The invention relates to a
titanium nickel aluminium molybdenum alloy material which is of a hollow
cathode plasma sintering body and comprises the following components in atomic percent: 47-48.5% of
titanium, 45-46.5% of
nickel, 0.5-1% of
molybdenum and the balance of
aluminium, wherein the
titanium content is 1-3% higher than the
nickel content. A preparation process of the titanium nickel
aluminium molybdenum alloy material comprises the following steps of: weighing
titanium powder with certain
granularity, nickel
powder,
aluminium powder and prealloy
powder with the molybdenum content of 20wt% in the atomic percent of each component, carrying out ball milling, mixing, sieving, and obtaining a compacted blank by virtue of compression moulding; and forming a hollow
cathode by virtue of the compacted blank and a
graphite plate reflecting screen, realizing high-temperature rapid
sintering on the compacted blank by adopting a hollow
cathode plasma sintering method, and cooling, so that the
alloy material is obtained. The titanium nickel aluminium molybdenum alloy material provided by the invention has good
plasticity and strength, grains of the sintering body are uniform, the structure is compact, and the cost is low. The hollow cathode
plasma sintering preparation process is simple, the problem that requirement on
smelting and
casting technological equipment is high is solved, the preparation temperature is obviously reduced, the material utilization is improved, the
energy consumption is reduced, and the cost is saved.