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34results about How to "Reduce magnesium oxide content" patented technology

Method for extracting phosphate concentrate from phosphate tailings and cooperatively producing calcium carbonate and magnesium oxide

The invention discloses a method for extracting phosphate concentrate from phosphate tailings and cooperatively producing calcium carbonate and magnesium oxide. First, phosphate tailings are calcined under high temperature, hot water is added into the calcined material for digestion treatment, an ammonium nitrate solution is added to the calcined material, the mixture is stirred, calcium is extracted under a certain temperature, calcium-containing leaching liquid and leaching residues are obtained, phosphate concentrate and magnesium-containing leaching liquid are obtained after magnesium is extracted from the leaching residues with an ammonium sulfate solution, calcium carbonate is obtained after the calcium-containing leaching liquid is precipitated by an ammonium carbonate solution, magnesium carbonate is obtained after the magnesium-containing leaching liquid is precipitated by an ammonium carbonate solution, and magnesium oxide is obtained after the magnesium carbonate is calcined. According to the method, phosphate concentrate, calcium carbonate and magnesium oxide are prepared with phosphate tailings as the main raw materials, large-scale treatment can be carried out on the phosphate tailings, the problem that because phosphate tailings pile up in quantity, the phosphate tailings occupy a lot of land and pollute the environment is solved, and the products of phosphate concentrate, calcium carbonate and magnesium oxide are obtained.
Owner:GUIZHOU RES INST OF CHEM IND

Beneficiation method for separating copper-nickel sulfide ore from serpentine gangue

ActiveCN105413877AIncrease buoyancyWeaken heterogeneous condensationFlotationPyrophosphateSulfide minerals
The invention relates to a beneficiation method for separating copper-nickel sulfide ore from serpentine gangue. The beneficiation method comprises the following steps: when the copper-nickel sulfide ore is roughly concentrated, a polymer reagent poloxamer which can be adsorbed onto the surface of sulfide mineral through hydrophobic interaction but cannot be adsorbed onto the surface of the serpentine gangue is added; ore pulp is dispersed through the steric hindrance of the polymer reagent, the heterocoagulation of serpentine and sulfide minerals is eliminated, the inhibiting effect of serpentine on the sulfide minerals is reduced, and the recovery rate of rough concentration of the copper-nickel sulfide ore containing serpentine is increased; for rough copper-nickel sulfide concentrate obtained through rough concentration, regulators sodium pyrophosphate and carboxymethyl cellulose are added to further disperse and inhibit gangue minerals; meanwhile a collector is added before the regulators are added, so that the collector is adsorbed onto the surfaces of sulfide minerals to protect the sulfide minerals; the selective inhibition to the gangue minerals is realized, and therefore the concentrate grade is increased. The beneficiation method solves the problems that the reagent dosage is large, valuable minerals are inhibited and tailings hardly sedimentate in the traditional method.
Owner:JIANGXI UNIV OF SCI & TECH

Preparation method of metal magnesium by magnesium-containing mineral and equipment adopted by preparation method

The invention belongs to the field of metal material, and relates to a preparation method of metal magnesium by magnesium-containing mineral and equipment adopted by the preparation method. The method comprises the following steps of: converting useful components in magnesium-containing mineral into high-activity magnesium oxide, and under the effects of high temperature and a catalytic midbody, enabling the high-activity magnesium oxide to have chlorination reaction with chlorine and carbon monoxide, so that molten magnesium chloride anhydrous is generated; and mixing the molten magnesium chloride anhydrous with the other molten inorganic salt according to a certain proportion to be taken as electrolyte, and leading the electrolyte into a multi-polarity electrolytic cell to electrolyze, so that the metal magnesium is prepared. The technology adopts the fluidzed chlorination bed and the multi-polarity electrolytic cell of the novel equipment, and adds the midbody of catalytic reaction in the process of chlorination, so that the preparation method is more high-efficiency and energy-saving compared with the conventional method. The waste gas and the waste residue generated in the whole process are treated to be reused, so that the preparation method and the equipment are environment-friendly.
Owner:UNIV OF SCI & TECH BEIJING

Method for extracting phosphate concentrate from phosphate tailings and cooperatively producing calcium ammonium nitrate and magnesium ammonium sulphate

The invention discloses a method for extracting phosphate concentrate from phosphate tailings and cooperatively producing calcium ammonium nitrate and magnesium ammonium sulphate. Phosphate tailings are calcined under high temperature, hot water is added into the calcined material for digestion treatment, an ammonium nitrate solution is added to the calcined material, the mixture is stirred, calcium is extracted under a certain temperature, calcium-containing leaching liquid and leaching residues are obtained, phosphate concentrate and magnesium-containing leaching liquid are obtained after magnesium is extracted from the leaching residues with an ammonium sulfate solution, and calcium ammonium nitrate and magnesium ammonium sulphate are obtained after the calcium-containing leaching liquid and the magnesium-containing leaching liquid are concentrated and dried. According to the method, phosphate concentrate, calcium ammonium nitrate and magnesium ammonium sulphate are prepared with phosphate tailings as the main raw materials, large-scale treatment can be carried out on the phosphate tailings, the problem that because phosphate tailings pile up in quantity, the phosphate tailings occupy a lot of land and pollute the environment is solved, and the obtained phosphate concentrate, calcium ammonium nitrate and magnesium ammonium sulphate can bring certain economic interests.
Owner:GUIZHOU RES INST OF CHEM IND

