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38results about How to "Mix reaction evenly" patented technology

Method for continuously preparing ultrafine sliver powder on basis of microchannel mixed reaction system

ActiveCN104209529ASolve technical problems in mass productionIncrease productivityFiltrationSodium ascorbate
The invention belongs to the field of preparation of metal ultrafine powder materials and particularly relates to a method for continuously preparing ultrafine sliver powder on the basis of a microchannel mixed reaction system. According to the method, an oxidation solution containing soluble silver salt and nitric acid and a reduction solution containing ascorbic acid or sodium ascorbate are continuously conveyed to the microchannel mixed reaction system respectively through driving devices, mixing is carried out in a Y-type tee joint or a tee joint in the microchannel mixed reaction system, wherein the Y-type tee joint or the tee joint serves as a mixing unit of reactive materials, the mixed solutions flow out of reaction microchannels after being subjected to a reaction in the reaction microchannels in the microchannel mixed reaction system, standing is carried out on obtained reaction products, washing and sediment are carried out on the products, and ultrafine sliver powder of different morphologies and sizes can be obtained after suction filtration and drying. According to the method, control over the crystallization morphologies and the sizes of ultrafine sliver powder particle products can be achieved by adjusting the components of the oxidation solution, the components of the reduction solution, the molar concentration, the temperature and other parameters.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Multi-mode stirring type co-precipitation precipitation device for rare earth

The invention relates to a co-precipitation precipitation device for rare earth, in particular to a multi-mode stirring type co-precipitation precipitation device for the rare earth. To solve the technical problem of providing the multi-mode stirring type co-precipitation precipitation device, capable of being adjusted and stirring rare earth mixture liquid in various ways, for the rare earth, thetechnical scheme of the multi-mode stirring type co-precipitation precipitation device for the rare earth is that the multi-mode stirring type co-precipitation precipitation device for the rare earthcomprises various parts such as a base, a first bearing, a support shaft, a cylinder, a drain pipe, a first valve, a filter screen, a discharge pipe, a second valve, a second bearing and long connecting shaft; the first bearing is embedded in the base; the lower end of the support shaft and the first bearing are in interference connection. The multi-mode stirring type co-precipitation precipitation device for the rare earth has the advantages of being easy to adjust and capable of stirring the rare earth mixture liquid in various ways, realizing uniform mixing reaction of the rare earth mixture liquid, having simple structure, easy operation and low labor intensity, and being time-saving and labor-saving.
Owner:东港智科产业园有限公司

Process method for treating refractory CODs (chemical oxygen demands) in produced water of high-sulfur-content gas field

The invention belongs to the technical field of ground engineering of oil and gas fields and in particular relates to a process for removing refractory CODs (chemical oxygen demands) in produced waterof a high-sulfur-content gas field. Aiming at situations that refractory COD components in produced water of a high-sulfur-content gas field and CODs in fed water after pretreatment are generally 1000mg/L and are refractory CODs, and to achieve resource recycling of the produced water of the high-sulfur-content gas field, the invention discloses the process applicable to removal of refractory CODs in produced water of the high-sulfur-content gas field, a treatment process of "Fenton oxidation+ozone ultraviolet photocatalytic oxidation+micro/ultrafiltration membrane+reverse osmosis membrane" is adopted, and organic components such as refractory CODs and volatile phenols in the produced water of the high-sulfur-content gas field can be degraded and removed. In a situation that the CODs of produced water are less than or equal to 1000mg/L, the process is adopted for treatment, and CODs of an effluent after treatment qualification are less than or equal to 50mg/L.
Owner:中石化石油工程技术服务有限公司 +1

Integrated fluidized catalytic oxidation tower and method for deeply treating wastewater by using same

The invention discloses an integrated fluidized catalytic oxidation tower and a method for deeply treating wastewater by using the same. A balance adjusting unit of the catalytic oxidation tower is connected with a water distribution pipe at the bottom of a catalytic oxidation unit through a pipeline; the outer side of the upper part of the catalytic oxidation unit is provided with a circulating water tank, the outer side of the circulating water tank is provided with an intermediate water tank, and the top of the circulating water tank is connected with the intermediate water tank through an overflow port; the intermediate water tank is connected with a water distribution pipe of a coagulation sedimentation unit through a pipeline, and a water collecting basin is connected with the balance adjusting unit through a pipeline; the balance adjusting unit is connected with the water collecting basin through a first overflow pipe, and the intermediate water tank is connected with the water collecting basin through a second overflow pipe; a water outlet of a water outlet tank is connected with a clean water basin through a water outlet pipe. By using the integrated fluidized catalytic oxidation tower, the mass transfer efficiency and the chemical reaction speed are effectively increased, the oxidative degradation effect for organic pollutants in wastewater is improved, the dosage of a Fenton reagent can be reduced, and the yield of chemical sludge in the later coagulation process can be reduced.
Owner:SOUTH CHINA UNIV OF TECH

