51results about How to "Fast extraction time" patented technology

The invention provides a method for extracting cornel iridoid glycoside by virtue of ultrasonic-microwave synergetic extraction. The method comprises the following steps: (1) preparing cornus officinalis coarse powder; (2) adding the cornus officinalis coarse powder into a 80% methanol solution in a material-liquid ratio of (1:5)-(1:25), sealing, weighing and determining the weight, connecting a condensing device, and extracting for 3-15 minutes with microwave power of 300-700W and ultrasonic powder of 120-600W to obtain an extract; (3) carrying out suction filtration on the extract to obtain filtrate, keeping the constant volume, filtering, concentrating, drying and purifying to obtain the cornel iridoid glycoside. A method for determining the cornel iridoid glycoside comprises the following steps: a, preparing a mixed reference substance solution; b, preparing a test substance solution; c, determining the contents of morroniside, loganin, sweroside and cornel iridoid glycoside in the mixed reference substance and the test substance; d, respectively calculating the contents of the four glycosides according to the result of liquid chromatographic analysis.

The invention provides a classifier training method and a computer readable storage medium, and the classifier training method comprises the steps: carrying out the decomposition of a time sequence ofan electroencephalogram signal containing crymodynia information, so as to obtain decomposed sub-band components; determining a ratio of the energy value of any sub-band component to the sum of the energy values of all the sub-band components, a fine composite multi-scale dispersion entropy of any sub-band component, a fine composite multi-scale fuzzy entropy and an autoregression model coefficient; determining a feature set according to the ratio of the energy value of any sub-band component to the sum of the energy values of all the sub-band components, the fine composite multi-scale dispersion entropy, the fine composite multi-scale fuzzy entropy and the autoregression model coefficient; and training the classifier according to the feature set to obtain the target classifier. The classification effect of the classifier obtained through training according to the feature variables on the crymodynia information is better, and the reliability of the diagnosis result of the neurologicaldiseases is improved.

The supersonically reinforced process of extracting yolk phospholipid with yolk powder containing protein and fat as material includes supersonically reinforced extraction of yolk powder in 80-99 % concentration alcohol solution of 3-20 times weight of yolk powder at 20-70 deg.c for 1-3 times 0.1-1 hr each, with the supersonic wave frequency being 20-150 KHz; centrifuging and filtering the extracted liquid; and decompression concentrating the supernatant and vacuum drying to obtain yolk phospholipid. Compared with available processes, the present invention has the advantages of simple operation, short extraction period, low power consumption, low extraction cost, high effective component transferring rate, etc.

The invention discloses a method for brewing fermentation-type mulberry liquor. The method comprises the following steps of selecting raw materials, cleaning, extruding, soaking, pulping, protecting color, carrying out enzymolysis, sterilizing, inoculating, carrying out main fermentation, accelerating aging, filtering, classifying and the like. Due to adoption of the method disclosed by the invention, the brewing time of mulberry liquor is shortened, the labor and the production cost are saved and the production efficiency and enterprises benefits are improved.

The present invention provides a concentrated Liuwei dihuang pill preparation method. According to the method, the existing preparation method is improved so as to effectively improve component transfer rate and paste yield, save energy consumption and reduce active ingredient loss.

The invention discloses an extraction technology of folium artemisiae argyi volatile oil. The technology comprises the steps that 1, folium artemisiae argyi is cleaned thoroughly, impurities are removed, and low-temperature drying and smashing are performed to obtain folium artemisiae argyi powder; 2, warm water is added into the folium artemisiae argyi powder till the folium artemisiae argyi powder is soaked to be expanded, and freezing treatment is performed at the temperature of subzero 6 DEG C to 0 DEG C for 2-3 h; microwave defrosting is performed on the frozen folium artemisiae argyi powder; 3, water with the weight 10-15 times that of the folium artemisiae argyi powder is added into the defrosted folium artemisiae argyi powder for soaking for 5-10 h, then, steam distillation is performed on the folium artemisiae argyi powder and the soaking solution, distillation is performed for 5-8 h, and a distillate is collected; standing, cooling and layering are performed on the distillate, and then an upper oil layer is obtained and is the folium artemisiae argyi volatile oil. According to the extraction technology of the folium artemisiae argyi volatile oil, freezing-microwave defrosting pretreatment and a steam distillation steam method are combined, volatile oil in folium artemisiae argyi is extracted, the cost is low, operation is simple, the extraction time is short, and the volatile oil extraction rate is high.