Method for combining electrolytic manganese metal waste residues and gypsum to produce cement clinker and ammonium hydroxide

The invention relates to a treatment method of electrolytic manganese metal waste residues. The treatment method comprises the following steps: A, grinding gypsum or drying calcined gypsum and then grinding to obtain gypsum powder; B, slurrying the electrolytic manganese metal waste residues, leaching, and adding the gypsum powder; adjusting the pH of a solution to 6.0-6.4, removing iron, carryingout filter pressing to obtain a filter pressing block A and a filter pressing solution A, washing the filter pressing block A with water, and then carrying out filter pressing to obtain a filter pressing block B and a filter pressing solution B; adjusting the pH of the filter pressing solution A to 11.5-12, and carrying out filter pressing to obtain a filter pressing block C and a filter pressingsolution C; C, adding silicon dioxide, calcium oxide, aluminum oxide and iron oxide into the filter pressing block B, drying, pre-decomposing, and calcining to obtain cement clinker; D, slurrying thefilter pressing block C, leaching, adjusting the pH to 6.0-6.4, removing impurities, standing, and carrying out filter pressing to obtain a filter pressing block D and a filter pressing solution D, adding ammonia water into the filter pressing solution D to adjust the pH to 8.8-9, and continuously adding an ammonia water solution to adjust the pH to 11.4-11.8. The method realizes recycling of resources.
Owner:庞炼红

Method for co-producing manganese hydroxide and sulfuric acid or ammonium sulfite by electrolytic manganese waste slag

The invention relates to a method for co-producing manganese hydroxide and sulfuric acid or ammonium sulfite with electrolytic manganese waste slag, comprising the following steps: A. slurrying electrolytic manganese metal waste slag, leaching, adjusting pH to 6.0-6.4, removing iron, and pressing filtration to obtain Press filter block A and press filter liquid A, press filter press block A after water washing, obtain press filter block B and press filter liquid B; Regulate the pH of press filter liquid A to 11.5-12, press filter, obtain press filter block C and press filter liquid C, press filtrate C circulation treatment, after potassium and sodium enrichment, remove calcium sulfate, evaporate and crystallize, separate potassium sulfate and sodium sulfate; B. calculate according to production needs and add the required substances to the press block B, dry Drying, pre-decomposition, and calcination to obtain cement additives or solids. The sulfur dioxide produced by calcination is separated from the dedusting ash for powder gas separation. The sulfur dioxide gas is used to make sulfuric acid. The dedusting ash and filter press block B are calcined together to enrich selenium and zinc; C. Slurry the filter block C, leaching, adjust the pH to 6.0-6.4, remove impurities, stand still, and press filter to obtain the filter block D and the filter liquid D, adjust the pH of the filter liquid D to 8.8-9, and continue to adjust the solution pH to 11.4‑11.8. This method realizes the joint output of multiple products.
Owner:庞炼红

A kind of beneficiation method for separating copper-nickel sulfide ore and serpentine gangue

ActiveCN105413877BIncrease buoyancyWeaken heterogeneous condensationFlotationPyrophosphateSulfide minerals
The invention relates to a beneficiation method for separating copper-nickel sulfide ore from serpentine gangue. The beneficiation method comprises the following steps: when the copper-nickel sulfide ore is roughly concentrated, a polymer reagent poloxamer which can be adsorbed onto the surface of sulfide mineral through hydrophobic interaction but cannot be adsorbed onto the surface of the serpentine gangue is added; ore pulp is dispersed through the steric hindrance of the polymer reagent, the heterocoagulation of serpentine and sulfide minerals is eliminated, the inhibiting effect of serpentine on the sulfide minerals is reduced, and the recovery rate of rough concentration of the copper-nickel sulfide ore containing serpentine is increased; for rough copper-nickel sulfide concentrate obtained through rough concentration, regulators sodium pyrophosphate and carboxymethyl cellulose are added to further disperse and inhibit gangue minerals; meanwhile a collector is added before the regulators are added, so that the collector is adsorbed onto the surfaces of sulfide minerals to protect the sulfide minerals; the selective inhibition to the gangue minerals is realized, and therefore the concentrate grade is increased. The beneficiation method solves the problems that the reagent dosage is large, valuable minerals are inhibited and tailings hardly sedimentate in the traditional method.
Owner:JIANGXI UNIV OF SCI & TECH

