82 results about "Amorphous silicon dioxide" patented technology

A fire-resistant, cellulose-based composition of matter is provided that can be used in a variety of applications that benefit from added fire resistance. In at least one aspect, the composition of matter includes, by mass: 10 to 70% cellulose; 1 to 15% insulating compound; and 5 to 30% insulative particles. The composition of matter may further include one or more of, by mass: 1 to 15% phosphate additive, 5 to 30% phosphate filler, 3 to 30% water-based binder, or 1 to 20% silica. The insulating compound of the composition of matter may include, by mass: 2 to 60% insulative particles, 5 to 40% silica, and 15 to 50% amorphous silica. Other aspects are described herein.

The invention relates to a novel phosphorus-fluorine curing agent for phosphogypsum and a preparation method thereof, and belongs to the technical field of industrial solid waste treatment and resource utilization. The curing agent comprises superfine slag powder, anhydrous sodium sulfate, water glass, water, sodium hydroxide and a Fe3O4 (at) SiO2 (at) Zr-Al bimetallic oxide stabilizer. The Fe3O4 (at) SiO2 (at) Zr-Al bimetallic oxide stabilizer is of a core-shell structure, magnetic ferroferric oxide particles serve as a core, and the surfaces of the magnetic ferroferric oxide particles are sequentially coated with an amorphous silicon dioxide protection layer and an active layer. And the active layer is an amorphous and porous zirconium-aluminum bimetallic oxide with a network structure. The preparation method of the curing agent is simple, mild in condition and easy for industrial production, the main raw material is the industrial solid waste slag, the effect of treating waste with waste is achieved, the agent addition amount is small, and the comprehensive treatment cost is low.

The application discloses an amorphous silicon dioxide coating prepared based on micro-arc oxidation, a preparation method and application thereof, and belongs to the technical field of metal surface protection and silicon dioxide coating. In the application, a magnesium alloy, an aluminum alloy, a titanium alloy, a titanium-aluminum base and a nickel-aluminum base are used as anodes and are placed in a micro-arc oxidation tank, a hydrolytic solution of organic silicon is used as an electrolyte, and an amorphous silicon dioxide coating with a thickness of more than 100 mu m can be prepared within 20 minutes through a step-by-step step-incremental constant potential control means. The application utilizes the advantages of the micro-arc oxidation process and the sol-gel process, avoids their shortcomings, and realizes the superimposed synergistic effect of "1+1>2". The process steps of the application are simple, and the application is very suitable for full-automatic operation and processing in industry. The amorphous silicon dioxide coating with the required thickness, wear resistance, corrosion resistance, erosion resistance, oxidation resistance and other characteristics can be prepared by changing the electrolyte concentration, the micro-arc oxidation time and the electric control parameters, or through the conventional micro-arc oxidation constant voltage and constant current control means.

The invention relates to the technical field of preparation of novel bio-based materials, in particular to a preparation method for producing a rice hull-based high-purity high-modulus sodium silicate solution by taking rice hulls as raw materials. Rural solid waste rice hulls / grass are used as raw materials, combustion is carried out at the fixed low temperature of 700-750 DEG C, generated steam is used for supplying heat to the production or the park, and the combusted rice hull ash contains amorphous silicon dioxide gt; 90%; the method comprises the following steps: activating rice hull ash just out of a chamber and diluted hydrochloric acid (5-10%) to generate polyhydroxy surface modified silicon dioxide active seeds; the method comprises the following steps: dynamically mixing rice hull ash and a 25% NaOH solution according to a molar ratio of (3.25-4): 2, adding 3-7% of active seeds in batches at 105 + / -5 DEG C, and reacting for more than or equal to 3 hours; the high-purity sodium silicate solution with the modulus of 3.25-4.0 is finally obtained through pH segmented regulation (Mg < 2 + > is removed at the pH of gt and 12, and Ca < 2 + > is removed at the pH of 9.5-10) in combination with high-pressure refined filtration; the product is mainly used for preparing nano silicon dioxide, especially for preparing 5nm silicon dioxide dispersion liquid and high-purity electronic grade silicon dioxide as raw materials.