The invention belongs to the comprehensive utilization field of agricultural product byproducts, and in particular relates to a method for continuously preparing millet bran coat crude oil and alcohol soluble protein. The method comprises the following steps: (1) millet bran coat screening and impurity-removing cleaning; (2) preparing of an extraction solution; (3) counter-current extraction; (4) solid-liquid separated millet bran coat crude oil and alcohol soluble protein mixture; (5) secondary extraction; (6) secondarily separated alcohol-soluble protein crude extract; (7) rotary-evaporation to obtain the millet bran coat crude oil. By use of the method of extracting twice, the grease and the alcohol-soluble protein in the millet bran coat are successively extracted, so the comprehensive utilization efficiency of the millet bran coat is improved; and meanwhile, the counter-current extraction method is use for extracting the bran coat, the extraction time is greatly shortened in comparison with that of the traditional solvent lixiviation method, the operation is simple, and the extraction rate is high.

Provided are a manufacturing method of a rotor of a motor integrated pump capable of more reliably restraining the influence of operating fluid of the pump on the magnet and a motor integrated pump with the rotor is provided. The method includes: a magnet support process, supporting a magnet (11) inserted in a die (30) through a first, second and third pins (40,41,42); and a support component removing process, drawing out the first, second and third pins (40,41,42) from a first cavity (34) of the die (30) through a first, second and third implementation components (46,47,48) in the process of filling resin in the die (30). Therefore, even if in the region wherein, magnet is supported by the first, second and third pins (40,41,42), the shaping resin can be used to overcast.

The invention belongs to the field of natural products extraction, and concretely relates to a method for extracting high-purity crambe abyssinica seed oil and a cream containing the crambe abyssinica seed oil. According to the invention, the crambe abyssinica seed oil can be extracted by using a microwave radiation method, the method comprises the following steps: 1) accurately weighing a certain amount of crambe abyssinica seeds and placing the crambe abyssinica seeds in a container, adding a certain amount of an extraction solvent, extracting the crambe abyssinica seeds under certain microwave power to obtain a mixture; 2) filtering the mixture, performing rotating separation on a filtrate on a rotary evaporator, removing the extraction solvent to obtain a residual substance crambe abyssinica seed crude oil; 3) placing the crude oil in a fixed container, adding sodium hydroxide for boiling the material, washing the material by warm water until the material presents neutrality; and 4) performing adsorption decoloring on the crambe abyssinica seed crude oil obtained in the step 3) and filtering the crambe abyssinica seed crude oil, and obtaining the filtrate which is the crambe abyssinica seed oil. The extraction technology is simple, and purity of the obtained crambe abyssinica seed oil is high. The invention also discloses an application of the crambe abyssinica seed oil in the cream.

The invention relates to a method for extracting effective component of traditional Chinese medicine, with dynamic overflow continuous reverse-flow method, wherein said method uses several extractors, while each extractor works independently and they use active overflow method, to transfer liquid continuously. Compared with traditional method, the invention improves extracting speed, reduce solvent consumption, reduce following energy consumption and improve efficiency. The invention can reduce extracting temperature, etc. And the invention comprise several pots, heater, condenser, tubes, pump and value which control the active overflow between pots, and the meter element controlling the balance of whole device.

The invention relates to an integrated circuit impedance network model extraction method and system. The method comprises the following steps: acquiring a multilayer integrated circuit layout; performing mesh generation on the multilayer integrated circuit layout to obtain a non-structural triangular mesh for segmenting the multilayer integrated circuit layout; listing a finite element equation set for calculating the potential field of the integrated circuit according to the information of the grid nodes on each triangular grid to obtain a finite element sparse matrix; enabling the finite element sparse matrix to be equivalent to a sparse matrix of an admittance network taking a finite element grid as association; repeatedly performing star triangle transformation on the sparse matrix ofthe admittance network to eliminate internal nodes of a non-port of the sparse matrix to obtain an admittance network of the port; and determining an impedance network model according to the admittance network of the port, and further extracting the impedance network model. The method improves the extraction speed of the impedance network model of the multi-layer super-large-scale integrated circuit.