Whole-plant water network monitoring device for thermal power plant

PendingCN114436353ARaise awareness of conservationImprove controlTreatment control/steeringProcess engineeringPower station
The invention discloses a thermal power plant whole plant water network monitoring device which comprises a mounting base, a pipeline monitoring mechanism is arranged at the top of the mounting base, and the pipeline monitoring mechanism comprises a mounting groove, a communicating pipe, a flow monitoring meter, a sewage guide pipe, a water guide pipe, a water storage cavity, a water invasion sensor, a water pump, a liquid guide pipe, an alarm and a monitoring camera. According to the invention, a whole-plant water consumption whole-process intelligent on-line supervision platform is established, a set of complete technical supervision system is established, a typical unit is taken as an example for trial, and through water balance test and application, power plant production management related personnel can master energy consumption, pollution discharge and energy quality conditions of each device in real time, supervise energy conditions and find problems in time, so that the power plant water consumption whole-process intelligent on-line supervision system is provided for the whole-plant water consumption whole-process intelligent on-line supervision. Real-time monitoring and management are achieved, saving consciousness of enterprise managers and employees is effectively improved, the energy quality control capability is improved, and real-time monitoring is carried out on water balance of the whole plant.
Owner:国家能源集团山西电力有限公司 +2

Control system for producing epoxy resin based on reaction kettle and automatic production method

The invention discloses a control system for producing epoxy resin based on a reaction kettle and an automatic production method. The control system comprises a PLC controller, an input component, aninput module, an output module, an execution component, a PC upper computer, a central processing unit, a communication interface, a power supply, and a memory. The input component comprises a temperature sensor, a liquid level meter, a pressure gauge, a mass flow meter, and a flow meter. The output component comprises loading pumps, a hot and cold water regulating valve, an electromagnetic regulating valve, a variable frequency pump, and a three-way regulating valve. The control system for producing epoxy resin based on the reaction kettle and the automatic production method enable the preheating, metering, conveying, mixing reaction and packaging of materials to be monitored and to be automatically adjusted by a PLC system, thereby realizing a complete sealing, automatic and continuous production process. The production process has a high production process efficiency, a stable product quality, a low labor cost, and environmental protection at the production site. The control systemfor producing epoxy resin based on the reaction kettle and the automatic production method have significant economic and social benefits, and ensure that the materials are uniformly mixed and reactedstrictly according to the mass ratio.
Owner:魏贵英

Method and device used for preparing dichloropropanol through micro channel chlorination reaction

The invention belongs to the field of dichloropropanol, and more specifically relates to a method and a device used for preparing dichloropropanol through micro channel chlorination reaction. The method comprises following steps: glycerin, and adipic acid are uniformly mixed so as to obtain a mixed solution, the mixed solution is mixed with hydrogen chloride in a pipeline before entering into a pre-reaction tank, and an obtained mixed material is introduced into the pre-reaction tank for pre-reaction, wherein the internal wall of the pre-reaction tank is attached with a solid acid catalyst; anobtained product is introduced into a micro channel reactor for chlorination reaction, wherein the internal wall of the micro channel reactor is provided with the solid acid catalyst; an obtained reaction product is introduced into a normal pressure tower for normal pressure distillation, the fractions collected from the top of the normal pressure tower are low-boiling-point substances, and are subjected to layering and water washing so as to obtain dichloropropanol; and the fractions collected from the bottom of the normal pressure tower are introduced into a pressure reduction tower for distillation so as to obtain dichloropropanol. According to the method, solid super strong acid SO4<2->/ZrO2-Pr2O3 is attached onto the internal wall of the pre-reaction tank and the micro channel internal wall of the micro channel reactor, so that reaction efficiency is increased, the subsequent processing difficulty is reduced, and operation cost is reduced.
Owner:山东民基新材料科技有限公司