A method of catalytic hydrocracking. The method includes flowing a hydrocarbon feed comprising a heavy oil into a hydrocracking unit; and hydrocracking the hydrocarbon feed in the hydrocracking unit using a composite catalyst. The composite catalyst includes an ordered amorphous silica-alumina (OASA) having mesopores, a zeolite component having micropores, a first metal component, a second metal component, and a support material, where at least a fraction of the heavy oil is converted within the mesopores into an intermediate, and at least a fraction of the intermediate is further converted within the micropores to form a product stream including a middle distillate fraction.

The invention discloses alkali-activated gypsum glass particle concrete and a preparation method thereof, and belongs to the technical field of building materials. The invention aims to solve the technical problems of poor interface cohesiveness and stockpiling pollution of industrial byproduct gypsum caused by the use of inert aggregate in traditional alkali-activated gypsum concrete. The concrete is prepared from the following raw materials in parts by weight: 10-15 parts of an alkali activator, 30-40 parts of dehydrated gypsum and 50-60 parts of tempered glass particles. In addition, the concrete further comprises a polycarboxylate superplasticizer and a protein gypsum retarder, and the addition amounts of the polycarboxylate superplasticizer and the protein gypsum retarder are respectively determined based on the total mass of the main body material and the mass of the dehydrated gypsum. The core of the invention is that the active aggregate formed by crushing the waste toughened glass is utilized, and amorphous silicon dioxide rich in the active aggregate can react in an alkali excitation environment to generate CSH gel, so that an interface transition region between the aggregate and a rubber material is remarkably reinforced, and the mechanical property of the concrete is improved. Meanwhile, industrial by-product gypsum such as ardealite and the like can be used, and high-added-value resource utilization of the solid waste is achieved.

The invention relates to the technical field of rock mechanics tests, and discloses a multiphase transparent rock-soil body sample preparation method and a visual combined test system.The sample preparation method comprises the following steps that S1, fused quartz sand and transparent glass sand are mixed, cooled after being cleaned and subjected to heat preservation till solidification, and a transparent skeleton structure module is formed; s2, removing impurities from amorphous silicon dioxide formed by melting natural silica, washing with water, and mixing with an epoxy resin solution to form a transparent rock matrix module; s3, filling the transparent rock matrix module and the transparent skeleton structure module into a sample shaping mold, and uniformly mixing the transparent rock matrix module and the transparent skeleton structure module; s4, demoulding and naturally cooling; s5, absolute ethyl alcohol is used for cleaning, then drying is conducted, and the multiphase transparent rock-soil body sample is obtained. According to the invention, real-time visual monitoring of the target sample is realized, and acoustic-optical-thermal-electric combined monitoring of the target sample is realized through the four-dimensional combined test system.

To provide an amorphous silica-alumina capable of controlling a hydrocracking reaction of a long-chain paraffin to primary cracking with high efficiency and exhibiting high catalytic activity when containing an active metal element, and to provide a method for producing the same.SOLUTION: The amorphous silica-alumina has a ratio of the pore volume of pores having a diameter of 0-2 nm to the pore volume of pores having a diameter of 0-10 nm of ≥60% and a specific surface area of ≥280m2 / g.SELECTED DRAWING: None

The invention discloses a high-capacity sodium-ion battery layered oxide positive electrode material, and relates to the technical field of sodium-ion battery preparation, the high-capacity sodium-ion battery layered oxide positive electrode material is prepared by ball-milling a precursor and sodium carbonate and then roasting, amorphous silicon dioxide is formed by a polysiloxane main chain in a molecule during roasting, and the high-capacity sodium-ion battery layered oxide positive electrode material is obtained. Silicon dioxide can inhibit transition metal ions from being dissolved in electrolyte in the circulation process, so that capacity fading and negative electrode SEI film damage caused by dissolution of the transition metal ions are avoided, meanwhile, the silicon dioxide serves as a buffer matrix to absorb mechanical stress and prevent particles from being broken, the circulation stability of the material is remarkably improved, and the service life of the material is prolonged. The boron element and part of the silicon element on the main chain form a boron-silicon oxide which can expand the sodium layer and the transition metal layer and broaden the diffusion channel of sodium ions, so that the ion migration energy barrier is reduced, the rate capability is improved, the transition metal ions can be prevented from being migrated to the sodium layer, and the mixed arrangement of cations is reduced.

