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32results about How to "Good performance at high temperature" patented technology

Composite interlayer and method for brazing metal with ceramic and ceramic matrix composite material by utilizing same

The invention relates to a composite interlayer and a method for brazing metal with a ceramic and ceramic matrix composite material by utilizing the same, and solves a difficult problem of poor connector performance caused by a large amount of brittle phases generated in a strong reaction of a connector interface during brazing of the metal and the ceramic and ceramic matrix composite material by adopting an active brazing material and large residual stress of the connector after welding. The composite interlayer comprises an upper-layer brazing material, a soft interlayer and a lower-layer brazing material. The method comprises the following steps: 1, brazing material preparation, wherein the brazing material is prepared at a certain ratio; 2, cleaning, wherein cleaning is performed by acetone; 3, assembling, wherein a to-be-welded base material and the composite interlayer are assembled according to a certain sequence; 4, welding, wherein welding is performed in a vacuum brazing furnace. The operation is simple, and the addition of the interlayer inhibits over-reaction of the brazing material and the base material, reduces residual stress of the connector, and greatly improves the connector performance. The method is used for brazing the metal with the ceramic and ceramic matrix composite material.
Owner:HARBIN INST OF TECH

Low-alloy heat-resisting cast iron and preparation method thereof

ActiveCN102337452ALow degree of alloyingImprove antioxidant capacityAlloyOxidation resistant
The invention relates to low-alloy heat-resisting cast iron, which comprises the ingredients of 2.5 to 3.5 percent of C, 2.5 to 3.5 percent of Si, 0.1 to 1.0 percent of Cr, less than 1.0 percent of Mn, less than 0.3 percent of P, less than 0.1 percent of S, 1.8 to 4.0 percent of Al, 0.05 to 0.1 percent of Sr and the balance of Fe. The preparation method comprises the steps that: scrap steel, chromium iron, pig iron, silicon iron, pure aluminum and aluminum-strontium intermediate alloy are mixed and smelted according to the mass percentage of the chemical ingredients in the target product, wherein the pure aluminum is placed at the bottom of a casting ladle in advance, after an aluminum block is smelted, the aluminum-strontium intermediate alloy is added, 75SiFe nucleating agents are filled along with flows, and the drossing and the casting are carried out after stirring; in the preparation method, the aluminum content is low, the aluminum-strontium intermediate alloy is matched for carrying out spheroidisation on molten iron; and a protecting film is promoted to be formed on the surface of the cast iron at a high temperature. The low-alloy heat-resisting cast iron has the advantages that the process method is simple, the operation is convenient, the production cost is low, the comprehensive mechanical performance is good, the inoxidizability is high, and the low-alloy heat-resisting cast iron adapts to various application processes requiring repeated heating and cooling, such as crucibles, fire grates and the like for nonferrous metal smelting. The low-alloy heat-resistingcast iron is suitable for industrial production.
Owner:CENT SOUTH UNIV

Environment-friendly method for preparing mullite fiber based porous ceramic through gel casting

The invention belongs to the field of porous ceramic and in particular relates to an environment-friendly method for preparing mullite fiber based porous ceramic through gel casting. The mullite fiberbased porous ceramic is prepared from the following raw materials in percentage by mass: 11 to 32 percent of rho-Al2O3 powder, 13 to 36 percent of kaolin or zircon powder and 33 to 75 percent of mullite fiber. The method comprises the following steps: taking the rho-Al2O3 powder and the kaolin or zircon powder; adding a certain amount of de-ionized water; mechanically stirring and carrying out ultrasonic oscillation to obtain stable and uniform ceramic slurry; then uniformly adding the mullite fibers into the ceramic slurry; continually stirring and oscillating to obtain gel ceramic-fiber slurry; then carrying out injection molding and curing at room temperature; putting a molded biscuit into a constant-temperature drying box and drying; after de-molding, putting into a high-temperature furnace; sintering under an air atmosphere to obtain mullite combined or ZrO2-mullite combined mullite fiber based porous ceramic. The environment-friendly method has a simple and feasible technology and is environmentally friendly; the prepared mullite fiber based porous ceramic has high porosity, low heat conductivity and relatively high strength.
Owner:NORTHEASTERN UNIV

Sleeve lime kiln empty-kiln baking method

The invention relates to a sleeve lime kiln. A sleeve lime kiln empty-kiln baking method comprises the steps: introducing coal gas to temporary burners of the sleeve lime kiln; starting up an exhaust gas draught fan to allow a negative pressure in the kiln to be greater than or equal to -0.05 kPa; igniting the temporary burners in order, inserting ash discharging devices from ash discharging device observation holes, and making the burners upward and fixing; when the temperature in the kiln rises to 50 DEG C, controlling the temperature rising speed at 3 DEG C to 5 DEG C per hour for rising the temperature; when the temperature rises to 280 to 300 DEG C, carrying out heat preservation; 24 hours later after beginning to baking the kiln, opening burner drainage screws and exhaust gas flue drainage holes, after the burners drain, tightening the screws, and timing for every 4 hours to drain once; carrying out continuous heat preservation until drainage ports have no obvious water, that is to said moisture of a refractory material in the kiln is baked to a reasonable control range; cutting off temporary burner coal gas valves; closing the exhaust gas draught fan; and eight hours later, closing a cooling draught fan. The method can effectively remove the moisture in the refractory material and ensure the high-temperature using performance of the refractory material.
Owner:SHANGHAI BAOYE CONSTR INDAL FURNACE ENG TECH +1

