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41results about How to "The extraction process is environmentally friendly" patented technology

A method for smelting high-purity nickel-molybdenum alloy by using nickel-molybdenum complex ore

The invention provides a method for smelting high-purity nickel-molybdenum alloy by using complex nickel-molybdenum ore. The alloy comprises the following components in percentage by mass: 8 to 30 percent of Ni, 10 to 30 percent of Mo, less than or equal to 0.5 percent of Si, less than or equal to 0.5 percent of C, less than or equal to 0.1 percent of Cu, less than or equal to 0.03 percent of P, less than or equal to 0.03 percent of S, and the balance of iron. According to the characteristic that the complex nickel-molybdenum ore is difficult to separate, the high-purity nickel-molybdenum alloy is smelted by adopting the routes of oxidizing and roasting nickel-molybdenum sulfide type mineral to remove sulfur, reducing and smelting high-alkalinity slag to obtain crude alloy, refining high-alkalinity weak oxidative slag to remove silicon and phosphorus and treating and refining Ba-Ca in vacuum to deeply remove phosphorus, sulfur and oxygen; the alloy can be used for nickel-molybdenum alloying and alloying of high nickel-molybdenum alloy steel in high-purity steel production, and has the advantages of high purity, no pollution, good alloying effect and the like; and the method has the characteristics of pure fire method, greenness, no pollution, simplicity in process and the like, realizes efficient utilization of the difficultly separated complex nickel-molybdenum ore, and is worthy of popularization.
Owner:JIANGSU UNIV

Preparation method and application of camellia flower extracting solution

The invention provides a preparation method and an application of a camellia flower extracting solution. The method comprises steps as follows: A, selecting fresh camellia flowers without damage and diseases, and drying the camellia flowers with a refraction window drying technology to obtain a dried camellia flower product; B, performing airflow superfine crushing and sieving on the dried camellia flower product, and adding a quaternary system deep-eutectic solvent for ultrasonic extraction to obtain an extracted mixture; C, mixing the extracted mixture and deionized water, regulating pH, andadding enzyme for enzymolysis; D, leaving a product to stand for a certain time after enzymolysis, and filtering the product to obtain the camellia flower extracting solution. According to the method, drying is performed with the refraction window drying technology, superfine crushing is performed, the non-toxic deep-eutectic solvent is taken as an extracting agent, and the production process issimple, efficient, safe and green; the defects that a large quantity of toxic organic solvents and complicated column separation processes are required for production of conventional epicatechin are overcome. The obtained extracting solution has the skin repairing efficacy, the bacteriostasis function and high antioxidation capability and is safe and non-irritant.
Owner:SHANGHAI FOREST CABIN BIOLOGICAL TECH +1

Extraction method of polysaccharide with activities of kidney warming and Yang tonifying from Aspongopus chinensis Dallas insects of Pentatomidae and application of polysaccharide

ActiveCN109280090ARestore immune function activityHigh cure rateAntinoxious agentsUrinary disorderFiltrationYang deficiency
The invention discloses an extraction method of polysaccharide with activities of kidney warming and Yang tonifying from Aspongopus chinensis Dallas insects of Pentatomidae and application of the polysaccharide. The extraction method comprises the following steps: (1) drying Aspongopus chinensis Dallas insect bodies, performing pulverization, performing reflux extraction with petroleum ether, andconducting filtration liquid-solid separation so as to obtain drug residues with removal of grease; (2) evaporating the drug residues, performing reflux extraction with distilled water, performing filtration, combining the filtrate, and performing concentration so as to obtain total water extract; (3) adding distilled water to the total water extract for slight dilution, performing precipitation on polysaccharide with an alcohol solution, performing stirring while the alcohol solution is added, and performing still standing and filtration so as to obtain an insect polysaccharide alcohol precipitate; and (4) adding water to the insect polysaccharide alcohol precipitate for dilution and dissolution, performing chromatography separation and purification by using a DEAE-Sephadex ged cellulosecolumn, and performing rinsing with distilled water and a sodium chloride solution so as to obtain the Aspongopus chinensis Dallas polysaccharide. The invention also relates to the application of thepolysaccharide in preparation of drugs for treating or preventing Yang deficiency, impotence and erectile dysfunctions, the method is easy has simple and convenient operation, and the obtained polysaccharide compound with a purity of up to 95% has strong effects of kidney warming, Yang tonifying, fatigue resistance and body immunity recovery.
Owner:HUBEI UNIV OF CHINESE MEDICINE

