The invention belongs to the technical field of environmental
pollution control, and particularly relates to a preparation method of a flexible carbon / MoS2
heterojunction adsorption material and application of the flexible carbon / MoS2
heterojunction adsorption material as an adsorbent. The preparation method comprises the following steps: S1, cleaning waste
cellulose fibers with deionized water and
ethanol,
drying, heating to 700-900 DEG C for
carbonization in an
inert atmosphere, and preserving heat for 1-3 hours to obtain a flexible
carbon skeleton substrate with a complete structure; s2, carrying out oxidation treatment on the
carbon skeleton substrate in an
air atmosphere at 200-400 DEG C for 0.5-2 hours; s3, a
molybdenum source and a
sulfur source are dissolved in deionized water according to the
molar ratio of Mo to S being 1: 2-1: 20; immersing the oxidized
carbon skeleton substrate into the precursor solution, putting into a reaction kettle, and carrying out
hydrothermal reaction at 140-200 DEG C for 6-18 hours; and washing the product, and carrying out
vacuum drying. The flexible
heterojunction material prepared by the method has macroscopic flexibility, super-hydrophilicity and abundant high-activity sites, and can be directly used as a self-supporting adsorption film; the defects that a traditional
powder adsorbent is difficult to separate and easy to lose are overcome.