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81 results about "Potassium aluminate" patented technology

Potassium aluminate is an inorganic compound with the formula KAlO₂, which in aqueous solution exists as K[Al(OH)₄]. It is used as a dyeing and printing mordant, as a paper sizing, as an accelerant in the setting of concrete.

High-performance superfine cement based grouting material for microfissuring and silty fine sand soil grouting treatment and application of grouting material

The invention discloses a high-performance superfine cement based grouting material for microfissuring and silty fine sand soil grouting treatment, and application of the grouting material. The grouting material comprises the following ingredients in parts by weight: 50-79 parts of Portland cement clinker, 19-48 parts of an auxiliary cementing material and 2-7 parts of desulfurized gypsum, whereinthe auxiliary cementing material comprises the following ingredients in parts by weight: 25-57 parts of mineral slag, 8-21 parts of steel slag, 18-36 parts of pulverized fuel ash, 6-12 parts of limestone flour, 1-8 parts of silica fume and 2.5-12.8 parts of a high-performance composite regulator; the high-performance composite regulator comprises the following ingredients in parts by weight: 5-16parts of sodium hydroxide, 4-12 parts of sodium silicate, 4-14 parts of potassium metaaluminate, 12-21 parts of calcium chloride, 11-18 parts of lithium chloride, 4-12 parts of triethanolamine, 21-27parts of alum, 18-29 parts of aluminum sulfate, 0.2-1.5 parts of hydroxypropyl methyl cellulose, 0.1-3.0 parts of viscous polymer, 0-0.8 parts of polypropylene fiber and 0.5-3.0 parts of a superplasticizer; and the viscous polymer is an acrylic ester polymer or an ethylene-vinyl acetate copolymer.
Owner:SHANDONG UNIV

Process for preparing potassium molecular sieve based slow-release fertilizer carrier from potassium feldspar powder

The invention relates to a process for preparing potassium molecular sieve based slow-release fertilizer carrier from potassium feldspar powder. The process comprises the following steps of: crushing raw potassium feldspar ores, grinding, carrying out ore dressing pretreatment to obtain the potassium feldspar powder of a certain granularity, then mixing the potassium feldspar powder with potassium carbonate based on a certain ratio, and sintering at 750-900 DEG C; hydrothermally leaching the sintered potassium silicate or potassium aluminate materials at 100-200 DEG C, and introducing CO2 to slurry obtained after the hydrothermal leaching at 70-90 DEG C until the pH value is reduced to 8-9; filtering the slurry, and washing a filter cake; mixing the carbon filter cake with potassium hydroxide and water, stirring, hydrothermally crystallizing, filtering, washing, and drying an obtained solid at 105 DEG C to obtain the product of compound powder of an L-type molecular sieve and a facellite phase, which can be used as a potassium composite molecular sieve based slow-release fertilizer carrier material. The invention has the advantages of low material cost, no three wastes (waste gas,waste water, industrial residue) discharge in the process and no pollution to the environment and facilitates the implementation and the generalization.
Owner:CHINA UNIV OF GEOSCIENCES (BEIJING)

Fly ash low-temperature wet activating treatment method

The invention provides a fly ash low-temperature wet activating treatment method, comprising the following steps of: (1) mixing the fly ash with the strong alkali solution of which the concentration is 300-700g / l, to perform activating treatment, wherein the volume-to-mass ratio of the alkali solution and the fly ash is (3:1)-(20:1) (ml / g), the activating temperature is 130-180 DEG C, the activating time is 0.5-10 hours, and the activating pressure is normal pressure to 0.5Mpa; performing liquid-solid separation after activation to get the crude alkali liquor and the activated fly ash; (2) diluting the crude alkali liquor, then, adding calcium oxide into the diluted crude alkali liquor for purification, performing liquid-solid separation to get calcareous residues and strong alkali solution, wherein the calcareous residues is output to the system as byproducts, and the strong alkali solution is recycled for fly ash activating treatment. In the method, the alkali solution is NaOH water solution, KOH water solution, sodium aluminate solution or potassium aluminate solution, after being activated, the fly ash is dissolved out by diluted acid, and the dissolution rate of aluminum oxide is up to 95-99%. In the method, the activation temperature is low, the activation effect is excellent, the activation process cannot cause secondary pollution, and essential conditions for follow-up fly ash treatment, especially for extraction of aluminum oxide, zeolite preparation, and the like, are created.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Automobile tail gas purification catalyst carrier and preparation method thereof

The invention discloses an automobile tail gas purification catalyst carrier and a preparation method thereof. The impurity Na content in the automobile tail gas purification catalyst carrier is lowerthan 400ppm; the apparent density is 1.8g / L or higher; the specific surface area at 950 DEG C at 2h is 110m<2> / g or higher; the pore volume is 0.4ml / g or higher. According to a preparation method, sodium aluminate / potassium aluminate are used as raw materials, and nitric acid, modification agents and surfactants are used as auxiliary materials; coprecipitation, aging, filtering washing, drying, roasting and crushing are performed; then, modified aluminum hydroxide or aluminum oxide is used as raw materials, surfactant and oxidizing agent containing modified aluminum hydroxide or aluminum oxide slurry is used as substrate materials; precipitators and modification agents are jointly sprayed into a bottom solution for precipitation; after the precipitation, aging, filtering washing, materialmixing, drying, roasting and crushing are performed to obtain the composite modified automobile tail gas purification catalyst carrier of composite modification aluminum oxide; the contents of impurities Na, S, P and the like are low; the requirements of the automobile tail gas purification agent carrier can be met.
Owner:KUNMING METALLURGY INST +1