The present invention relates to process for producing a hot blended material of amorphous silicon dioxide - crystalline silicon dioxide (Hot Blending silica - PheniSilic™) from materials containing silicon dioxide such as sand, cristobalite, crushed glass, waste rock powder / burrs from process of producing artificial stone, waste products and by-products from the exploitation and processing of natural quartz stone. The present invention also relates to artificial stone product produced by using base resins such as unsaturated polyester, epoxy, acrylic or combination thereof and reinforcement is the hot blended material of amorphous silicon dioxide - crystalline silicon dioxide wherein the artificial stone has a flexural strength > 40N / mm2, a water absorption ≤ 0.05%, an impact resistance ≥ 3J, as well as process for producing this artificial stone.

The invention relates to a process for preparing an aged building material from a process for additively manufacturing a three-dimensional object, wherein the preparation process comprises: mixing i) an aged building material from a process for additively manufacturing a three-dimensional object, wherein: the process for additively manufacturing a three-dimensional object comprises providing a building material layer by layer and selectively solidifying the building material layer by layer by the action of electromagnetic radiation, emitted by a radiation source, at positions in each layer that correspond to the cross section of the object in this layer; and the non-solidified building material is detached and forms the aged building material, and ii) a fresh building material for additively manufacturing a three-dimensional object, wherein: a prepared building material for additively manufacturing a three-dimensional object is formed; the aged building material and the fresh building material each contain a polymer and at least the fresh building material contains an amorphous silicon dioxide; and the ratio based on percent by weight of aged building material to fresh building material is greater than 60:40.

The invention relates to the technical field of papermaking, in particular to a preparation method of ultrathin high-strength paper-based adhesive tape base paper. The preparation method comprises the following steps: mixing softwood pulp and hardwood pulp, forming base paper by adopting a double-net dehydration process, and forming a covalent cross-linked network in a paper sheet by adopting a cellulose reactive coupling agent with an o-benzoquinone structure and a multi-sulfydryl compound based on a sulfydryl-benzoquinone click chemistry and interface supramolecular assembly multi-bonding enhancement system; meanwhile, a dual intelligent enhancement system based on a biomacromolecule self-assembly body and a dynamic metal coordination network is established, and dynamic reversible crosslinking is constructed through a polyelectrolyte compound and a Fe < 3 + >-tannic acid coordination network; a multifunctional surface treatment technology combining a zwitterionic polymer brush and bionic in-situ mineralization is developed, a sulphobetaine methacrylate polymer brush grows through a surface-initiated atom transfer radical polymerization method, amorphous silicon dioxide is induced to be mineralized, and the adhesive tape body paper prepared through the method is high in strength.

A method for separating a fluorocarbon gas including feeding a mixed gas that includes two or more kinds of fluorocarbon gases having different molecular diameters from each other to a porous membrane and separating a gas composition in which a mixing ratio of one kind of a fluorocarbon gas selected from the two or more kinds of fluorocarbon gases is increased or a single gas, where the porous membrane includes amorphous silica formed by a sol-gel method.

The invention provides a low-permeability complex porous medium molecular modeling method which comprises the following steps: performing three-dimensional space expansion on a silicon dioxide crystal based on a selected CLAYFF force field to obtain a superunit cell with a preset size; carrying out simulated annealing on the super-unit cell according to a preset heating parameter and a preset cooling parameter to obtain amorphous silicon dioxide; carrying out three-dimensional space stretching expansion on the amorphous silicon dioxide system according to the total porosity to obtain a porous medium model; obtaining the number of hydroxyl groups needing to be added according to the pore surface area of the porous medium model, and adding the hydroxyl groups to silicon atoms of the porous medium model for surface end capping to obtain a first porous medium model; the second porous medium model is used for carrying out quantity adjustment and / or replacement of hydrophilic hydroxyl groups / hydrophobic methyl groups on the first porous medium model and is adjustable in hydrophilicity and hydrophobicity; and carrying out water molecule input or gas molecule injection on the second porous medium model to obtain a target porous medium molecular model.

