The invention discloses an in-situ preparation method for 
cadmium telluride / 
polyvinyl alcohol fluorescent 
fiber and relates to a preparation method for fluorescent 
fiber. The invention aims to solve the problems that in the prior method, the 
quantum dots of 
cadmium telluride reunite easily in a 
polymer solution, the 
fluorescence of the 
fiber is led to be non-uniform, so that the fluorescent effect is poor. The in-situ preparation method comprises the following steps: firstly, 
sodium borohydride, 
tellurium powder and deionized water are mixed and reacted to obtain 
sodium hydrogen telluride solution under the condition of ice-water bath; secondly, 
polyvinyl alcohol solution is added to a three-necked flask, 
nitrogen is introduced to the three-necked flask while the solution in the flask is stirred, then CdCl.2.5 H2O and 
mercaptoacetic acid are added to the flask, 
sodium hydroxide solution is dropwise added to the flask while the solution in the flask is stirred, then sodium 
hydrogen telluride solution is added to the flask, and the solution in the flask is subjected to heating and 
reflux, so that telluride / 
polyvinyl alcohol spinning solution is obtained; and thirdly, the 
spinning solution is subjected to static 
spinning, so that the fluorescent fiber is obtained. With the in-situ preparation method, the 
quantum dots of 
cadmium telluride can be uniformly scattered in 
polymer, and the prepared fluorescent fiber has good fluorescent effect. The in-situ preparation method is used for preparing the fluorescent fiber.