Beneficiation-metallurgy combination process with function of comprehensive recovery for vanadium, aluminum, potassium and silicon in vanadium-containing siliceous shale

The invention relates to the field of beneficiation and metallurgy with a function of comprehensively recovering valuable components such as vanadium, aluminum, potassium and silicon from the vanadium-containing siliceous shale as a raw material. The process comprises steps as follows: the low-grade vanadium-containing siliceous shale is taken as the raw material, firstly, the vanadium-containingsiliceous shale is desiliconized with a flotation method, vanadium ore concentrate is uniformly mixed with excessive limestone and sodium carbonate, a mixture is subjected to high-temperature roastingin a rotary kiln, and products such as potassium aluminate, potassium ferrite, calcium metavanadate, calcium orthosilicate, carbon dioxide and the like are obtained; the sintered products are dissolved in a dilute alkaline solution, after a dissolution solution is desiliconized and purified, carbon dioxide gas produced by the rotary kiln is introduced into a closed container for carbonization reaction, Al(OH)3 precipitates are separated out, a dealumination solution is subjected to hydrolytic precipitation under the acidic condition, coarse vanadium is obtained and dissolved with alkali, ammonium chloride is added, ammonium metavanadate is obtained, a final solution is a potassium-rich and sodium-rich solution and evaporated step by step, and potash and soda are obtained. According to theinvention, the problem of environmental pollution produced by stockpiling of stone coal leaching residues is solved completely.
Owner:CENT SOUTH UNIV

Method for preparing superfine alumina by solid-phase reaction

The invention discloses a method for preparing superfine alumina by reacting alkaline aluminum salt powder (such as sodium aluminate, potassium aluminate and the like) and acid powder raw materials (aluminum chloride, aluminum sulfate, aluminum nitrate, oxalic acid, citric acid, trichloroacetic acid, ammonium chloride, ammonium sulfate and the like) to overcome the defect of difficulty in filtering and washing in a liquid-phase precipitation method. The method is characterized by comprising the following steps of: (1) performing solid-phase reaction, namely mixing the acid powder raw materials and alkaline aluminum salt powder, heating to over 60 DEG C to evaporate water generated by reaction, and keeping materials in a basically dried solid state; and (2) filtering and washing and drying, namely after cooling, mixing the materials and water to obtain suspension, filtering, washing and drying. The temperature of the solid-phase reaction is lower than temperature of harmful gas such as nitrogen oxide, sulfur oxide, carbon monoxide and the like decomposed by a reactant system; and if the temperature of the solid-phase reaction is lower than temperature when the required crystal is formed, calcining is performed at the temperature of 500 to 1,200 DEG C after filtering, washing and drying so as to prepare the required crystal.
Owner:SHANDONG AOPENG NEW MATERIAL TECH

Technique for decomposing potassium aluminate solution seed crystal to produce aluminum hydroxide

The invention relates to the field of alkaline medium wet metallurgy and particularly discloses a technique for decomposing potassium aluminate solution seed crystal to produce aluminum hydroxide. The technique comprises the steps of (A) pouring a potassium aluminate solution to a reactor, controlling the alkali concentration to be 200-280g / L and the caustic ratio of the solution to be 1.35-1.75, starting water bath circulating and stirring, controlling an initial temperature of decomposition to be 60-90 DEG C; (B) adding aluminum hydroxide seed crystal to a system, and stirring for decomposing, wherein the seed crystal coefficient is 0.5-4.0 and the stirring rate is 100-500rpm; and (C) cooling the decomposition system to 40-50 DEG C, after seed crystal decomposition reaction is terminated, stopping water bath circulating and stirring, and filtering and separating to obtain a seed pregnant solution and an aluminum hydroxide product. According to the method, the decomposition rate can reach 70% under an operation condition, and is much higher than 55% seed crystal decomposition efficiency of a traditional sodium aluminate system; and meanwhile, the product is high in purity, good in shape and form and large in particle size.
Owner:EAST CHINA UNIV OF SCI & TECH