The invention relates to the technical field of molding sand binders for casting, in particular to preparation and application of a water-resistant and moisture-resistant silicate inorganic binder, the binder is composed of a liquid component and a solid powdery reinforced modifier, based on the mass of sand, the adding amount of the liquid component is 2%, and the adding amount of the solid powdery reinforced modifier is 1%; the liquid component comprises liquid sodium silicate, a silane coupling agent and an organic silicon waterproof agent; the solid powdery reinforced modifier comprises amorphous silicon dioxide, metakaolin and fly ash; the hardening condition of the binder is that the binder is heated and hardened at 150-200 DEG C. According to the invention, geopolymers such as metakaolin and the like are introduced into a solid powdery reinforced modifier, and a three-dimensional network structure is formed by a silica tetrahedron and an alumina tetrahedron, so that water resistance and moisture resistance are realized through an alkali excitation reaction; and meanwhile, silane and an organic silicon waterproof agent are combined to form a synergistic waterproof effect, so that the prepared sand core does not bleed in water and does not fall apart after being soaked in water for several days.

The invention discloses black spherical silicon as well as a preparation method and application thereof, and relates to the technical field of copper-clad plates. The black spherical silicon provided by the embodiment of the invention has a core-shell structure, a shell layer is a silicon dioxide layer, a core layer is an amorphous silicon dioxide composite material, and the black spherical silicon can give consideration to dielectric loss and peel strength by regulating and controlling the content of surface active groups under unit mass to meet a specific range; and the thickness of the silicon dioxide of the shell layer accounts for 0.4-12% of the overall size, so that the absorption capacity of the powder to ultraviolet light is controlled, the reflective rate R is less than or equal to 10%, and the withstand voltage is greater than or equal to 5KV. The black spherical silicon provided by the invention has the characteristics of low dielectric loss and low reflective rate, and can reduce dielectric loss, reduce signal attenuation and improve stability after being used for a copper-clad plate.

The present application relates to a kind of tetrahydrofurfuryl alcohol preparation method, which includes the following steps: in the presence of catalyst, furfural and hydrogen are contacted and reacted;The catalyst includes the composite of nickel and silicon dioxide, wherein, nickel is crystal structure, and silicon dioxide is amorphous structure.The present application uses the composite of crystalline nickel and amorphous silicon dioxide as catalyst to catalyze furfural hydrogenation, so that the whole reaction process has less side reaction, and conversion and yield are relatively high, can realize tetrahydrofurfuryl alcohol stable, continuous and efficient production, and has important significance to bio-chemical industry, medicine and health and other fields.

An adhesive includes a styrenic block copolymer having a styrenic block and a conjugated diene block that is hydrogenated or not hydrogenated, a tackifying resin, and at least one of precipitated amorphous silica or a precipitated amorphous silicate. The adhesive can further include at least one of a plasticizer or a second tackifying resin having a glass transition temperature lower than the first tackifying resin. The precipitated amorphous silica or precipitated amorphous silicate may be surface modified with hydrophobic groups. The adhesive can further include natural rubber. The adhesive may have not more than 4.5 weight percent polyisobutylene or a polyisobutylene copolymer, based on the total weight of the adhesive, or may be free of polyisobutylene and a polyisobutylene copolymer. A tape includes the adhesive disposed on a backing. Processes for making and using the tape are also provided.

The invention relates to the technical field of solid waste recycling, and discloses a method for preparing a water purifying agent from lithium extraction tailings and the prepared water purifying agent, quartz, feldspar and magnetic minerals are separated by a physical separation method through an impurity removal and extraction technology of selective purification, activated calcination, acid leaching polymerization and composite blending, and an iron-containing clay phase is reserved; the PAC-PPS-porous silica gel composite system water purifying agent with an efficient water purifying effect is obtained by calcining and activating kaolin, removing hydroxyl and converting into metakaolin, carrying out controllable acid leaching to avoid excessive purification of iron ions, and finally, carrying out composite blending to obtain the PAC-PPS-porous silica gel composite system water purifying agent with an efficient water purifying effect. According to the method, the lithium extraction tailings are creatively used as the raw material, and the iron-containing ore phase and the iron element are reserved as far as possible, so that the flocculation capacity of the water purifying agent is improved, and the water purifying effect is improved; amorphous silicon dioxide filter residues and polymeric ferric sulfate are added step by step, the pH is adjusted in stages, and PAC, PFS and amorphous silicon dioxide are compounded for use, so that the water purification effect of the water purifier is further enhanced.