Lift pipe reactor pre-lifting device and process flow thereof

The invention relates to a lift pipe reactor pre-lifting device and a process flow thereof. The lift pie reactor pre-lifting device comprises a fluidized vapor ring, a pre-lifting vapor nozzle, a pre-lifting vapor pipe, an expansion section, a single-action slide valve and a regeneration inclined pipe. An inner conveyor pipe is arranged in the expansion section, the lower part of the inner conveyor pipe is connected with the upper part of the pre-lifting vapor pipe, and the inner diameter of the pre-lifting device is twice as large as the inner diameter of the upper part of a lift pipe reactor. By adopting the method in which the inner conveyor pipe is increased, the inner diameter of the pre-lifting device is increased and therefore the structure of the expansion section is changed, the catalyst entering the expansion section has a sufficient buffering space, so that the blanking pressure fluctuation of the regeneration inclined pipe is reduced, the bias current generated by an S-shaped movement orbit can be eliminated, the pre-lifting vapor pipe can avoid the regeneration inclined pipe, the direct impact of the pre-lifting vapor on a blanking port of the regeneration inclined pipe can be avoided, the circulating capacity of the catalyst of a settlement regenerator can be increased, the catalyst in the lift pipe can be uniformly distributed, and the yield of a target product can be improved.
Owner:LUOYANG ZHIBANG PETROCHEM EQUIP

Sludge treatment sedimentation tank capable of reducing sludge flocculation

The invention discloses a sludge treatment sedimentation tank capable of reducing sludge flocculation, and relates to the technical field of sewage treatment devices. The sludge treatment sedimentation tank capable of reducing sludge flocculation comprises a sedimentation tank body, wherein cross arm positioning shafts are symmetrically welded to an opening in the top end of the sedimentation tank body; a motor is arranged at the top end of the right outer wall of the sedimentation tank; the middle positions of the top ends of the inner walls of the front side and the rear side of the sedimentation tank are symmetrically and rotationally sleeved with flocculant spraying pieces; a cross arm positioning shaft is sleeved with the driving mechanism in the sliding manner; the driving mechanism comprises a first rack. Through mutual cooperation of first hollow spraying piece, second hollow spraying piece, scraping plate and like, when second hollow spraying piece continues to slide into first hollow spraying piece and is aligned with medicine spraying hole in first hollow spraying piece, high-pressure liquid in second hollow spraying piece flows out of aligned liquid spraying hole and impacts liquid spraying hole, and then medicine spraying hole is cleaned. Therefore, the phenomenon that the medicine spraying holes are blocked by dirt deposition is avoided.
Owner:张锐

Novel ship waste gas washing and desulfurizing device

The invention discloses a novel ship waste gas washing and desulfurizing deviceinvention, and relates to the technical field of marine diesel engine tail gas treatment. The device comprises a desulfurization tower, a cooling spraying layer, a main spraying layer and a rotational flow plate demister are sequentially arranged in the desulfurization tower from bottom to top, the device further comprises a grid structure, a plurality of floating balls and two annular flow guide plates, which are arranged in the desulfurization tower, the grid structure is arranged between the cooling spraying layer and the main spraying layer, a plurality of isolated small accommodating cavities are formed between the grid structure and the desulfurization tower, the floating balls are respectively arranged inthe small accommodating cavities, and the two annular flow guide plates are fixed on the inner wall of the desulfurization tower. The ship waste gas washing and desulfurizing device has the advantages of low blocking possibility and easy washing of the floating balls in the accommodating cavities, high working condition adaptability, low investment, low operation and maintenance cost and the like, the wet desulphurization efficiency can be remarkably improved, and the side wall effect of airflow is avoided by arranging the annular flow guide plates to make sulfur oxide and washing liquid fully mixed and reacted.
Owner:SHANGHAI MARITIME UNIVERSITY

External circulation ammonification reactor

The invention discloses an external circulation ammoniation reactor. The external circulation ammoniation reactor comprises a settling separator, a stirring device, a lifting pipe, a return pipe, a circulating pump, a gas distributor and a plurality of mesh grids, wherein the gas distributor comprises a gas inlet pipe and a gas ammonia nozzle, the gas ammonia nozzle is detachably installed at the gas outlet end of the gas inlet pipe, the gas ammonia nozzle horizontally sprays gas, and the multiple mesh grids are arranged in the lifting pipe at intervals and located above the gas distributor. The gas ammonia nozzle is detachably installed on the gas inlet pipe, the gas ammonia nozzles with different hole diameters can be replaced conveniently, the requirements for different gas phase treatment capacities can be met, the nozzles conduct horizontal spraying, the problem that slurry blocks gas spraying holes can be avoided, flocculent solid particles can be detached through the mesh, and the viscosity is reduced. And on the other hand, the mesh breaks large-size bubbles in the central area of the lifting pipe, so that the bubble breaking probability and the bubble surface updating rate are increased, the specific surface area of the bubbles is increased, and the gas-liquid two-phase mass transfer reaction rate can be effectively increased through the mesh structure.
Owner:HUBEI UNIV OF EDUCATION

