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159 results about "Antimony compounds" patented technology

Antimony forms chemical compounds in three oxidation states: -3, +3, and +5. -3 compounds are called antimonides. They are made by reacting antimony with other metals. They react with acids to make the toxic and unstable gas stibine.

Preparation method for CZTS nano-particle material

A preparation method for a CZTS nano-particle material belongs to the technical field of materials. The method comprises the following steps: first, respectively preparing a reaction system A (dissolving copper salt, antimonic salt and elemental sulfur in ethylene diamine in an ultrasonic manner) and a reaction system B (a water solution of zinc salt and tin salt); then, mixing the system A and the system B in an ultrasonic manner, sealing and heating to 200 DEG C; keeping the the temperature for 7-24 hours for reaction; finally, taking black powder at the lower layer, and obtaining a target product through centrifugation and washing. According to the invention, a moderate amount of an antimony compound is added to allow copper ions and Sb ions to react with the sulfur so as to generate a mobile-phase copper-antimony-sulfur compound and to promote the growth of Cu2ZnSnS4; meanwhile, the crystal grain dimensions of the Cu2ZnSnS4 nano particles are more uniform. The prepared CZTS nano-particle is good in crystallinity, has no other impurity phase, and is more uniform in dimension distribution; the reaction time is greatly shortened under the action of the mobile phase; only sealing and heating equipment is required during the preparation process, so that the preparation steps are simple, and mass production is achieved.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA
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