The invention relates to the technical field of perovskite thin film material preparation and structural design, and discloses a barium titanate thin film structure and a preparation method thereof. The barium titanate film structure comprises a substrate, an amorphous buried oxide layer, a silicon nitride or silicon core layer waveguide, a crystallized magnesium oxide buffer layer and a crystallized barium titanate layer. The amorphous buried oxide layer is arranged on the substrate, the silicon nitride or silicon core layer waveguide is located in the buried oxide layer, and the crystal buffer layer film is arranged on the amorphous buried oxide layer. Wherein the buffer layer film can directly grow and crystallize on an amorphous buried oxide layer (such as amorphous silicon dioxide), the barium titanate film takes the buffer layer as a growth template to perform growth and crystallization, the growth of barium titanate is not restrained by a substrate of a specific material or a crystal structure, and the preparation process from bottom to top is simple; and the used preparation means is low in cost and suitable for large-scale industrial production.

The invention discloses a sewage treatment agent preparation method and a sewage treatment method and device, and relates to the technical field of sewage treatment. The preparation method of the sewage treatment agent comprises the following steps: step 1, grinding steel slag until the particle size is 0.1-2.5 mm; 2, dilute sulphuric acid with the concentration of 5%-20% is added into the reaction tank according to the solid-to-liquid ratio of 1 kg: (8-15) L, and a reaction is conducted for 50-7 min under stirring at the temperature of 20-25 DEG C and the speed of 150-200 rpm. By adopting the technical scheme, ferrous sulfate and polyaluminum chloride are replaced by the steel slag, so that the steel slag is reutilized with high value, the addition of sewage treatment chemicals is reduced, and the output of sludge is reduced; indissolvable solid residues in the steel slag are dehydrated into calcium sulfate dihydrate, calcium silicate and amorphous silicon dioxide which can be used as building raw materials, secondary pollution caused by the building raw materials is avoided, and the value of the steel slag is fully exerted.

The present disclosure aims to provide a novel method for separating a fluorocarbon. A method for separating a fluorocarbon gas comprising: feeding a mixed gas comprising two or more kinds of fluorocarbon gases having different molecular diameters from each other to a porous membrane and separating a gas composition in which a mixing ratio of one kind of a fluorocarbon gas selected from the two or more kinds of fluorocarbon gases is increased or a single gas, wherein the porous membrane comprises amorphous silica formed by a sol-gel method.

The present application is an NPK-Si fertilizer, a method for its production and use. The present application relates to a combined NPK-Si fertilizer product comprising a mineral NPK fertilizer, which comprises at least one nutrient compound of nitrogen, phosphorus or potassium, and particulate amorphous silicon dioxide, wherein the ratio of the mineral NPK fertilizer to the amorphous silicon dioxide is 10:90 to 90:10, based on the dry weight of the at least one nutrient compound of nitrogen, phosphorus or potassium and the amorphous silicon dioxide contained in the product. The present application also relates to a method for producing the NPK-Si fertilizer of the present application.

An article having a coating system configured to inhibit or prevent crystallization of TGO at the operating temperature of the article. An article includes a substrate defining a surface and a coating layer that includes a dopant configured to inhibit crystallization of amorphous silicon dioxide thermally grown oxide on the bond coat at an operating temperature of the article. The dopant includes a glass modifier. By inhibiting or preventing TGO crystallization, the described coating systems may increase a useable life of the component.