High-efficiency production device for preparing hydrochloric acid by drying hydrogen chloride through water absorption

The invention discloses a high-efficiency production device for preparing hydrochloric acid by drying hydrogen chloride through water absorption. The high-efficiency production device comprises a wave-shaped reaction tube, wherein the wave-shaped reaction tube comprises two inlet pipes, a reaction pipeline and an outlet pipe which are of an integrated structure, the two inlet pipes are respectively connected with a hydrogen chloride gas storage tank and a distilled water storage tank by virtue of a gas inlet pipe and a liquid inlet pipe, the outlet pipe is communicated with the top of a cyclone separation tank, the top of the cyclone separation tank is also connected with the gas inlet pipe by virtue of a hydrogen chloride gas recycling pipe, and a liquid outlet pipe at the bottom of the cyclone separation tank is connected to a finished product hydrochloric acid storage tank; a reaction pipeline of a wave-shaped tube reactor is a wave-shaped tube body, a cooling pipe is sheathed outside the reaction pipeline of the wave-shaped tube reactor, a cooling water inlet is formed in the bottom of the cooling pipe, and a hot water outlet is formed in the top of the cooling pipe. The high-efficiency production device has the advantages that distilled water and hydrogen chloride are forcedly transplaced for multiple times in a reducing wave-shaped tube, so that the contact area is expanded, mixing and reaction are uniform, the production efficiency is high, and the product quality is high; meanwhile, the device structure is simple, and the manufacturing cost and the operating cost are respectively low.
Owner:NANYANG NORMAL UNIV

Integrated fluidized catalytic oxidation tower and method for deeply treating wastewater by using same

The invention discloses an integrated fluidized catalytic oxidation tower and a method for deeply treating wastewater by using the same. A balance adjusting unit of the catalytic oxidation tower is connected with a water distribution pipe at the bottom of a catalytic oxidation unit through a pipeline; the outer side of the upper part of the catalytic oxidation unit is provided with a circulating water tank, the outer side of the circulating water tank is provided with an intermediate water tank, and the top of the circulating water tank is connected with the intermediate water tank through an overflow port; the intermediate water tank is connected with a water distribution pipe of a coagulation sedimentation unit through a pipeline, and a water collecting basin is connected with the balance adjusting unit through a pipeline; the balance adjusting unit is connected with the water collecting basin through a first overflow pipe, and the intermediate water tank is connected with the water collecting basin through a second overflow pipe; a water outlet of a water outlet tank is connected with a clean water basin through a water outlet pipe. By using the integrated fluidized catalytic oxidation tower, the mass transfer efficiency and the chemical reaction speed are effectively increased, the oxidative degradation effect for organic pollutants in wastewater is improved, the dosage of a Fenton reagent can be reduced, and the yield of chemical sludge in the later coagulation process can be reduced.
Owner:SOUTH CHINA UNIV OF TECH

A multi-mode stirring co-precipitation device for rare earth

The invention relates to a co-precipitation precipitation device for rare earth, in particular to a multi-mode stirring type co-precipitation precipitation device for the rare earth. To solve the technical problem of providing the multi-mode stirring type co-precipitation precipitation device, capable of being adjusted and stirring rare earth mixture liquid in various ways, for the rare earth, thetechnical scheme of the multi-mode stirring type co-precipitation precipitation device for the rare earth is that the multi-mode stirring type co-precipitation precipitation device for the rare earthcomprises various parts such as a base, a first bearing, a support shaft, a cylinder, a drain pipe, a first valve, a filter screen, a discharge pipe, a second valve, a second bearing and long connecting shaft; the first bearing is embedded in the base; the lower end of the support shaft and the first bearing are in interference connection. The multi-mode stirring type co-precipitation precipitation device for the rare earth has the advantages of being easy to adjust and capable of stirring the rare earth mixture liquid in various ways, realizing uniform mixing reaction of the rare earth mixture liquid, having simple structure, easy operation and low labor intensity, and being time-saving and labor-saving.
Owner:东港智科产业园有限公司
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