503 results about "Sulfur oxide" patented technology

The invention relates to the technical field of coal-fired power plant environmental protection, in particular to a coal-fired power plant intelligent environmental protection island control system based on multi-source data fusion. Comprising a multi-source data acquisition module, a data transmission module, a data preprocessing module, a multi-source data fusion module, an operation state analysis module, an intelligent control decision module, a control instruction execution module and a man-machine interaction module. According to the coal-fired power plant intelligent environmental protection island control system based on multi-source data fusion, equipment operation, environmental monitoring, power grid, fuel and meteorological data are widely acquired through the multi-source data acquisition module, the limitation of a single data source of a traditional system is broken through, a distributed Kalman filtering algorithm is combined with a neural network algorithm for data fusion, and the data fusion efficiency is improved. According to the method, the incidence relation between data can be deeply mined, temperature and pressure parameters of desulfurization equipment and flue gas sulfur dioxide concentration data are subjected to fusion analysis, the reason of desulfurization efficiency reduction can be accurately positioned, and compared with traditional single data source judgment, the fault diagnosis accuracy is improved.

The invention relates to a device and a method of a high-sensitivity suspension single-droplet sensor for monitoring PM2.5 pollution, belongs to the technical field of aerosol microdroplet spectrum trace analysis, and solves the problem that ppb-magnitude gas cannot be monitored in the prior art. The method comprises the following steps: pumping aerosol into a sample cell of a droplet suspension system in a single droplet form; introducing required reaction gas into the sample pool through an atmosphere control system; scattered light signals of the single liquid drops are respectively input into the dynamic signal processing system and the microdroplet imaging system; acquiring the characteristic peak displacement change of the metal ion sensing microdroplet; establishing a gas particle distribution Mie scattering inversion model based on micro-droplet dynamic response; inverting the radius of the liquid drop according to the stimulated Raman scattering / stimulated elastic scattering signal; according to the quantitative relationship of the reaction, calculating the generation of sulfate by the droplet suspension system (sensor); and judging which gas in the actual atmosphere is a main oxidation pathway for oxidizing sulfur dioxide to generate sulfate pollutants according to a calculation result.

The invention relates to the technical field of industrial waste gas treatment, in particular to a waste gas treatment system and method based on wet desulphurization. The system comprises a waste gas pretreatment unit, a composite absorption reaction unit, a gas-liquid separation unit, an absorption liquid circulation system, an intelligent control system and a waste liquid treatment unit, wherein each unit is communicated with a shielding signal line through a corrosion-resistant pipeline to form a closed-loop operation system; industrial waste gas is subjected to pre-dedusting and cooling through the waste gas pretreatment unit and then enters the composite absorption reaction unit to be in countercurrent contact with a composite absorbent to achieve sulfur dioxide removal, a gas-liquid mixture obtained after reaction is separated through the gas-liquid separation unit, purified gas is directly discharged, and absorption liquid enters the absorption liquid circulation system to be recycled. And the saturated absorption liquid with the density of 1.15-1.25 g / cm < 3 > is conveyed to a waste liquid treatment unit for treatment. According to the invention, sulfur dioxide in waste gas can be efficiently removed through synergistic absorption and intelligent control, the operation cost is reduced, and equipment corrosion is reduced.

The invention relates to the technical field of atmospheric science and remote sensing, in particular to a volcanic sulfur dioxide vertical section inversion method based on a Lagrange diffusion model, and the method comprises the steps: obtaining volcanic eruption total mass constraint, satellite sulfur dioxide column concentration and effective pixels, three-dimensional meteorological driving data and chemical clearing parameters; calculating a vertical weighting function by utilizing a radiation transmission mode, and generating initial vertical distribution by combining with a column concentration layering ratio; constructing a diffusion model to simulate an air mass backward track and match observation pixels to obtain attribution air mass distribution; optimizing a volcanic sulfur dioxide vertical emission profile time sequence based on attribution distribution and total mass constraint; and inputting the sequence into a diffusion model for forward simulation, comparing satellite observation data to calculate a verification index, correcting a diffusion coefficient according to a threshold value, and outputting a target vertical emission profile time sequence. According to the method, through backward trajectory attribution and forward verification closed-loop optimization, the volcanic sulfur dioxide vertical distribution inversion precision is remarkably improved.