Preparation method and application of animal blood active complex peptide

The invention provides a preparation method of an animal blood active complex peptide. The method combines a membrane separation technology and a biologically directional enzyme digestion technology,can effectively protect animal serum protein and polypeptide activities, and can be used for preparing high-activity animal blood active peptide. According to the method, steps including chemical or high-temperature deformation, spray-drying and the like in a traditional animal blood polypeptide extraction process are removed, a grade-by grade extraction mode is adopted, in the same technical process, an active peptide A (plasma ultrafiltration peptide) contained in plasma is first extracted with a 5000Da ultrafiltration membrane, a plasma protein peptide B (plasma protease digestion peptide)is extracted by using plasma subjected to ultrafiltration and concentration as a raw material and conducting direct enzyme digestion, ultrafiltration and reverse osmosis concentration, an active polypeptide complex formed by combining the active peptide A and the plasma protein peptide B is rich and comprehensive in types, and the two active polypeptides can achieve a biological synergistic effectsince the two active polypeptides are complementary after being mixed. Compared with a relatively single animal polypeptide extracted by a traditional process, the active complex peptide has the advantage of stronger effects in the fields of medical treatment, cosmetology, health protection and the like.
Owner:王福芳

Method for extracting antioxidant ingredients from eggplant and product

The invention discloses a method for extracting antioxidant ingredients from an eggplant and a product. The method for extracting antioxidant ingredients from the eggplant comprises the following steps of: cutting the fresh eggplant into pieces; adding 0-30vol% ethanol pulp to the eggplant pieces; centrifuging the serous fluid; penetrating liquid supernatant through a non-polar macroporous resin column, washing the liquid supernatant until the liquid supernatant has no sugar; eluting the liquid supernatant by 40%-100vol% ethanol with volume 3-20 times that of the resin; concentrating and drying the eluant to obtain the eggplant antioxidant extract. The method disclosed by the invention is environment-friendly in extracting process and low in energy consumption; the total antioxidant activity of the extract is equivalent to that of ascorbic acid, and therefore, the method can be extensively applied to the fields including the food field, the medicine and health product field and the like.
Owner:GUANGXI INST OF BOTANY THE CHINESE ACAD OF SCI

Hyaluronic acid fermentation liquor extraction method

The invention belongs to the technical field of microbial polysaccharide production and discloses a hyaluronic acid fermentation liquor extraction method. The method includes the first step of obtaining hyaluronic acid filter liquor A, the second step of conducting decoloring, impurity removal and precipitation, the third step of conducting dissolving and complexing, the fourth step of conducting dissociation and filtering, and the fifth step of carrying out precipitation, dewatering and drying. The extraction method has the advantages of being high in extraction yield and product purity, little in environment pollution and the like.
Owner:SHANDONG FUFENG FERMENTATION CO LTD

Method for extracting tricin from corn bracts

The invention discloses a method for extracting tricin from corn bracts. The method includes the steps that the corn bracts are subjected to normal temperature extraction with water, and extraction residues are obtained; an ethanol solution with the volume fraction of 80% to 90% is used for conducting reflux extraction on the extraction residues, an acid medium is added to the ethanol solution, an obtained extracting solution is subjected to vacuum concentration, and concentrate is obtained; the concentrate is diluted with water, the pH value is adjusted to 7.8 to 8.2, and supernatant is taken after solid-liquid separation; macroreticular resin column chromatography is conducted on the supernatant, and corn bract extract containing tricin is obtained. Normal temperature extraction is firstly conducted with water during alcohol extraction, and therefore protein, polysaccharide and other impurities can be removed in advance. The acid medium is added to the ethanol solution used for reflux extraction, and therefore the extraction efficiency of low-polarity tricin can be effectively improved. The pH value of the concentrate diluent is adjusted to 7.8 to 8.2, at the moment, chlorophyll, protein, polysaccharide and other impurities in the concentrate diluent quickly settle in the weak base environment, and the extraction period of tricin is greatly shortened.
Owner:杭州研谱科技有限公司

