetraethyl orthosilicate at the temperature of 30-70 DEG C. The invention also provides the preparation method of the self-lubricating ceramic cutting tool material. The added h-BN@SiO2 can improve the wettability of h-BN@SiO2 and a matrix and the mechanical property of the cutting tool material when the excellent lubricating property of the cutting tool material is remained, and reduce the agglomeration of air holes and the h-BN@SiO2 and the negative influence of the added h-BN on the mechanical property of the self-lubricating ceramic cutting tool material. The self-lubricating ceramic cutting tool material is suitable for application in manufacturing of self-lubricating ceramic cutting tools and can also be used for manufacturing ceramic molds, bearings and other wear-resisting anti-corrosion components and parts.
Owner:QILU UNIV OF TECH

Preparation method of molecular sieve coating material on surface of porous silicon carbide ceramic with surface rich in silicon

The invention relates to a preparation method of a molecular sieve coating material on the surface of porous silicon carbide ceramic with the surface rich in silicon, and the molecular sieve coating material is prepared by using the porous silicon carbide ceramic with the surface rich in silicon as a carrier; using solid materials, such as silicon blocks, quartz, sliicon-alumininm composite oxide sintering powder with adjustable sliicon-alumininm atomic ratio, and the like as a silicon source or a sliicon-alumininm source, and adopting a in situ hydrothermally synthesizing method. Molecular sieve crystals preferentially nucleate on the surface of the porous silicon carbide ceramic due to a surface silicon layer of the porous silicon carbide ceramic, the solid silicon source or the sliicon-alumininm source are used so that the release speed of the silicon source or sliicon-alumininm source for the growth of crystal nucleus is controllable. Therefore, prepared molecular sieve coating is uniformly loaded on the surface of the silicon carbide ceramic carrier; the composite material formed by a molecular sieve and the porous silicon carbide ceramic has a unique micropore / macropore structure; chemical combination is realized between the molecular sieve and the porous silicon carbide ceramic, and the molecular sieve and the porous silicon carbide ceramic have high interface combination strength. The preparation method has simple technology, convenient operation without complex equipment and low manufacturing cost and is more suitable for industrialized and mass production.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Biology polypeptide medicament blood vessel bracket and preparation method thereof

The invention relates to a biologic polypeptide medicine blood vessel support and a preparation method thereof. The biologic polypeptide medicine blood vessel support comprises a support body and active medicines. The support body which is medical material with pores and good biocompatibility is made from stainless steel, cobalt-base alloy, titanium alloy, nickel-titanium alloy or polylactic acid biopolymer; the active medicines comprise a biologic polypeptide medicine and a smooth muscle cell proliferation inhibition medicine. The support is characterized in that: the support body with the pores has the biologic polypeptide medicine fixed on the internal surface of the body and the smooth muscle cell proliferation inhibition medicine coated on the external surface of the body. The preparation me(3) carrying out the after-treatment of the surface of the support body; (4) preparing the medicines; (5) coating the external surface; (6) fixing the medicine onto the internal surface; (7) carrying out the process step of low temperature drying. The support can selectively absorb endothelium progenitor cells which quickly differentiate into endothelium cells to promote the restoration of the endothelium after the support is built in; the support can also effectively inhibit the proliferation and migration of vascular smooth muscle cells, persistently and effectively reduce the formation of a new inner membrane, effectively prevent restenosis inside the support, and avoid the risk of potentially fatal late thrombosis.
Owner:乐普(深圳)国际发展中心有限公司

Preparation method and application for reaction-type halogen-containing flame-retardant polyether polyol

A preparation method for a reaction-type halogen-containing flame-retardant polyether polyol belongs to the field of organic synthesis. The preparation method comprises: initiating a ring-opening polymerization reaction of chloropropylene oxide by a bromine-containing dihydric alcohol/phenol initiator under the effect of a catalyst, to prepare a bifunctionalpolyepichlorohydrin; reacting bifunctionalpolyepichlorohydrin with a strong alkali solution to remove partial chlorine atoms and further to obtain an epoxy-terminated compound; under the effect of an acidic catalyst, in the presence of water and an organic solvent, performing a hydrolysis reaction on the epoxy-terminated compound to obtain a multi-functional halogen-containing flame-retardant polyether polyol solution; performing reduced pressure distillation on the polyether polyol solution to obtain the product halogen-containing flame-retardant polyether polyol. The method has the advantages of cheap and easily available raw materials, a simple and controllable reaction and a yield of 95% or more; the prepared reaction-type halogen-containing flame-retardant polyether polyol is moderate in viscosity, and good in compatibility with foaming agents or other auxiliary agents; a combined material by using the polyether polyol is uniform, transparent, excellent in fluidity and good in stability.
Owner:JIANGSU YOKE TECH

Reaction type polysiloxane flame-retardant coating and preparation method thereof

The invention discloses a reaction type polysiloxane flame-retardant coating and a preparation method thereof, and belongs to the technical field of flame-retardant coatings. The reaction type polysiloxane flame-retardant coating consists of a silane coupling agent, ammonium polyphosphate, a film-forming agent, a polysiloxane flame retardant, a wetting agent and ethanol. The film-forming agent and the silane coupling agent of the reaction type polysiloxane flame-retardant coating have the function of film forming simultaneously, the silane coupling agent and the synthesized polysiloxane flame retardant can be also acted with each other, and the silane coupling agent and the flame retardant can implement microencapsulation on the ammonium polyphosphate, and can be also reacted, so that the reaction type polysiloxane flame-retardant coating of a spatial cross-linked net structure can be prepared, the coating adopts ethanol as a solvent, and the raw materials of the whole system are environmental-friendly reagents which can do no harm to the environment and operators; the coating is a reaction type coating, is high in flame retardancy efficiency, and can be deformed together with a substrate without dropping, the limit oxygen index LOI of polypropylene can be up to 31.3% and can be qualified in UL-94 V0 tests, and the mechanical property of the substrate can be barely affected.
Owner:TAIYUAN UNIV OF TECH