The invention discloses a desulfurizing agent for a cement kiln as well as a production method and application of the desulfurizing agent. The desulfurizing agent is prepared from the following raw material components in percentage by weight: 88-96 wt% of limestone; 2-6 wt% of an iron raw material; 1-6 wt% of gypsum; and 0-4 wt% of a silicon-aluminum material. The desulfurizer is produced by utilizing a kiln line of a cement enterprise, is dried and ground with raw materials according to a mass ratio of 1: 100 to 3: 100, and then is put into a cement kiln system for cement clinker production, so that the emission concentration of sulfur oxides in kiln tail flue gas produced by sulphoaluminate cement clinker can be reduced from more than 2000mg / Nm < 3 > to less than 35mg / Nm < 3 >; and for other types of cement clinker, the content of the cement clinker can be reduced from 1000 mg / Nm < 3 > or above to 35 mg / Nm < 3 > or below, the desulfurization effect is stable, and the environment-friendly emission requirement can be continuously met.

The application provides a preparation method of ergothioneine and application of a mercapto compound in the method. The method comprises the following steps: in the presence of a catalyst system, a sulfur oxide is reacted to generate ergothioneine. The catalyst system comprises a first catalyst and a second catalyst. The first catalyst is ergothioneine synthase, and the second catalyst is one or more of a mercapto-containing amino acid and a mercapto-containing polypeptide. The preparation method of ergothioneine provided by the application does not need to use a large amount of a chemical mercaptan reagent with a foul smell, has the advantages of high efficiency, green environmental protection, and friendly production scene, and is beneficial to industrial production of ergothioneine.

The invention belongs to the field of medicine, health and health, and particularly relates to a preparation method for controllably synthesizing polysulfonic acid mucopolysaccharide with different molecular weights, which comprises the following steps: reaction, acid-base neutralization, formamide removal by alcohol precipitation, desalting and freeze-drying. Wherein the reaction process comprises the following steps: adding sodium chondroitin sulfate and a pyridine sulfur trioxide complex into a mixed solvent of N, N-dimethylformamide and dimethyl sulfoxide, and heating for reaction to obtain a reaction mixture; the volume fraction of the dimethyl sulfoxide in the mixed solvent is 0-80%. According to the method, the low-price pyridine sulfur trioxide complex (about 150 yuan / 500g) is used, and the ratio of N, N-dimethylformamide to dimethyl sulfoxide in the mixed solvent is adjusted, so that the solubility of the chondroitin sulfate sodium and the pyridine sulfur trioxide complex is changed, and the polysulfonic acid mucopolysaccharide with molecular weights in different ranges can be regulated and generated.

The invention provides a prebaked anode flue gas carbon capture integrated system which comprises an integrated purification unit, a pollutant removal unit and a pressure swing adsorption carbon capture unit which are sequentially connected through a pipeline, flue gas is subjected to dust pre-removal and organic pollutant adsorption of the integrated purification unit and deep treatment of nitrogen and sulfur oxides of the pollutant removal unit, and the flue gas is subjected to carbon capture and carbon capture. According to the invention, the flue gas enters the pressure swing adsorption unit and then is efficiently captured by the pressure swing adsorption unit, and a continuous and synergistic treatment chain is formed in the whole process, so that the heat loss of the flue gas transmitted among the units is obviously reduced, and the energy waste caused by equipment dispersion in the traditional system is avoided; meanwhile, in the aspect of equipment layout, the modular integrated design greatly compresses the occupied area, efficient utilization of an industrial site is achieved, the flue gas treatment cost is reduced, and the flue gas treatment reliability is improved.

In some embodiments, the present disclosure relates to a system. The system includes a substrate and a fluid trapping material formed on one or more surfaces of the substrate. The fluid capture material includes a sorbent material incorporating one or more fluids including water, carbon dioxide, sulfur oxides, alcohols, or a combination thereof. The fluid capture material also includes one or more binder materials, wherein the binder materials are optionally at least partially cross-linked. The fluid capture material includes at least one aperture.

