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2 results about "Starch indicator" patented technology

Starch is often used in chemistry as an indicator for redox titrations where triiodide is present. Starch forms a very dark blue-black complex with triiodide which can be made by mixing iodine with iodide. However, the complex is not formed if only iodine or only iodide is present. The colour of the starch complex is so deep, that it can be detected visually when the concentration of the iodine is as low as 0.00002 M at 20 °C. The colour sensitivity decreases with increasing temperature, and upon the addition of organic solvents such as ethanol or propanone. During iodine titrations, concentrated iodine solutions must be reacted with some titrant, often thiosulfate, in order to remove most of the iodine before the starch is added. This is due to the insolubility of the starch-iodine complex which may prevent some of the iodine reacting with the titrant. Close to the end-point, the starch is added, and the titration process is resumed taking into account the amount of thiosulfate added before adding the starch. To prepare starch indicator solution, add 1 gram of starch into 10 mL of distilled water, shake well, and pour into 100 mL of boiling, distilled water.

A nitrite high-sensitivity rapid detection kit and a detection method

PendingCN122330094ARisk classificationBiology
This invention provides a highly sensitive and rapid nitrite detection kit and method. The kit includes a detection solution, a standard colorimetric card, and test tubes. The molar ratio of sulfuric acid, potassium iodide, and starch indicator is 3:4:39. This invention solves the problems of existing nitrite detection technologies, such as reliance on specialized instruments and laboratory environments, cumbersome and time-consuming operation, inability to meet the needs of on-site, real-time testing, poor matrix compatibility of detection kits, lack of graded warnings based on national food safety standards and toxicological risks, insufficient reagent stability, and difficulty in balancing detection sensitivity and accuracy. It features convenient operation, suitability for on-site, real-time testing; excellent detection performance, accurate and reliable results; stable physicochemical properties of the detection solution, good storage properties; intuitive risk classification, and strong practicality.
Owner:INNER MONGOLIA UNIVERSITY

Industrial anhydrous hydrogen fluoride oxidizing impurity detection method

The invention relates to the technical field of chemical test methods, and particularly discloses a method for detecting oxidizing impurities in industrial anhydrous hydrogen fluoride, which comprises the following steps: S1, in a fuming cupboard, in a closed container made of a hydrofluoric acid-resistant material, mixing an original sample of industrial anhydrous hydrogen fluoride with quantitative crushed ice to obtain a diluted sample with the hydrogen fluoride mass fraction of 45-55%, calculating a dilution coefficient X; s2, accurately weighing a diluted sample with the mass of m, sequentially adding a starch indicator solution and a potassium iodide solution into a reaction vessel made of a hydrofluoric acid-resistant material, uniformly mixing, and carrying out sealed and dark standing reaction for 1-3 minutes; s3, titrating the solution obtained in the step S2 by using a sodium thiosulfate standard titration solution with the concentration of c, and recording consumption V; and S4, calculating the content of the oxidizing impurities in the industrial anhydrous hydrogen fluoride original sample according to a formula C (ppm) = [((V-V0) * c * M) / (m * X)] * 1000. The invention provides a safe and accurate detection method by combining crushed ice dilution, specific concentration window control and iodometry.
Owner:GUIZHOU WENGFU LANTIAN FLUORCHEM CO LTD