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119 results about "Mica substrate" patented technology

Method for low-cost preparation of large-size monocrystal graphene

The invention discloses a method for low-cost preparation of large-size monocrystal graphene, relates to a preparation method of monocrystal graphene, and is used for solving the technical problems that in the chemical vapor deposition (CVD) method for preparing the large-size monocrystal graphene material, the common monocrystal substrate surface treatment process is complex, and the monocrystal substrate is difficult to reuse and high in cost. The method disclosed by the invention comprises the following steps of: I, evaporating a monocrystal metal thin film on a monocrystal mica substrate; II, placing the monocrystal metal thin film obtained from the step I into chemical vapor deposition equipment, vacuumizing and filling H2 and Ar, increasing temperature and implementing heat treatment; III, continuing to fill a CH4 gas, and depositing; and IV, closing a heating power supply, stopping filling the CH4 gas, rapidly cooling to room temperature by taking Ar and H2 as protective gases, and promoting uniform growth of high-quality monocrystal graphene on the surface of the monocrystal metal substrate. The monocrystal graphene prepared by the invention is large in size, high in quality and few in defect; and the method disclosed by the invention is applicable to monocrystal graphene material manufacturing field.
Owner:HARBIN INST OF TECH

High-saturation iron-series pigment and production method thereof

The invention provides a high-saturation iron-series pigment and a production method thereof. The high-saturation iron-series pigment is characterized in that: mica is taken as a substrate, high-refractivity substances and low-refractivity substances are alternatively coated on the substrate, the low-refractivity substances include silicon dioxide, aluminum trioxide and diboron trioxide, and the high-refractivity substances include titanium dioxide, tin dioxide, ferric oxide, cobalt oxide, zirconium dioxide and dichromium trioxide. The production method of the pigment is mainly characterized in that: a soluble salt which corresponds to each of the substances is hydrolyzed and precipitated on the surface of the mica substrate at an appropriate pH value, and the precipitated soluble salt is calcined at the temperature of 450-750 DEG C, so that a coating substance is transformed into an oxide. Compared with a synthetic silicon dioxide substrate, the method has the advantages of higher convenience for drawing materials, low price and reduction in the production cost of the high-saturation iron-series pigment. A hydrolyzing coating process is easy to operate and control, the thickness of a coating layer can be controlled through the color phase change of the pigment, and a production process is simple.
Owner:河北欧克新型材料股份有限公司

Method for acquiring large-area high-quality flexible self-supporting single crystalline oxide film based on Van der Waals epitaxy

The invention discloses a method for acquiring a large-area high-quality flexible self-supporting single crystalline oxide film based on Van der Waals epitaxy, and mainly solves a problem in the priorart that a process for preparing the oxide film is complicated. The method comprises the following steps: 1, growing the oxide film on a mica substrate through a pulsed laser deposition technology; 2, spin-coating the surface of the oxide film by polymethyl methacrylate, and soaking in weakly acidic solution, while corners of the film are upwarping, taking out the film and placing in clear water,enabling the film to break away from the mica substrate by using a tension force of the water, and transferring to a follow-up needed substrate, to obtain the large-area high-quality flexible self-supporting single crystalline oxide film. The method is capable of, through using the mica substrate and the weakly acidic solution, acquiring the large-area high-quality flexible self-supporting singlecrystalline oxide film based on the Van der Waals epitaxy, greatly shortening the film preparation time, and preparing the multi-functional oxide film for a flexible electronic device.
Owner:XIDIAN UNIV

Ultra-smooth metal film surface preparation method

The invention discloses an ultra-smooth metal film surface preparation method. The method comprises the steps that firstly, a soft mica substrate is prepared; secondly, a layer of metal film is formed on the surface of the soft mica substrate in a vacuum evaporation mode; thirdly, the metal film is made to be evenly attached to the substrate through initial adhesion between adhesives and the metal film, and a sandwiched structure of the soft mica substrate, the metal film layer and the substrate is formed after solidification; and fourthly, the sandwiched structure obtained in the third step is soaked in a solvent, the substrate is clamped through tweezers and slightly rocked in the solvent or the soft mica substrate is dragged gently, the soft mica substrate on the outermost layer is removed through surface tension of the solvent, and an ultra-smooth metal film surface is obtained. By means of the method, a large-area flexible metal film can be acquired, the stripping process of the soft mica substrate is optimized through attachment of the adhesives, ultra-smooth metal films can be prepared on various kinds of substrates, the roughness of the ultra-smooth metal film surface can reach the atomic level, and the method is applicable to the surface treatment process during mass production.
Owner:山东韩师傅新材料有限公司