The invention discloses a flue gas treatment device based on a noble metal catalyst, and relates to the technical field of flue gas treatment. An inner mounting frame is fixedly mounted on the inner surface wall of the treatment box, an annular outer frame is fixedly mounted on one side of the outer wall of the inner mounting frame, and a rotating groove is pre-formed in the annular outer frame. Through a multi-stage collaborative filtering mechanism, a clean reaction environment is provided for a noble metal catalyst: a linkage frame drives a filter plate to rotate, and large-particle impurities, sulfur oxides and chlorides are intercepted by utilizing centrifugal force and a composite filter material (a stainless steel filter screen and activated carbon); the guide vanes form spiral airflow, and fine impurities with the particle size larger than or equal to 1 micron are separated through centrifugal force; the metal filter pipe is combined with dynamic negative pressure adsorption, deep removal of residual dust and three-stage filtration, so that the impurity content in flue gas can be greatly reduced, catalyst poisoning, blockage or sintering are avoided, the service life of the catalyst is prolonged, and the replacement cost of precious metal is greatly reduced.

Provided herein are methods and systems for treating a sulfur dioxide-containing gaseous stream. The method includes combusting a tail gas in an excess of oxygen gas to yield a thermal oxidizer effluent containing sulfur dioxide and oxygen. The thermal oxidizer effluent is introduced to an oxidative catalytic converter to convert sulfur dioxide to sulfur trioxide, thereby forming an oxidized gas stream. The oxidized gas stream is routed to a quench tower and contacted with a dilute aqueous acid quench stream to yield sulfurous acid, hydrated sulfur dioxide, or both. The sulfurous acid or hydrated sulfur dioxide is oxidized with the excess of oxygen from the thermal oxidizer effluent to yield sulfuric acid.

A system is described that enables the purification of COx, SOx, NOx, dioxin and furan, and H2S gases using wet and dry filters in a single chimney, comprising: a nozzle system (2) that sprays a mixture consisting of water, micronized zeolite, ammonia, and boron mineral in fine droplets to perform the first purification of SOx (sulfur oxides), NOx (nitrogen oxides), and COx (carbon oxides) gases entering the chimney (1) from the combustion gas, a zeolite-based dry filter (3) that purifies the dioxin and furan components in the flue gas (B) rising after the first purification, a first continuous measurement system (4) that measures the values of the combustion gas at the entry point to the chimney (1), a second continuous measurement system (5) that measures the values of the combustion gas after the dry filter (3), an Al-supported processor (6) that adjusts the amount of the mixture to be sprayed from the nozzle system (2) based on the comparison of the first continuous measurement system (4) and the second continuous measurement system (5).

The utility model relates to a tin bath sulfur dioxide blowing device which comprises a sulfur dioxide generating device used for generating small-flow sulfur dioxide gas, and the sulfur dioxide generating device is led into a blowing pipe; the blowing pipe is a metal pipe body, one end of the metal pipe body is sealed, the other end of the metal pipe body is connected to the sulfur dioxide generating device through a hose, a small hole is formed in the sealed end, and a nozzle is arranged at the position of the small hole; a flow meter is arranged on the hose and is used for monitoring the flow of sulfur dioxide in the blowing pipe to be small flow; a support is arranged on the metal pipe body, and the blowing pipe is fixed to the positions of climbing rollers, attached with tin sulfide, of the first to third transition roller tables through the support. Sulfur dioxide is blown to the roller through the small holes, sulfur dioxide and tin sulfide are subjected to a chemical reaction, SO2 and the glass plate can generate a Na2SO4 thin film protection layer capable of being wiped off under the high-temperature condition, the Na2SO4 thin film protection layer is attached to the lower surface of the glass plate, and the hardness of the glass plate is increased. The probability of gouges and abrasion is reduced, and the problem of quality defects is solved.

The utility model discloses a diesel generator flue gas purification mechanism for civil air defence engineering, including air inlet pipe and purification bin, the air inlet pipe one end is linked with diesel generator exhaust pipe in civil air defence engineering power generation room intercommunication, the other end of air inlet pipe is inserted into the purification bin and the opening direction is perpendicular to downward, the open end position of air inlet pipe in the purification bin is connected with the shunt joint, each interface of shunt joint all is connected with the jet pipe that the air hole of pipe body lateral wall is evenly set up, the utility model relates to civil air defence engineering technical field, utilize liquid supply booster pump and press into the spray subassembly in alkaline solution (15% magnesium hydroxide compound agent), and further via spray subassembly to the spray of filler layer, make the nitrogen monoxide, nitrogen dioxide, sulfur dioxide and particulate matter etc. in tail gas contact with the alkaline water mist in purification bin and filler layer, to the purification treatment of nitrogen monoxide, nitrogen dioxide, sulfur dioxide and particulate matter.