A kind of method for reducing magnesium oxide in nickel-iron slag and method for preparing slag wool

The invention discloses a method for reducing magnesium oxide in ferronickel slag and a method for preparing slag wool. In the process of making mineral wool from molten ferronickel slag, impregnated carbon is added during the slag discharge process of ferronickel smelting furnace, and the ferronickel slag is treated with impregnated carbon. During the transfer process, the molten nickel iron slag and the impregnated carbon are fully mixed and kept in a holding furnace to reduce the magnesium oxide content in the nickel iron slag; wherein, the preparation process of the impregnated carbon includes: fully mixing the calcium chloride aqueous solution with the carbonaceous material , and then perform solid-liquid separation and drying to obtain impregnated carbon; the amount of impregnated carbon used is determined according to the magnesium oxide content in the nickel-iron slag. The invention can reduce the magnesium oxide content in the ferronickel smelting slag, especially can reduce the magnesium oxide in the free state in the ferronickel smelting slag, is beneficial to improve the quality of slag wool, and is a great reduction in the ferronickel slag containing high magnesium oxide. And high-value utilization has created conditions, and can also realize the recovery of magnesium in nickel-iron slag.
Owner:XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY

Preparation method of metal magnesium by magnesium-containing mineral and equipment adopted by preparation method

The invention belongs to the field of metal material, and relates to a preparation method of metal magnesium by magnesium-containing mineral and equipment adopted by the preparation method. The method comprises the following steps of: converting useful components in magnesium-containing mineral into high-activity magnesium oxide, and under the effects of high temperature and a catalytic midbody, enabling the high-activity magnesium oxide to have chlorination reaction with chlorine and carbon monoxide, so that molten magnesium chloride anhydrous is generated; and mixing the molten magnesium chloride anhydrous with the other molten inorganic salt according to a certain proportion to be taken as electrolyte, and leading the electrolyte into a multi-polarity electrolytic cell to electrolyze, so that the metal magnesium is prepared. The technology adopts the fluidzed chlorination bed and the multi-polarity electrolytic cell of the novel equipment, and adds the midbody of catalytic reaction in the process of chlorination, so that the preparation method is more high-efficiency and energy-saving compared with the conventional method. The waste gas and the waste residue generated in the whole process are treated to be reused, so that the preparation method and the equipment are environment-friendly.
Owner:UNIV OF SCI & TECH BEIJING

A kind of graphene-reinforced magnesium-based composite material and preparation method thereof

The invention relates to a graphene-reinforced magnesium-based composite material and a preparation method thereof. The method is as follows: heating and melting the magnesium matrix in a crucible to obtain a magnesium matrix melt; introducing air or a mixed gas formed by mixing oxygen and rare gas at the top of the crucible; the magnesium matrix is ​​magnesium-zinc alloy, magnesium-calcium alloy, magnesium One or more of copper alloys and magnesium-zinc-calcium alloys; CO is continuously introduced into the magnesium matrix melt for gas-liquid in-situ reaction to obtain a graphene-enhanced alloy melt; when CO reacts with the magnesium matrix melt At the same time, ensure that the temperature of the top of the crucible is above 300° C., and ignite the escaped CO on the top of the crucible; solidify the graphene-reinforced alloy melt to obtain a graphene-reinforced magnesium-based composite material. The invention has the advantages of low cost and feasibility, simple operation and high operation safety factor. The invention obtains a graphene-reinforced magnesium-based composite material with low content of magnesium oxide, high dispersion of graphene with high volume fraction, high interface bonding strength and excellent mechanical properties.
Owner:HARBIN INST OF TECH

Method for reducing magnesium oxide in ferronickel slag and method for preparing mineral wool

The invention discloses a method for reducing magnesium oxide in ferronickel slag and a method for preparing mineral wool. In the process of preparing mineral wool by using molten ferronickel slag, impregnated carbon is added in the slagging process of a ferronickel smelting furnace, the molten ferronickel slag and the impregnated carbon are fully mixed in the transfer process of the ferronickel slag, and heat preservation is carried out in a heat preservation furnace, so that the content of magnesium oxide in the ferronickel slag is reduced; wherein the impregnated carbon preparation processcomprises the following steps: fully mixing a calcium chloride aqueous solution with a carbonaceous material, and then carrying out solid-liquid separation and drying to obtain impregnated carbon; andthe usage amount of the impregnated carbon is determined according to the content of magnesium oxide in the ferronickel slag. According to the method, the content of magnesium oxide in the ferronickel smelting slag can be reduced, particularly, magnesium oxide in a free state in the ferronickel smelting slag can be reduced, the quality of slag wool can be improved, conditions are created for large reduction and high-value utilization of the ferronickel slag containing high magnesium oxide, and recovery of magnesium in the ferronickel slag can also be achieved.
Owner:XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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