The invention belongs to the technical field of fine
chemistry, and relates to a method and equipment for refining
raw material liquid paraffin and by-product
hydrochloric acid simultaneously during a
continuous production process for chlorinated paraffin, wherein the equipment is an extraction
tower. The method comprises the following steps of: continuously and manually extracting the by-product
hydrochloric acid and the
raw material liquid paraffin generated during the
continuous production process for chlorinated paraffin, so as to improve the purity of the
liquid paraffin entering in a chlorination reaction phase; and reacting the
raw material liquid paraffin with free
chlorine in the
hydrochloric acid, so as to reduce the concentration of the free
chlorine in the by-product hydrochloric acid. According to the method and the equipment disclosed by the invention, via the mutual extraction and reaction of the by-product hydrochloric acid and the raw material liquid paraffin, the contents of
aromatic hydrocarbon, basic
nitrogen, mechanical impurities and water in the liquid paraffin are reduced, the purity of the raw material liquid paraffin is improved, and then the colour of the chlorinated
paraffin product is improved, and the colour numbers of
platinum and
cobalt are reduced to be less than 100; simultaneously, the raw material liquid paraffin can be reacted with the free
chlorine in the by-product hydrochloric acid, so that the quality of the by-product hydrochloric acid is improved, and the content of the free chlorine in the by-product hydrochloric acid is reduced to 0.006 from about 0.015 originally after extraction.