The invention relates to a filter unit for removing gaseous compounds (nitrogen oxides, sulfur oxides, volatile organic compounds, carbon monoxide and the like) and bacteria and viruses from interior air, in particular interior air of a motor vehicle, the invention also relates to a method for removing gaseous harmful substances and bacteria and viruses from interior air, in particular interior air of a motor vehicle.

The invention discloses a thermal power plant boiler flue gas desulfurization and denitrification integrated method, namely, a chemical absorption and catalytic reduction combined mode is researched to effectively treat sulfur oxide sulfur (SO2) and nitrogen oxide (NOx). The method comprises the following steps: firstly, converting sulfur-containing emissions into harmless substances by using a redox agent through a wet desulphurization technology, and then converting NOx into nitrogen and water by applying a selective catalytic reduction (SCR) technology. Operation data analysis shows that the removal rates of SO2 and NOx respectively reach 97% and 94%, and the desulfurization and denitrification efficiency is far higher than that of a traditional thermal power plant boiler. According to the desulfurization and denitrification integrated technology, the limitation of a traditional desulfurization and denitrification technology is broken through, and a new technical scheme is provided for a thermal power plant.

The utility model discloses a countercurrent absorption device for sulfurous acid, which consists of a process water pipe, a tail gas fan, a third-stage absorption tower, a second-stage absorption tower, a shower nozzle, a first-stage absorption tower, a finished product acid pump, a sulfur furnace, a circulating acid pump and a baffle plate. According to the sulfur dioxide absorption tower disclosed by the invention, the problems that sulfur dioxide gas is not thoroughly absorbed and tail gas pollutes the environment in a sulfurous acid preparation process are solved by adopting countercurrent absorption of the flow direction of sulfur dioxide gas and the flow direction of process water and adopting an absorption mode of combining a shower nozzle and baffle plate water distribution; the sulfur dioxide gas absorption efficiency is high, and equipment and power energy are saved.

This invention discloses a process for preparing high-purity vinyl sulfite using a jet-type loop reactor. Based on the jet-type loop reactor, it employs multiple catalytic systems, using ethylene oxide and sulfur dioxide as raw materials, combined with relevant solvents. This invention relates to the field of vinyl sulfite technology. This process for preparing high-purity vinyl sulfite using a jet-type loop reactor enhances gas-liquid mass transfer through an external circulation jet-type loop reactor. Combined with optimized raw material pretreatment, the reaction cycle is shortened to 2.5-3.0 hours, improving efficiency by more than 50% compared to batch processes. The entire process is continuous, with equipment utilization exceeding 85%, suitable for large-scale production of tens of thousands of tons per year. It addresses the shortcomings of existing processes in terms of scalability, achieving high production efficiency and significant scalability advantages. Furthermore, the entire process is a closed loop, preventing sulfur dioxide leakage. Excess sulfur dioxide is recovered, and solvents are recycled, reducing pollutant emissions by more than 80%.

The present application relates to the technical field of health, environmental management and resource development, and discloses an alkaline-sulfur oxidizing bacteria and its application in water pollution treatment and bioleaching. The alkaline-sulfur oxidizing bacteria is named 381-2, which has been preserved in the China General Microbiological Culture Collection Center on December 23, 2024, and the preservation number is CGMCC No. 33017; the microbial classification name is Stutzerimonas sp. The present application isolates a new species of Stizolobium strain from a deep-sea hydrothermal area Stutzerimonas sp. . The strain has strong and rapid oxidation ability of thiosulfate ions, and also has the characteristics of producing alkali, so it can be applied to the fields of water pollution treatment and bioleaching.

The invention discloses a system and a method for generating power by utilizing sulfur dioxide in boiler flue gas. The system comprises a boiler induced draft fan rear flue, a sulfur dioxide absorption module and a flue gas emission module, the method comprises the following steps: flue gas discharged from a rear flue of a boiler induced draft fan enters a first inlet of a sulfur dioxide absorption module, an iodine solution of the sulfur dioxide absorption module is sprayed out from an atomizing nozzle from top to bottom and the flue gas from bottom to top, and a filler layer is arranged between the atomizing nozzle and the flue gas inlet to increase the contact between the flue gas and the iodine solution; iodine, sulfur dioxide and water react to generate a hydrogen iodide solution and a sulfuric acid solution, and flue gas with absorbed sulfur dioxide is discharged into the flue gas discharge module from a first outlet of the sulfur dioxide absorption module. Through the closed-loop process of iodine solution absorption-hydrogen iodide decomposition-hydrogen fuel cell power generation, the limitation that only pollutant removal is concerned in the traditional desulfurization technology is broken through.