The invention relates to nutrient soil with broad-spectrum insecticidal property and good water retention capacity. The nutrient soil is characterized by being prepared by the following steps: firstly extracting and separating sophocarpidine by virtue of an ultrasonic extraction-microwave extraction combined technique and trichloromethane extraction; and then carrying out microwave heating on attapulgite, vermiculite and zeolite so as to increase effective apertures of the attapulgite, the vermiculite and the zeolite, and introducing the sophocarpidine into the apertures of the attapulgite, the vermiculite and the zeolite; and finally carrying out cross-linking polymerization on acrylamide, as a monomer, and the attapulgite, the vermiculite and the zeolite under the catalysis of potassium persulfate, so as to obtain spatial reticular inorganic mineral-polymer particles, namely the nutrient soil with the broad-spectrum insecticidal property and the good water retention capacity. The nutrient soil disclosed by the invention has the broad-spectrum insecticidal property, is capable of improving a soil structure, improving soil organic matters and adjusting a soil microenvironment and is applicable to plantation of flowers and nursery stocks.

The invention relates to the technical field of traditional Chinese medicinal pharmacy, and especially relates to a compound thrombus relieving soft capsule and a preparation technology thereof. The content of the soft capsule is composed of effective dry extract powder, soybean oil and beeswax; the effective dry extract powder comprises extracts obtained through extracting the following medicinal materials, by weight, 600-800 parts of panax notoginseng, 200-300 parts of Radix Astragali, 100-200 parts of Salvia miltiorrhiza and 200-300 parts of Radix Scrophulariae; a weight ratio of the effective dry extract powder to the soybean oil is 3-5:7-5, and the proportion of the beeswax is 4-6% of the proportion of the soybean oil; and the shell of the capsule is prepared from, by weight, 0.95-1.05 parts of gelatin, 0.3-0.5 parts of glycerin and 0.8-1.2 parts of water. The compound thrombus relieving soft capsule has the advantages of accurate content, good stability, good dissolution, fast absorption, small side effects, portability, small dosage, high bioavailability, rapid curative effect and good effect.

The invention belongs to the technical field of gene amplification detection, and particularly relates to a drug-related genotyping kit and a typing method for a thiopurine drug. Use of nano-silica ingene amplification detection is initiatively found, and gene amplification reaction efficiency and reaction specificity can be remarkably improved, so that the nano-silica is applied to drug-relatedgenotyping detection of the thiopurine drug to solve the problems that drug-related genotyping for the thiopurine drug is poor in specificity and low in detection speed, and a large number of samplescannot be rapidly detected in a high-specificity manner in the prior art.

The invention relates to a tremella fuciformis cookie. By adding tremella fuciformis polysaccharide and tremella fuciformis powder in a raw material formula and matching the tremella fuciformis polysaccharide and the tremella fuciformis powder reasonably, the synergy of the tremella fuciformis polysaccharide and the tremella fuciformis powder has the effects of improving body immunity, resisting tumors, resisting anabrosis, resisting blood coagulation, preventing cerebral thrombosis, lowering lipid, lowering blood glucose, promoting the body protein synthesis, slimming and the like, so that the finally obtained tremella fuciformis cookie is obvious in health care effect, is suitable for mid-aged population with relatively high blood glucose and blood lipid, has good taste and is rich in nutrition.

The invention discloses biomass charcoal particles loaded with matrine-chitosan sustained-release microspheres and a preparation method thereof. The preparation method is characterized in that adopting ultrasonic extraction and microwave extraction combined technology and chloroform extraction to extract and separate matrine; performing glutaraldehyde and chitosan in-situ crosslinking on the surface of matrine to obtain matrine coated chitosan sustained-release microspheres; loading the chitosan sustained-release microspheres on the surfaces of biomass charcoal particles through action between maleic anhydride and the chitosan sustained-release microspheres and hydroxyl on the surfaces of the biomass charcoal particles to obtain the biomass charcoal particles loaded with the matrine-chitosan sustained-release microspheres. The biomass charcoal particles loaded with the matrine-chitosan sustained-release microspheres have broad-spectrum insecticidal property, can improve soil structure, increase soil organic matter and adjust soil microenvironment, and can serve as a high-quality energy source and a soil improver to be applied in the aspects of water source purification and soil improvement.

The invention provides a microwave extraction technology for steroid saponins in caltrops, which comprises the following steps: weighing caltrop sample and placing the caltrop sample into a microwave extraction bottle, adding alcohol in the microwave extraction bottle, placing the microwave extraction bottle in a MAS-II type normal-pressure microwave-assisted synthesis/extraction reaction instrument for extraction, performing decompression filtration to an obtained extract, and then evaporating a solvent on a rotary evaporator to obtain a crude extract of the steroid saponins of the caltrops; adopting a HCl solution to hydrolyze the steroid saponins extracted by microwave, obtaining sapogenins corresponding to the steroid saponins of the caltrops after the hydrolysis, dissolving the saponins with chloroform, and then filtering the saponins for GC-MS detection. The technology adopts a microwave-assisted hot reflux method to extract the steroid saponins of the caltrops, combines a gas chromatography mass spectrometry to detect steroidal sapogenins of the caltrops, ensures that the pretreatment is simple and convenient and the operation is simple by optimizing extraction conditions, has high extraction efficiency, and is environment-friendly and nontoxic.