Quaternary ammonium cation and quaternary phosphonium cation-containing modified clay, its preparation and application

Belonging to the field of organic-inorganic hybrid materials, the invention provides a quaternary ammonium cation and quaternary phosphonium cation-containing organic cation modified clay, its preparation method and application. The preparation method comprises: reacting a suspending solution of a sodium base treated clay mineral with quaternary ammonium cations and quaternary phosphonium cations, conducting filtering, washing, drying and crushing, thus obtaining the quaternary ammonium cation and quaternary phosphonium cation-containing organic cation modified clay with a synergistic effect. The organic cation modified clay provided in the invention has good stability, excellent weather resistance, and no toxicity. The organic cation modified clay contains quaternary ammonium cation modified clay and quaternary phosphonium cation modified clay simultaneously, and shows a synergistic antibacterial activity, so that it can be applied to plastics, rubber, fibers, coatings, adhesives, paper, wood-plastic composite materials and a variety of polymer materials to improve the antibacterial property, the flame retardance and the barrier property of polymers, and has no influence on the mechanical properties of the polymers.
Owner:JINAN UNIVERSITY

Matte TPO skin material with low processing viscosity as well as preparation method and application of TPO skin material

The invention provides a matte TPO skin material with low processing viscosity as well as a preparation method and application of the TPO skin material. The TPO skin material is formed by filling a thermoplastic polyolefin (TPO) with nanoparticles, wherein the mass ratio of the TPO to the nanoparticles is (90-99.5):(0.5-10); and the nanoparticles include one or more selected from the group consisting of multi-layer graphene, carbon nanotubes, monodisperse polystyrene microspheres, manganese oxide nanowires, iron tetroxide nanoparticles, fumed silica, and nano carbon black particles. The nanoparticles are packed in the TPO, so that the free volume of the polymer is increased, and the density of entanglement points is reduced; at the same time, interface slip occurs between the nanoparticlesand the polymer, the interface slip acts as a lubricant to reduce the viscosity of the system, so that the process temperature of operation such as mixing, calendaring and extrusion in the material processing process is reduced; the nanoparticles play a matting effect; the added nanoparticles have little effect on the mechanical properties of the material and improves the friction-resistant coefficient; and the TPO skin material provides guidance for industrial production.
Owner:CHANGCHUN INST OF APPLIED CHEMISTRY - CHINESE ACAD OF SCI

Sulfur-group lead-compound thermoelectric material and preparation method thereof

The invention relates to a sulfur-group lead-compound thermoelectric material and a preparation method thereof. The chemical formula of the sulfur-group lead-compound thermoelectric material is Pb(1-x)Sb(2x / 3)Se, wherein the x is larger than 0 and is less than 0.09. According to the preparation method, a high-purity simple substance is used as a raw material; batching is carried out based on a stoichiometric ratio in the chemical formula; after vacuum packaging, high-temperature melting, and annealing heat treatment are carried out, grinding is carried out to obtain powder; vacuum hot pressing sintering and slow cooling are carried out to obtain a sheet type block material that is a lead selenide material based on target components. A controllable preparation method of forming a dislocation structure by introducing a Pb positive ion vacancy structure is designed; and because a high-density transgranular dislocation structure is introduced into the material, intermediate-frequency phonons can be scattered effectively, so that the lattic thermal conductivity, less than 0.4W / m-K, of the material, can be reduced substantially. According to the prepared novel high-performance thermoelectric material based on Pb(1-x)Sb(2x / 3)Se, the zT value reaches 1.6 on the condition of 900K, wherein the zT value is a highest value of the existing PbSe system terminal. Therefore, the sulfur-group lead-compound thermoelectric material is a novel thermoelectric material with great large-scale application potential.
Owner:TONGJI UNIV

Oscillating arm type strong grinding mill

InactiveCN102744127AIncrease the rolling pressureImprove crushing effectGrain treatmentsGrinding millCentrifugal force
The invention discloses an oscillating arm type strong grinding mill. A grinding roller device and a grinding ring of a host grinding mill are arranged in a host grinding mill shell; the grinding roller device is installed on a host spindle; the grinding roller device comprises grinding roller racks, oscillating arms, grinding rollers, grinding roller shafts, grinding roller shaft pushing racks and thrust mechanisms; the inner ends of the oscillating arms are hinged in grinding roller rack ring slots; the outer ends of the oscillating arms extend out of the grinding roller racks; the grinding roller shafts are arranged on the ring slot holes of the oscillating arm extending ends; the upper ends and the lower ends of the grinding roller shafts are arranged in radial slots arranged on the top and the bottom of the ring slot in a sliding fit mode; the grinding roller shaft pushing racks for pushing the grinding roller shafts are arranged in oscillating arm ring slots in a sliding mode; the thrust mechanisms for generating radial thrust to the grinding roller shaft pushing racks are arranged on the bottoms of the oscillating arm ring slots; and the grinding rollers are arranged in the grinding roller shaft pushing racks and are installed on the grinding roller shafts by bearings. According to the oscillating arm type strong grinding mill disclosed by the invention, the thrust mechanisms are adopted to apply additional thrust on the grinding rollers in addition to centrifugal force, and grinding force on the material by the grinding rollers is increased so as to obtain better crushing effect and improve the yield.
Owner:GUILIN SHENGXING MACHINERY MFG
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