Smelting process of carbon nanotube reinforced aluminum matrix composite

The invention provides a smelting process of a carbon nanotube reinforced aluminum matrix composite. The smelting process comprises the following steps: carrying out ball-milling mixing dispersing ona smelting assistant, a carbon nanotube and aluminum/aluminum alloy powder in a planetary ball mill to obtain mixed powder; putting the mixed powder into a mold for cold pressing to obtain a carbon nanotube-aluminum/aluminum alloy precast block; and pressing the carbon nanotube-aluminum/aluminum alloy precast block into molten aluminum through a bell jar, carrying out smelting under stirring, carrying out standing, and then carrying out casting molding, wherein the smelting assistant is any one of potassium boroaluminate (KBF4), potassium titanium fluoroaluminate (K2TiF6), potassium fluoroaluminate (K3AlF6) or sodium fluoroaluminate (Na3AlF6). According to the smelting process of the carbon nanotube reinforced aluminum matrix composite, the carbon nanotube reinforced aluminum matrix composite is prepared through the smelting process, the efficient dispersion of the carbon nanotube in the smelting process is realized, meanwhile, traditional metal smelting equipment can be used, and thusthe smelting process has the advantages of being simple, small in investment, high in product strength and the like and is suitable for industrial mass production.
Owner:WUHAN NANRUI ELECTRIC POWER ENG TECH EQUIP +4

Method for separating potassium oxide from potassium-containing sodium aluminate solution

The invention discloses a method for separating potassium oxide from a potassium-containing sodium aluminate solution, relating to a method comprising the steps of in the production of aluminum oxide, introducing SO4<2-> by adding one or a mixture of more of sodium sulfate, aluminum sulfate (basic aluminum sulfate) and an alunite ore into seeded precipitation evaporation liquor, converting potassium oxide into potassium sulfate, and performing precipitation and separation in a form of sodium aphthitalite, wherein the precipitation is implemented under high-causticizing alkali and low-temperature conditions, so that residual sodium sulfate in the solution can be avoided, and the solution can be purified; sodium aphthitalite can be used for dissolving and separating out a potassium sulfate product by virtue of variable temperature, and sodium sulfate can be recycled; or a high-potassium low-sodium ore is used for generating a pure potassium aluminate solution by using a limestone sintering method, and then the pure potassium aluminate solution is subjected to a replacement reaction with sodium aphthitalite to generate potassium sulfate and sodium aluminate; potassium chloride also can be used for converting sodium aphthitalite into pure potassium sulfate. The method disclosed by the invention can be used for producing aluminum oxide and potassium sulfate by adopting nepheline and the alunite ore by virtue of a multiple process technology, and also can be used for producing chemicals namely aluminum oxide and potassium sulfate by adopting high-silicon ores such as potassium feldspar, lepidolite and illite by virtue of an acid-alkali combination method.
Owner:赵凿元

Potassium aluminosilicate nanogel precursor admixture and application thereof in low-calcium-system geopolymer

ActiveCN113548823AUniform and dense pore structureAvoid affecting the mechanical propertiesCement productionHydration reactionGeopolymer
The invention provides a potassium aluminosilicate nanogel precursor admixture and application thereof in a low-calcium-system geopolymer, belonging to the technical field of geopolymer admixtures. The potassium aluminosilicate nanogel precursor external admixture provided by the invention has a structure of a high-activity potassium aluminosilicate short-chain structure, is a precursor of the low-calcium-system geopolymer, and comprises the following chemical components: K2O, SiO2 and Al2O3, wherein molar ratio of K to Si is 1.0-4.0, and a molar ratio of Al to Si is 0.25-1.5. When the potassium aluminosilicate nanogel precursor admixture provided by the invention is added into a low-calcium-system geopolymer matrix material, the hydration process of the low-calcium-system geopolymer such as metakaolin can be effectively optimized, internal reaction is balanced, and a pore structure is improved; and thus, the mechanical properties of the material are improved, the problems of harsh maintenance conditions, non-uniform hydration reaction and substandard mechanical properties of the low-calcium-system geopolymer are effectively solved, and a feasible scheme is provided for application of the low-calcium-system geopolymer.
Owner:SHENZHEN UNIV

Efficient magnesium-containing aluminum alloy refining and slagging dual-purpose flux and preparation method thereof

ActiveCN112301248AEnhanced complexation reactionFacilitated releasePotassium aluminateChloride
The invention relates to an efficient magnesium-containing aluminum alloy refining and slagging dual-purpose flux and a preparation method thereof, and belongs to the field of alloy smelting. The fluxcomprises the following components of, in percentage by weight, 30%-55% of magnesium chloride, 10%-45% of potassium chloride, 1%-5% of potassium feldspar, 0%-20% of calcium fluoride and 2%-10% of potassium fluoroaluminate. The flux preparation process comprises the following steps of (1), fully mixing magnesium chloride, potassium chloride, potassium fluoroaluminate, calcium fluoride and other salts which are dried at 240-300 DEG C for 3-5 hours, melting in a resistance furnace, heating to 650-750 DEG C, keeping the temperature, and stirring for 10-30 minutes to obtain a uniform salt melt; (2), pouring the salt melt into a mold for cooling, and solidifying into a blocky flux; and (3), crushing the blocky flux into particles with the average particle size of about 0.5 cm, and fully mixingthe particles with dry potassium feldspar to obtain the magnesium-containing aluminum alloy melt refining and slagging flux. The magnesium-containing aluminum alloy flux does not contain sodium salt,has refining and slagging effects, and is an ideal flux for magnesium-containing aluminum alloy.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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