The invention provides a high-strength cement-based grouting material and a preparation method thereof. The high-strength cement-based grouting material comprises the following components: Portland cement, fly ash, an expanding agent, quartz sand, a water reducing agent, a powder defoaming agent, a plastic expanding agent and a strength enhancer. Wherein the strength enhancer is prepared by taking rice hulls as a raw material, carrying out constant-temperature calcination to obtain rice hull ash, modifying one part of the rice hull ash with KH560, carrying out heating calcination on the other part of the rice hull ash, carrying out hydroxylation treatment on the other part of the rice hull ash, then carrying out KH550 modification, and finally carrying out blending reaction on the two parts of products. In the strength enhancer disclosed by the invention, products obtained by calcining rice hulls in two stages are respectively amorphous silicon dioxide and cristobalite, and after the rice hulls are modified by KH560 and KH550, an epoxy group is grafted on the surface of the amorphous silicon dioxide, and an amino group is grafted on the surface of the cristobalite. The early strength and the later strength of the cement-based grouting material can be remarkably improved through the interaction of the amorphous silicon dioxide, the cristobalite and the cement matrix.

A method of making an aluminosilicate SSZ-82 is disclosed. The process comprises: (1) preparing a reaction mixture comprising: an amorphous alumina source comprising predominantly aluminum hydroxide; an amorphous silica source comprising predominantly colloidal silica; a source of alkali metal cations [M]; an organic structure directing agent [Q] comprising a 1, 6-bis (N-cyclohexylpyrrolidinium) hexane divalent cation; hydroxyl ions; a seed crystal, wherein the seed crystal comprises a crystalline molecular sieve having an SSZ-82 framework; and water; (2) heating the reaction mixture under crystallization conditions including a temperature from 100 DEG C to 200 DEG C for a time sufficient to form crystals of the aluminosilicate zeolite; (3) recovering at least a portion of the aluminosilicate zeolite from step (2).

The application relates to the technical field of plating, and discloses a low-expansion oxidation-resistant iron-nickel alloy base material and a preparation method thereof; the method comprises the following operation steps: in the scheme, an iron-nickel alloy base material is sequentially subjected to embedding aluminizing, micro-arc oxidation, coating of aluminum composite sol and temperature rising solidification to obtain the low-expansion oxidation-resistant iron-nickel alloy base material; wherein the iron-nickel alloy base material itself has the low-expansion characteristic, but the oxidation resistance is poor; if a ceramic layer is directly arranged on the surface of the iron-nickel alloy base material, the oxidation resistance can be improved, but the low-expansion characteristic of the material is reduced; in order to solve the problem, in the scheme, a transition layer is formed by embedding aluminizing to improve the combination of the micro-arc oxidation layer and the oxidation-resistant layer, and modified macrocyclic polysiloxane is added to raw materials of the micro-arc oxidation layer and the oxidation-resistant layer; the temperature is controlled to make the modified macrocyclic polysiloxane be converted into amorphous silicon dioxide at high temperature, and the thermal expansion of aluminum oxide is balanced.

This invention provides a sustainable and environmentally friendly consolidating material that can be supplied stably and does not cause environmental problems such as environmental pollution or increased carbon dioxide emissions, thereby enabling not only carbon neutrality but also carbon negativity, as well as a method for constructing soil structures and a ground improvement method using this material. [Solution] This solidifying material is mainly composed of silica-containing combustion products, which are obtained by partially burning and cooling land-derived waste and contain SiO2 and carbon as active ingredients. The amorphous silica in the silica-containing combustion products undergoes a hydration reaction and solidifies, thereby enabling carbon negativity.

The present application relates to electronic packaging materials, discloses a kind of surface coating modified silicon powder high modulus flow high reliability epoxy plastic packaging material and preparation method thereof.Epoxy functional oligomeric siloxane, tetraethyl orthosilicate and 3-glycidoxypropyltrimethoxysilane are co-prehydrolyzed and coated on the surface of spherical amorphous silicon dioxide in weak acidic ethanol-water system, then 3-glycidoxypropyltrimethoxysilane is added, and pre-hydrolyzed and non-pre-hydrolyzed 3-aminopropyltriethoxysilane is introduced in sequence to obtain modified silicon powder;After melting and mixing with epoxy resin, phenolic resin and the like, epoxy plastic packaging material with longer modulus flow length, lower water absorption and fewer packaging pores can be obtained, which is suitable for integrated circuit packaging.