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56results about How to "Clear grain" patented technology

Preparation method of metallographic samples of zirconium and zirconium alloy

The invention relates to a preparation method of metallographic samples of zirconium and zirconium alloy. The preparation method comprises the following steps: (a) sample pretreatment, namely sampling a to-be-tested material, ultrasonically cleaning to remove oil stain on the surface of a sample; (b) coarse grinding and fine grinding, namely grinding the sample processed in the step (a) on metallographic sand paper, wherein particle size marks of the utilized sand paper sequentially are 400#, 800#, 1200#, 2000# and 3000#; (3) chemical polishing, namely preparing a solution in a volume ratio that HF to HNO3 to H2O is 10 to 45 to 45, dipping the solution with an absorbent ball, and lightly wiping the surface of the sample with the absorbent ball for several times until the surface of the sample presents a polished surface as bright as a mirror; (d) cleaning, namely lightly wiping the surface of the polished sample in the step (c) by dipping absolute ethyl alcohol with the absorbent ball so as to remove complexes generated by chemical polishing; (e) oxidation cooling, namely dehydrating the cleaned sample, arranging the sample in a constant temperature region of a muffle furnace for oxidation for 2-10 minutes until the color of the surface of the sample is changed from bright white to faint yellow, taking out the sample, cooling, and carrying out metallographic observation and particle size evaluation.
Owner:HUNAN UNIV

No-salt pickling-free short-process no-chrome tanning method

The invention discloses a no-salt pickling-free short-process no-chrome tanning method. One the basis of advantages and disadvantages of chrome and requirements for environment protection, the no-salt pickling-free no-chrome tanning method suitable for production and feasible is needed at the present, and the finished leather quality of the method can be favorably compared with that of a traditional chrome tanning technology. The no-salt pickling-free short-process no-chrome tanning method comprises the steps that softened naked leather is directly tanned with no-chrome tanning agents to obtain wet white leather; the uniformly shaved wet white leather is tanned with substitute type synthetic tanning agents, then tanned with vegetable tanning agents and finally tanned with a defined amount of aluminum tanning agents; and a no-salt pickling-free no-chrome tanning leather blank is obtained. According to the no-salt pickling-free short-process no-chrome tanning method, the shrinkage temperature of the obtained no-chrome tanning crust leather is higher than 95 DEG C, and a body of the finished leather is soft and rich and capable of being favorably compared with chrome tanning leather in the quality, performance and other aspects; and meanwhile, the pickling process is omitted, the tanning time is shortened, and the consumption of sodium chloride and chrome salt in the leather production process and the pollution of the sodium chloride and the chrome salt to human and the environment are eradicated.
Owner:JIAXING UNIV

Metallographic corrosion method and metallographic corrosive agent for aluminum alloy

ActiveCN114318341APrevent smearingCorrosion method is simplePreparing sample for investigationHydrogen SulfateGrain boundary
The invention discloses an aluminum alloy metallographic corrosion method and a metallographic corrosive agent thereof. The metallographic corrosion method comprises the following steps that a, a 7055 aluminum alloy sample is subjected to pre-cleaning, hot inlaying, mechanical grinding and mechanical polishing treatment, washed with clear water and blow-dried, and then a metallographic sample is obtained; b, sequentially adding nitric acid, hydrochloric acid, sulfuric acid, hydrofluoric acid and deionized water into a container, and mixing to obtain a metallographic corrosive agent, wherein the metallographic corrosive agent comprises the following components in percentage by volume: 4-5% of nitric acid, 2-3% of hydrochloric acid, 1.5-2.5% of sulfuric acid, 2.5-3.5% of hydrofluoric acid and the balance of deionized water; and c, pouring the metallographic corrosive into a culture dish, placing the culture dish in a constant-temperature environment of 22-28 DEG C, immersing the metallographic sample into the metallographic corrosive, corroding for 25-35 seconds, taking out, washing, drying, and observing. The corrosion method is simple, the corrosion time is short, the effect of the metallographic corrosive agent is fully exerted, and the crystal boundary and crystal grains of the 7055 aluminum alloy are clearly displayed.
Owner:DONGFENG MOTOR GRP