This invention belongs to the field of mineral processing technology, specifically relating to a selective sulfidation roasting-flotation separation method for a smithsonite-calcite mixed ore. The method first involves crushing and grinding the smithsonite, calcite, and sulfiding agent, then mixing them in a certain proportion and subjecting them to sulfidation roasting, preferentially causing the smithsonite to undergo sulfidation. After cooling the roasted product in an inert atmosphere, flotation separation is performed using xanthate as a collector to obtain zinc concentrate. By controlling the atmospheric conditions during the sulfidation roasting process, the sulfidation reaction efficiency of the smithsonite can be improved, and the generation of sulfur oxide gases during roasting can be reduced. When using this method to process the smithsonite-calcite mixed ore, effective recovery of the smithsonite can be achieved, with a flotation recovery rate exceeding 88%. This invention features a simple process flow and easily controllable operating conditions, providing a new technical approach for the efficient utilization of smithsonite resources.

The invention belongs to the field of chemical reagent moisture detection, and particularly relates to a coulometry Karl Fischer reagent for aldehyde ketone moisture detection and a preparation method of the coulometry Karl Fischer reagent. The coulometry Karl Fischer reagent for aldehyde ketone moisture detection is prepared from the following components in parts by weight: 1 to 15 percent of imidazole, 1 to 15 percent of 2-methylimidazole, 25 to 70 percent of ethylene glycol monomethyl ether, 5 to 30 percent of trichloromethane, 2 to 30 percent of trifluoroethanol, 2 to 10 percent of sulfur dioxide, 1 to 10 percent of methyl iodide, 0.1 to 5 percent of tetrabutylammonium iodide and 0.1 to 5 percent of iodine. The method does not contain hydroxyl compounds, effectively inhibits the generation of side reactions in detection, ensures the detection accuracy, and improves the product stability and effectively shortens the instrument equilibrium time by adding iodomethane and tetrabutylammonium iodide.

This invention provides a hydrocarbon gas separation system, comprising a double-layered tube assembly and a negative pressure system. The double-layered tube assembly includes a medium delivery inner tube, a multi-layered membrane assembly, an annular interlayer gap, and a pressure-bearing protection section outer tube. The double-layered tube assembly is sealed at both ends. The multi-layered membrane assembly includes a retention layer, an isolation layer, and a selectively permeable membrane layer. The medium delivery inner tube is nested inside the pressure-bearing protection section outer tube and encloses the multi-layered membrane assembly. The negative pressure system is connected to the double-layered tube assembly. After the mixed gas is processed by the multi-layered membrane assembly in the medium delivery inner tube, sulfur dioxide is retained. The hydrocarbon gas enters the annular interlayer gap for extraction, and the retained sulfur dioxide is released back into the gas. Finally, the gas enters a sulfur dioxide detection instrument and is detected using ultraviolet fluorescence, making the data more consistent with the actual value and providing a scientific basis for relevant decision-making.

A RedOx furnace and process is provided for regenerating a spent sulfuric acid stream or other sulfur-containing stream by decomposing the spent sulfuric acid stream and / or other sulfur-containing stream to recover sulfur dioxide from the streams. The RedOx furnace includes a reduction chamber having an interior atmosphere, an oxidation chamber having an interior atmosphere positioned downstream from, and in fluid communication with, the reduction chamber, an inlet for supplying a spent sulfuric acid stream or other sulfur-containing stream into the interior atmosphere of the reduction chamber, and an inlet for supplying a pure oxygen stream into the interior atmosphere of the reduction chamber.

This invention relates to a rare earth denitrification catalyst, its preparation method, and its application. The rare earth denitrification catalyst comprises rare earth element single atoms and a titanium dioxide-based composite oxide doped with rare earth single atoms. The rare earth element single atoms in this invention exhibit a high adsorption priority for sulfur dioxide, allowing the position and quantity of sulfate to be controlled by the rare earth element single atoms. Furthermore, the hydroxyl groups in the sulfate can enhance the acidity of the catalyst, thereby further improving its redox capacity. The titanium dioxide-based composite oxide can effectively inhibit sulfur dioxide poisoning and further improve the catalyst's denitrification ability in the presence of sulfur dioxide. The rare earth denitrification catalyst of this invention maintains high catalytic activity even in the presence of sulfur dioxide, exhibiting excellent denitrification and sulfur resistance performance.