Method for preparing two-dimensional indium trisulfide mono-crystals on mica substrate

The invention discloses a method for preparing two-dimensional indium trisulfide mono-crystals on a mica substrate. The method comprises the following steps: S1; washing a mica sheet; S2: preparing materials: weighing 10 to 15mg of indium trisulfide powder; putting indium trisulfide powder on a clean quartz boat; flatly placing the washed mica sheet on the quartz boat; then putting the quartz boatin a tubular furnace; S3: controlling gas flow: completely switching on a gas inlet valve and a gas outlet valve of the tubular furnace; opening an argon gas bottle and adjusting the gas flow mount of a gas flow meter to 500 to 600sccm; introducing argon gas into a quartz pipe of the tubular furnace for 10 to 30min to discharge all air impurities; S4: heating and growing: opening the tubular furnace and raising the temperature to 980 DEG C within 20min; after keeping heat at 980 DEG C for 5 to 10min, naturally cooling to obtain the two-dimensional indium trisulfide mono-crystals. The method disclosed by the invention has the advantages of simple needed equipment and preparation technology, short growth time, capability of directly obtaining two-dimensional indium trisulfide with good crystallization degree relatively high purity and relatively large size and the like.
Owner:GUANGDONG UNIV OF TECH

Method for preparing non-layered two-dimensional nano-cadmium sulfide crystal material and product

ActiveCN108048900ARaise the energy barrier of crystal facet reactionAchieve independent controlPolycrystalline material growthNanotechnologyProduct gasOxygen
The invention belongs to the field of cadmium sulfide crystal materials, and discloses a method for preparing a non-layered two-dimensional nano-cadmium sulfide crystal material and the product. The method includes the following steps that (a) a reaction vessel is selected and divided into an upstream area, a central area and a downstream area, and a Cd source and an S source are selected and separately placed in the upstream area; (b) an In compound is selected as a surface inhibitor and placed in the central area, and mica is selected as a substrate and placed in the downstream area; (c) inert gas is introduced into the reaction vessel to isolate oxygen for a reaction, and after the reaction, the desired non-layered two-dimensional nano-cadmium sulfide crystal material is formed on the mica substrate. The invention further discloses the product prepared through the method. By means of the method, the requirement for large-batch preparation of the two-dimensional nano-CdS crystal material is met, and the product has a flat crystal surface and a uniform morphology and is uniform in element distribution; besides, rich raw materials are available, the price is low, the preparation method is simple, and large-scale production and promotion are convenient.
Owner:HUAZHONG UNIV OF SCI & TECH

Method for growing single crystal [gamma]-phase indium selenide film on mica substrate

The invention relates to a method for growing a single crystal [gamma]-phase indium selenide film on a mica substrate. The method comprises the following steps of: the step 1) chemically cleaning andmechanically cleaving a single crystal mica substrate to peel off a surface layer to obtain a flat mica substrate with a clean surface; the step 2) transferring the mica substrate prepared in the step1) into a molecular beam epitaxy vacuum system, performing heating to a temperature of 450 DEG C, and performing degassing until the vacuum degree of the system is better than 8*10 <-10> mbar; the step 3) after the mica is degassed, performing natural cooling to a growth temperature range, and simultaneously opening an In beam flow source and a Se beam flow source to start to grow an In2Se3 film;and the step 4) immediately stopping heating the substrate after the film growth is finished, and quickly cooling the substrate to a room temperature to obtain the single crystal [gamma]-phase In2Se3film. According to the method for growing the In2Se3 film, the In2Se3 film is deposited and grown on the surface of the mica substrate by utilizing a molecular beam epitaxy technology, and the high-quality single crystal [gamma]-phase In2Se3 film can be prepared at a lower growth temperature.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA
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