The invention belongs to the technical field of gene amplification detection, and particularly relates to a kit and a method for drug-related gene typing detection of warfarin. Use of nano-silica in gene amplification detection is initiatively found, and gene amplification reaction efficiency and reaction specificity can be remarkably improved, so that the nano-silica is applied to drug-related genotyping detection of the warfarin to solve the problems that drug-related genotyping for the warfarin is poor in specificity and low in detection speed, and a large number of samples cannot be rapidly detected in a high-specificity manner in the prior art.

The invention belongs to the technical field of gene amplification detection, and particularly relates to application of nano silicon dioxide in gene amplification detection, a nucleic acid amplification reagent utilizing nano silicon dioxide and a detection kit and a detection method of individualized administration related gene subtyping. It is found for the first time that reaction efficiency and reaction specificity of gene amplification can be improved remarkably by using nano silicon dioxide in gene amplification detection, and the problem that gene amplification is low in detection rateand specificity in the prior art and the problem that quick and highly specific detection of samples in a large amount cannot be realized due to low specificity and slow detection speed of gene typing are solved.

The invention belongs to the technical field of collagen extraction, and particularly relates to an extraction method and application of fish skin collagen. The invention provides a method for rapidly extracting non-denatured fish skin collagen, which solves the problem of waste of freshwater fish processing byproducts and overcomes the defects of low extraction rate and long extraction time of the traditional collagen extraction method. The technical method disclosed by the invention is simple and feasible, short in extraction time and high in extraction efficiency, most importantly, the integrity of collagen macromolecular structures is ensured, and the extraction time is greatly shortened compared with other methods. According to the extraction method, the collagen is subjected to ultrasonic treatment before being extracted by a traditional acid-enzyme combination method, so that the natural activity of extracted fish skin collagen molecules is ensured, and the fish skin collagen obtained by measurement keeps the natural structure of type I collagen and is non-denatured type I collagen. The method is simple to operate, lower in energy consumption, high in extraction efficiency and easy to amplify and apply to production.

The invention belongs to the technical field of preparation of feed additives and particularly relates to a preparation method and application of a compound Chinese herbal medicine preparation for sheep. The preparation method comprises the steps as follows: 100-150 g of high-quality radix astragali, 60-120 g of medicated leaven, 60-120 g of malt, 60-120 g of haws, 60-120 g of dried orange peel, 60-120 g of leaves of eucommia ulmoides, 100-150 g of officinal magnolia bark, 100-200 g of houttuynia cordata, 40-80 g of garlic, 40-80 g of ginger and 60-120 g of tarragon are thoroughly cleaned anddried, the obtained materials are crushed into 60-mesh powder, ultrasonic extraction is performed twice in the ratios of medicines to water (by weight) being 1:30 and 1:20 respectively at 60 DEG C atultrasonic power of 1250 W for 60 min, extraction liquids are mixed and concentrated into extract of 4.25-5.55 (25 DEG C), the extract is mixed with calcium lactate in the ratio being 1:5, and drying,crushing, sieving and uniform mixing are performed to prepare the preparation.

The invention relates to an extraction and separation method of lamb abomasum chymosin. According to the method, lamb abomasum tissues are dispersed, cells are destroyed and mixing is enhanced throughtreatment methods of tearing granularity, soaking and the like of the abomasum before extraction, and the extraction rate of the chymosin is remarkably improved in combination with an ultrasonic-assisted extraction method, so that the extraction time is greatly shortened, the preparation cost of the chymosin is reduced, and a technical support is provided for standardized production of lamb stomach extracts of related enterprises. Meanwhile, the solubility of the chymosin in the lamb stomach is systematically researched, an optimal solvent and an optimal extraction pH value are selected, anda reliable and feasible method is provided for enlarged production of chymosin extraction. The lamb abomasum chymosin obtained by the method is high in purity and strong in biological activity; the extraction method is simple and feasible; the whole extraction process is operated in a low-temperature environment, so that the activity of the lamb abomasum chymosin is better retained; and the obtained chymosin can be applied to cheese production.