Chromium-contained retaining-filling agent and preparation method thereof

The invention provides a preparation method of a chromium-contained retaining-filling agent. The method comprises the steps that (1), 100 parts of chrome leather scrap hydrolysate, 20 parts to 100 parts of retanning agents, 1 part to 5 parts of masking agents and 3 parts to 5 parts of fatting agents are metered, then, the masking agents and the solid retanning agents are dissolved with water, the fatting agents are diluted and emulsified through water, and acidifying or alkalizing agents are compounded with water to form acidifying or alkalizing agent solutions; (2), the chrome leather scrap hydrolysate is heated to 45 DEG C to 50 DEG C under stirring, then, the chrome leather scrap hydrolysate, the masking agents, and the solid retanning agents or/and liquid-state retanning agents which are at the same temperature and obtained in the step (1) are added into the chrome leather scrap hydrolysate and are evenly mixed, then, the acidifying or alkalizing agent solutions are added to adjust the pH value of mixed liquor to 1.5 to 4.5, undissolved substances are filtered out, and the chromium-contained retaining-filling agent is obtained, wherein the solid content ranges from 40 percent to 45 percent, the content of chromium sesquioxide ranges from 1.5 percent to 5 percent, and the pH value ranges from 1.5 to 4.5. According to the method, chromium and skin collagen protein in chrome leather scrap can be utilized at the same time, the prepared hromium-contained retaining-filling agent is more comprehensive in performance, and problems caused by an existing chemical modification manner can be solved.
Owner:SICHUAN UNIV +1

Production method of polished tiles having jade stone texture

A production method of polished tiles having a jade stone texture, wherein the polished tiles is prepared from following raw materials: high-whiteness albite powder being 5-10 wt% in the content of sodium, feldspar, clay, talcum being 28-32 wt% in the content of MgO, anorthite being 2.0-4.0 wt% in the content of CaO and bone ash being 45-50 wt% in the content of CaO. The production method includes following steps: powder producing, blank body moulding, high-temperature sintering and polishing. During the blank body moulding, firstly more than more than one stacks of a granular powder material is randomly arranged on a material arranging trolley in the form of a large-granular materials, and then a layer of mixed powder material is arranged at the periphery of the granular powder material. The powder materials are press-compacted by a press roller and then are cracked naturally, wherein the cracks are filled with a super-transparent jade material. Finally the prepared materials are fed into a die cavity for being compression-moulded. Compared with a method in the prior art, the production method is free of addition of a reinforcing agent and a whitening agent (such as zirconium silicate) which are harmful to environment. The polished tile has a super-transparent sense just like jade stone, is fine-and-smooth and has a layered sense, is clear in bottom pattern, and has such an excellent jade-like texture.
Owner:广东博华陶瓷有限公司

Cadmium stannate metallographic specimen and preparation method thereof

PendingCN113092199AAvoid ambiguous defectsAvoid slopesPreparing sample for investigationMicroscopic observationPolishing
The invention discloses a cadmium stannate metallographic specimen and a preparation method thereof, and belongs to the field of industrial material preparation. According to the preparation method of the cadmium stannate metallographic specimen, the cadmium stannate specimen is subjected to specific grinding and mechanical polishing treatment, so that the defect that the metallographic phase is blurred during observation due to the fact that an inclined plane appears in the traditional grinding process can be effectively avoided; after the metallographic sample is subjected to subsequent surface chemical corrosion treatment, the microscopic structure can be clearly and completely observed under microscopic observation, and the sample has no obvious scratch, defect or pit defect; the method has the advantages of simple operation steps, low cost and short time consumption, and has practical significance in the aspects of evaluating the grain condition of the cadmium stannate target material and researching the performance. The invention further discloses the cadmium stannate metallographic specimen obtained through the preparation method of the cadmium stannate metallographic specimen, the surface of the product is flat, smooth and flawless, the microstructure is clear under microscopic observation, and effective evaluation on the grain size and uniformity of the product can be achieved.
Owner:XIANDAO THIN FILM MATERIALS GUANGDONG CO LTD