A slurry reactor liquefied gas desulfurization device and a desulfurization method thereof relate to the technical field of liquefied gas treatment, and comprise a fixed bed reactor, a mercaptan removal tank, a water washing tank, an alkali liquor oxidation tower and an alkali liquor tank, a top inlet of the fixed bed reactor is communicated with liquefied gas obtained by desulfurization of a lean amine solution through a pipeline, a bottom outlet of the fixed bed reactor is communicated with a top inlet of the mercaptan removal tank through a pipeline, and a top outlet of the mercaptan removal tank is communicated with a top inlet of the washing tank through a pipeline; an outlet in the top of the washing tank is communicated with a refined liquefied gas pipe network through a pipeline; a bottom outlet of the mercaptan removal tank is communicated with a bottom inlet of the alkali liquor oxidation tower through a pipeline, a bottom outlet of the alkali liquor oxidation tower is communicated with a top inlet of the mercaptan removal tank through a pipeline, and one side of the lower end of the alkali liquor oxidation tower is connected with an air inlet pipeline; according to the method, mercaptan in liquefied gas can be removed, sulfur dioxide is prevented from being generated after combustion, acid rain and air pollution are reduced, meanwhile, consumption of alkali liquor can be reduced, and the discharge amount of waste alkali liquor is reduced.

The application belongs to the technical field of chondroitin sulfate preparation, and particularly relates to application and application method of liquid sulfur dioxide in preparation of chondroitin sulfate or chondroitin sulfate salt. In the application, liquid sulfur dioxide is used as a solvent to perform sulfonation modification treatment on unsulfated chondroitin, on the one hand, the use of traditional high-boiling organic reagents is avoided, the difficulty of three-waste treatment is reduced, and the process is more green and environmentally friendly; on the other hand, the post-treatment operation of the sulfonation reaction is simpler, and sulfur dioxide can be removed from the system by only temperature control or pressure adjustment, so that solvent residues possibly existing in the final product are avoided, and the product is safer. In addition, by adjusting the key conditions of the sulfonation reaction, the proportion of chondroitin sulfate with 6 independent sulfation in the disaccharide unit of the sulfonation product is 70% to 90%, the reaction is stable and reliable, and the sulfonation rate is high.

The invention relates to a limestone-gypsum wet desulphurization method and system.The method comprises the steps that desulfurized rich slurry is heated through a rich liquid heater and desorbed through a flash desorption device in sequence, obtained flash desorption steam is purified through a purification treatment unit, and desorbed sulfur dioxide gas can be obtained; and treating at least part of the desulfurized lean slurry by a gypsum treatment unit to obtain a gypsum product. By adopting the method disclosed by the invention, the discharge amount of the gypsum can be reduced and the quality of the gypsum can be improved while resource recycling of the sulfur is realized. Besides, the obtained desorbed sulfur dioxide gas can be converted into chemical products through subsequent process treatment, so that the current situation of sulfur resource shortage is relieved.

The invention discloses a synthesis process of tungsten hexafluoride, and relates to the technical field of special gas synthesis. The process comprises the following steps: mixing ammonium fluoride and hydrofluoric acid to prepare an activation solution, carrying out ultrasonic activation treatment on tungsten powder to obtain pretreated tungsten powder, and reacting the pretreated tungsten powder with fluorine gas at a certain temperature and pressure to prepare a liquefied crude product tungsten hexafluoride; the preparation method comprises the following steps: by taking aluminum sec-butoxide and the like as raw materials, carrying out sol-gel and ethanol supercritical drying and calcining to prepare highly porous activated aluminum oxide; gasifying the crude tungsten hexafluoride, adsorbing with activated aluminum oxide, and rectifying to obtain purified tungsten hexafluoride liquid; and finally, dissolving in liquid sulfur dioxide, treating under illumination with the wavelength of 395nm, and carrying out distillation separation to obtain high-purity tungsten hexafluoride. According to the method, the activation pretreatment is combined with multi-stage purification, so that the purity and the synthesis efficiency of tungsten hexafluoride are remarkably improved.