Method for extracting podocar-pusflavone from juniper berry meal

The invention discloses a method for extracting podocar-pusflavone from juniper berry meal. The method comprises the steps that reflux extraction is performed on the juniper berry meal through an ethanol solution with the volume fraction of 70%-80% to obtain an extracting solution, and the extracting solution is concentrated under reduced pressure to obtain concentrate; the concentrate is diluted by adding water, solid-liquid separation is performed after standing is performed, and supernatant liquor is taken; the ethanol degree of the supernatant liquor is regulated to be 20%-30% through ethanol, solid-liquid separation is performed after standing is performed, and precipitates are taken; the precipitates are dissolved with a diluted hydrochloric acid solution and then added into a macroporous resin column, elution is performed with water until the pH value of effluent is neutral, then desorption is performed with the ethanol solution, a desorption solution is collected, and the desorption solution is concentrated under reduced pressure and dried to obtain a juniper berry meal extract. According to the method, the steps are simple and convenient, operation is easy, and the method is suitable for industrialized production; due to the fact that only water and ethanol are adopted as the solvent, not only is the cost greatly reduced, but also no stimulation or toxicity is basically generated to operating personnel and the environment; the content of podocar-pusflavone in the juniper berry meal extract reaches up to 30%-40%, and the extraction efficiency is high.
Owner:杭州研谱科技有限公司

A method for extracting biflavonoids from bamboo and cypress from juniper pulp

The invention discloses a method for extracting podocar-pusflavone from juniper berry meal. The method comprises the steps that reflux extraction is performed on the juniper berry meal through an ethanol solution with the volume fraction of 70%-80% to obtain an extracting solution, and the extracting solution is concentrated under reduced pressure to obtain concentrate; the concentrate is diluted by adding water, solid-liquid separation is performed after standing is performed, and supernatant liquor is taken; the ethanol degree of the supernatant liquor is regulated to be 20%-30% through ethanol, solid-liquid separation is performed after standing is performed, and precipitates are taken; the precipitates are dissolved with a diluted hydrochloric acid solution and then added into a macroporous resin column, elution is performed with water until the pH value of effluent is neutral, then desorption is performed with the ethanol solution, a desorption solution is collected, and the desorption solution is concentrated under reduced pressure and dried to obtain a juniper berry meal extract. According to the method, the steps are simple and convenient, operation is easy, and the method is suitable for industrialized production; due to the fact that only water and ethanol are adopted as the solvent, not only is the cost greatly reduced, but also no stimulation or toxicity is basically generated to operating personnel and the environment; the content of podocar-pusflavone in the juniper berry meal extract reaches up to 30%-40%, and the extraction efficiency is high.
Owner:杭州研谱科技有限公司

A kind of polysaccharide extraction method and application of the polysaccharide of the stinkbug stinkbug insect with the activity of warming the kidney and strengthening yang

The invention discloses an extraction method of polysaccharide with activities of kidney warming and Yang tonifying from Aspongopus chinensis Dallas insects of Pentatomidae and application of the polysaccharide. The extraction method comprises the following steps: (1) drying Aspongopus chinensis Dallas insect bodies, performing pulverization, performing reflux extraction with petroleum ether, andconducting filtration liquid-solid separation so as to obtain drug residues with removal of grease; (2) evaporating the drug residues, performing reflux extraction with distilled water, performing filtration, combining the filtrate, and performing concentration so as to obtain total water extract; (3) adding distilled water to the total water extract for slight dilution, performing precipitation on polysaccharide with an alcohol solution, performing stirring while the alcohol solution is added, and performing still standing and filtration so as to obtain an insect polysaccharide alcohol precipitate; and (4) adding water to the insect polysaccharide alcohol precipitate for dilution and dissolution, performing chromatography separation and purification by using a DEAE-Sephadex ged cellulosecolumn, and performing rinsing with distilled water and a sodium chloride solution so as to obtain the Aspongopus chinensis Dallas polysaccharide. The invention also relates to the application of thepolysaccharide in preparation of drugs for treating or preventing Yang deficiency, impotence and erectile dysfunctions, the method is easy has simple and convenient operation, and the obtained polysaccharide compound with a purity of up to 95% has strong effects of kidney warming, Yang tonifying, fatigue resistance and body immunity recovery.
Owner:HUBEI UNIV OF CHINESE MEDICINE
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