Low-heat-conductivity multilayer composite potassium aluminosilicate brick and preparing method thereof

ActiveCN105777149AGood resistance to alkali corrosionExtended service lifeCeramicwareComposite structureAntioxidant
The invention discloses a low-heat-conductivity multilayer composite potassium aluminosilicate brick and a preparing method thereof.The low-heat-conductivity multilayer composite potassium aluminosilicate brick comprises a working layer, a heat preservation layer and a heat insulation layer, wherein the working layer and the heat preservation layer are connected into a whole in the length direction of the brick, a notch is formed in the end face, located in the width direction of the heat preservation layer, of the heat preservation layer, the shape of the heat insulation layer is matched with that of the notch, and the heat insulation layer is arranged in the notch.The working layer is prepared from synthesis potassium aluminate with the particle size ranging from 0 to 1 mm, silicon carbide with the particle size ranging from 1 mm to 3 mm, silicon carbide with the particle size ranging from 3 mm to 5 mm, synthesis potassium aluminate with the particle size smaller than 0.074 mm, silicon carbide with the particle size smaller than 0.074 mm, an antioxidant and a binding agent.The heat preservation layer is prepared from synthesis potassium aluminate with the particle size ranging from 0 to 1 mm, silicon carbide with the particle size ranging from 1 mm to 3 mm, silicon carbide with the particle size ranging from 3 mm to 5 mm, synthesis potassium aluminate with the particle size smaller than 0.074 mm, silicon carbide with the particle size smaller than 0.074 mm, a high-temperature reinforcing agent, a composite organic pore forming agent and a binding agent.The heat insulation layer is made of an aluminum oxide fiberboard.The low-heat-conductivity multilayer composite potassium aluminosilicate brick has excellent high-temperature usability by means of the advantages of the multilayer composite structure, and the heat conductivity coefficient and the body density are far lower than those of products of the same kind.
Owner:郑州瑞泰耐火科技有限公司

A method for preparing cf/zrc-sic ultra-high temperature ceramic composite materials by hot pressing sintering/precursor cracking method

The invention relates to a method for preparing a Cf / ZrC-SiC superhigh-temperature ceramic composite material through a hot-pressing sintering / precursor cracking process, and concretely relates to an in-situ preparation method for the Cf / ZrC-SiC superhigh-temperature ceramic composite material by combining a precursor cracking process and a hot-pressing sintering process. The method comprises: introducing ZrSi2 powder into carbon fiber fabric, employing the hot-pressing sintering process for in-situ generation of ZrC and SiC ceramic base bodies, and employing the precursor cracking process to perform final densification processing, so as to obtain the compact Cf / ZrC-Si superhigh-temperature ceramic composite material. The superhigh-temperature ceramic composite material prepared by employing the preparation method has excellent superhigh temperature usage performance, and the method is simple in process and short in time consumption. The obtained Cf / ZrC-SiC superhigh-temperature ceramic composite material can basically satisfy practical application of some heatproof structural members, and has wide application prospect in extreme environments such as super hypersonic speed flight, aerosphere reentry, trans-atmospheric flight, rocket propulsion system and the like.
Owner:AEROSPACE RES INST OF MATERIAL & PROCESSING TECH +1

Silicon nitride-based ceramic welding sealing component and preparation method thereof

The invention discloses a silicon nitride-based ceramic welding sealing component and a preparation method thereof, and relates to the technical field of metallized ceramic processing. The invention discloses a silicon nitride-based ceramic welding sealing component which comprises a silicon nitride ceramic matrix and a metallization layer, the silicon nitride ceramic matrix is prepared from modified silicon nitride, mullite fiber, aluminum nitride, calcium oxide, titanium oxide, a binder and a dispersing agent through the steps of modified silicon nitride preparation, mixing, granulation, primary sintering, secondary sintering and the like; raw materials of the metallization layer comprise copper powder, tungsten powder, copper oxide, yttrium oxide, zinc oxide and an organic binding agent. The invention further discloses a preparation method of the silicon nitride-based ceramic welding sealing component composed of the metallization layer and the silicon nitride ceramic matrix. According to the silicon nitride-based ceramic welding sealing component, the density of the silicon nitride ceramic matrix is improved, the silicon nitride-based ceramic welding sealing component has excellent strength, hardness and fracture toughness, the tensile strength of the sealing component is improved, and the silicon nitride-based ceramic welding sealing component has excellent high-temperature resistance.
Owner:湖南省新化县鑫星电子陶瓷有限责任公司

