The application relates to the technical field of inorganic non-
metallic materials, and discloses a high-entropy
oxide ceramic and a
solid-
phase reaction preparation method thereof; the high-entropy
oxide ceramic is prepared by using multiple
rare earth oxides,
alkaline earth metal oxides and
transition metal oxides with a purity of greater than or equal to 99.99% as raw materials, through the following steps of
raw material pretreatment, chemical stoichiometric ratio batching, wet ball milling mixing, pre-
sintering, secondary ball milling, composite forming,
internal stress release, normal-pressure
sintering densification and the like, and the high-entropy
oxide ceramic bulk body with a single-phase
solid solution structure,
high density and stable performance is prepared. The process
route of the application is simple and controllable, the
raw material cost is low, no complex equipment is needed, the generation of multiple-component
system heterogeneous phases can be effectively inhibited, the
powder component uniformity is excellent, the prepared ceramic bulk body has
high density, is suitable for large-scale industrial production, and can be widely applied to the fields of
electronic information,
aerospace, energy
catalysis, heat protection and the like.