Processing technology of broadleaf holly leaves

The scheme discloses a processing technology of broadleaf holly leaves in the technical field of tea processing. The technology is as follows: carrying out enzyme deactivation on tea leaves after withering, preparing a hot stir-frying pan during the enzyme deactivation, smearing vegetable oil on the wall of the pan, then pouring clear water, boiling the clear water, putting the obtained withered tea leaves into the pan with stirring, heating the tea leaves in boiling water for 30-60s, and filtering out the tea leaves; putting the tea leaves into cold water for cooling immediately after the filtering, and conducting primary rolling at 58-68 DEG C for 15-20min after dehydration; and conducting standing for 15-20min, conducting re-rolling, and then carrying out drying. The scheme of the invention is combined with a special enzyme deactivation mode, the tea leaves are flexible in texture and not easy to tear up after the enzyme deactivation; then the rapid cooling avoids the internal texture of tea leaves from destructive changes due to persistent high temperature; and under the early-stage preparation conditions, with the primary rolling and re-rolling process and the drying mode, theobtained broadleaf holly leaves have distinct particles, are granular, are high in toughness, and are not easy to break by external force.
Owner:余庆县玉笏春茶业有限责任公司

Making equipment of chopped red peppers

The application of the invention discloses making equipment of chopped red peppers, and belongs to the field of red pepper processing. The making equipment comprises a mixing mechanism and a cutting and chopping mechanism, wherein the mixing mechanism comprises a mixing barrel, a discharging opening is formed in the bottom of the mixing barrel, and a push and pull plate is in slip connection to the discharging opening; the cutting and chopping mechanism comprises a material accommodating barrel, chopping knives and supporting rods; a barrel opening of the material accommodating barrel communicates with the discharging opening; the two supporting rods are fixedly connected with the bottom of the mixing barrel; a roller is rotatably connected to the bottom end of each of the two supporting rods; a transmission belt is in sleeving connection between the two rollers; a connecting rod is rotatably connected to each roller; the same horizontal rod is rotatably connected to one ends away fromthe rollers, of the two connecting rods; the lower surface of the horizontal rod is connected with the chopping knives; a base is arranged under the material accommodating barrel; a second motor is arranged in the base; and a fixing rod is connected between the base and the mixing barrel, and is located on the outer wall of the base and the outer wall of the mixing barrel. Through the adoption ofthe scheme of the making equipment of the chopped red peppers disclosed by the invention, the problem that in conventional chopped red pepper mechanical processing, the mouth feel of the made choppedred peppers is poor because red pepper pulp and red pepper skins are separated is solved.
Owner:贵州胤通农业发展有限公司

A kind of production method of polished tile with jade stone texture

A production method of polished tiles having a jade stone texture, wherein the polished tiles is prepared from following raw materials: high-whiteness albite powder being 5-10 wt% in the content of sodium, feldspar, clay, talcum being 28-32 wt% in the content of MgO, anorthite being 2.0-4.0 wt% in the content of CaO and bone ash being 45-50 wt% in the content of CaO. The production method includes following steps: powder producing, blank body moulding, high-temperature sintering and polishing. During the blank body moulding, firstly more than more than one stacks of a granular powder material is randomly arranged on a material arranging trolley in the form of a large-granular materials, and then a layer of mixed powder material is arranged at the periphery of the granular powder material. The powder materials are press-compacted by a press roller and then are cracked naturally, wherein the cracks are filled with a super-transparent jade material. Finally the prepared materials are fed into a die cavity for being compression-moulded. Compared with a method in the prior art, the production method is free of addition of a reinforcing agent and a whitening agent (such as zirconium silicate) which are harmful to environment. The polished tile has a super-transparent sense just like jade stone, is fine-and-smooth and has a layered sense, is clear in bottom pattern, and has such an excellent jade-like texture.
Owner:广东博华陶瓷有限公司
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