Preparation method of high-strength chrome-free brick for steel-making RH (Ruhstahl Hausen) vacuum refining slot

ActiveCN104072163BHigh strengthImproved hot strength propertiesFiberBrick
The invention relates to a preparation method of a high-strength chrome-free brick for a steel-making RH (Ruhstahl Hausen) vacuum refining slot. The high-strength chrome-free brick comprises the raw materials: one or two of 6-1 mm low silicon fused magnesia, 1-0.088mm low silicon fused magnesia and fused magnesia-alumina spinel, one or two of 180-mesh large crystal fused magnesite and fused magnesia-alumina spinel, fused magnesia-alumina spinel micro powder, one or two of modified graphite and carbon black, a boron nitride and ferro-silicon nitride composite additive, a paper pulp and sodium lignosulphonate composite bonding agent and polycrystalline zirconia fibers. The raw materials are stirred in special stirring equipment according to specified proportions and charging sequence and are subject to compression molding, drying, checking and the like to complete a preparation process. Compared with the prior art, the preparation method has the beneficial effects that as a carbon-containing material and an efficient antioxidant are added into a substrate, the high temperature corrosion-resistant property of the chrome-free brick is greatly improved; as the zirconia fibers are added, the high temperature hot strength and the normal temperature cold repair strength are obviously enhanced and the service life of a working lining is effectively prolonged.
Owner:鞍山市和丰耐火材料有限公司

A vacuum heat-insulating refractory product and its preparation method

The invention discloses a vacuum insulating refractory product and a preparation method thereof. The vacuum insulating refractory product is composed of a core material and a high-resistance film wrapped on the exterior of the core material, wherein the core material is formed by uniformly dispersing and then pressing 95-70wt% of low heat-conducting micro-pore powder and 5-30wt% of dispersed fire-resistant staples; a high-temperature resisting airtight film which is prepared from an inorganic material used as a main component in the manner of tape casting is served as the high-resistance film; the vacuum insulating refractory product is prepared after the pressed and molded core material is wrapped with the high-resistance film and then the vacuum hot-pressing packaging is performed; the product can be used under a temperature condition at 500-1200 DEG C, can maintain a vacuum structure and has ultralow thermal conductivity and high performance cost ratio; and the vacuum insulating refractory product is suitable for large-scale production, is convenient in mounting and use, can be matched with lightweight and heavy refractory materials and has an obvious energy-saving effect in effectively insulating the liner compound of a high-temperature industrial furnace.
Owner:ZHENGZHOU UNIV

A composite intermediate layer and its method for brazing metal, ceramics and ceramic-based composite materials

The invention relates to a composite interlayer and a method for brazing metal with a ceramic and ceramic matrix composite material by utilizing the same, and solves a difficult problem of poor connector performance caused by a large amount of brittle phases generated in a strong reaction of a connector interface during brazing of the metal and the ceramic and ceramic matrix composite material by adopting an active brazing material and large residual stress of the connector after welding. The composite interlayer comprises an upper-layer brazing material, a soft interlayer and a lower-layer brazing material. The method comprises the following steps: 1, brazing material preparation, wherein the brazing material is prepared at a certain ratio; 2, cleaning, wherein cleaning is performed by acetone; 3, assembling, wherein a to-be-welded base material and the composite interlayer are assembled according to a certain sequence; 4, welding, wherein welding is performed in a vacuum brazing furnace. The operation is simple, and the addition of the interlayer inhibits over-reaction of the brazing material and the base material, reduces residual stress of the connector, and greatly improves the connector performance. The method is used for brazing the metal with the ceramic and ceramic matrix composite material.
Owner:HARBIN INST OF TECH

Low-heat-conductivity multi-layer composite magnesium-hercynite brick and preparation process thereof

The invention relates to a low-heat-conductivity multi-layer composite magnesium-hercynite brick and a preparation process thereof. The low-heat-conductivity multi-layer composite magnesium-hercynite brick is prepared from the following raw materials in percentage by weight: 70-95% of microporous high-purity magnesia, 4-15% of hercynite, 2-10% of light forsterite, and 1-5% of a binding agent in a working layer, and 10-50% of microporous high-purity magnesia, 50-80%of light forsterite and 1-10% of nano aluminum oxide micro powder in a heat insulation layer. The heat insulation layer is a nano aerogel plate. According to the low-heat-conductivity multi-layer composite magnesium-hercynite brick and the preparation process thereof, the overall volume density is small, the heat conductivity coefficient is far lower than that of an existing product, the energy consumption of a thermotechnical kiln can be remarkably reduced, the purposes of saving energy and reducing consumption are achieved, and in the actual production process, production and preparation are convenient and efficient, so that actual application and popularization are facilitated, and therefore, the problems of high energy consumption and short service life of the existing cement kiln adopting pleonaste bricks are effectively solved.
Owner:郑州瑞泰耐火科技有限公司
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