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49results about How to "Reduce aldehyde content" patented technology

Method for preparing TCPP (Tris(Chloroisopropyl)Phosphate) flame retardant

The invention relates to a preparation method which can effectively eliminate odor ingredients (mainly aldehydes compounds) in TCPP (Tris(Chloroisopropyl)Phosphate). The method is characterized by comprising the following steps of: adding excessive oxidant solution relative to the aldehydes compound for reaction after a TCPP crude product is obtained through reaction, standing, separating liquid, then alkaline washing, water washing and distilling. The aldehyde compound which has favorable compatibility with the TCPP and is not separated easily can be removed, the aldehyde content in the TCPP is reduced to below 10 ppm from the previous 100 ppm or more and can be reduced to 0.7 ppm in the maximum degree, the odor of the TCPP and the prepared product is less, and the mild odor of the TCPP flame retardant is realized; and oxidant aqueous solution converting aldehyde into acid is added to react, wash and remove the odor, the method has convenient operation as well as simple, convenient and easy implementation, is beneficial to operation in production and does not affect the TCPP yield (the yield can increase by 0.5-1%) and an acid value compared with the previous patents; the aldehyde content can be reduced to a lower degree, and the obtained TCPP product is more stable.
Owner:雅克(上海)化工新材料有限公司

Preparation method of multi-taste Maotai-flavor white spirit

ActiveCN102453651BLong aftertastePerfect display of personality styleAlcoholic beverage preparationBiotechnologyWhite spirit
The invention discloses a preparation method of multi-taste Maotai-flavor white spirit. Eleven flavor types of white spirits are taken as seasoning liquors, the preparation method is characterized by comprising the following steps of: finishing and soaking grains; cooking, gelatinizing and mixing with Luzhou-flavor white spirit fermented grains and Maotai-flavor white spirit fermented grains; spreading out and airing, stirring distiller's yeast, adding Maotai-flavor ending liquor, Luzhou-flavor yellow wine, Maotai-flavor fermented grains and Maotai-flavor yeast, and accumulating and fermenting; fermenting in a cellar, and spraying mixed solution of the Maotai-flavor ending liquor and the Luzhou-flavor yellow wine on the surface of each distilled grain layer; making sand and adding the Luzhou-flavor white spirit fermented grains, cooking and gelatinizing, then adding the Maotai-flavor ending liquor, the Luzhou-flavor yellow wine, the Maotai-flavor fermented grains and the Maotai-flavoryeast, accumulating and fermenting, and storing in the cellar and spraying the mixed solution of the Maotai-flavor ending liquor and the Luzhou-flavor yellow wine on each distilled grain layer; steaming by using a rice steamer to obtain unblended wine in rounds of 1, 2, 3, 4, 5, 6 and 7, and the wine in the seven rounds are combined according to taste and-flavor characteristics, so as to obtain combined Maotai-flavor unblended wine; and then blending the combined unblended wine with flavoring liquor, thus obtaining the multi-taste Maotai-flavor white spirit. The preparation method disclosed by the invention has the advantages of enriching-flavor of Maotai-flavor white spirit, meeting market demand and promoting development of the Maotai-flavor white spirit.
Owner:SICHUAN TUOPAI SHEDE WINE

A kind of extraction method of litsea cubeba oil

The invention discloses a method for extracting litsea cubeba oil. The whole fresh fruit of litsea cubeba is added in a boiling state, the steam pressure is 0.2-0.3MPa, and the water is distilled for 1-1.5h, the oil and water are separated to obtain litsea cubeba oil, and the liquid residue is separated , drying the combined seed cores to obtain dry litsea cubeba seed cores, and adding strains to the fruit puree to produce bio-organic fertilizers according to the usual method. Compared with the existing crushing or peeling technology, the present invention reduces the equipment investment for fresh fruit crushing or peeling, prevents litsea cubeba pulp from contacting with air, improves the oil yield and product quality, and the oil yield is 5.5-5.8%. The total aldehyde content reaches more than 75%. The by-product dried cubeb seeds are used as medicinal materials and food, and bio-organic fertilizers are used for forestry and agriculture, realizing resource recycling economy, shortening the production cycle, high equipment utilization rate, large processing capacity, energy saving and reduction consumption, reduces production costs, and has good economic, social and ecological benefits. Patents have good economic, social and ecological benefits.
Owner:GUANGXI FORESTRY RES INST

Negative pressure mash tower degassing, aldehyde-discharging and acid-discharging device for fuel ethanol and edible alcohol

The invention discloses a negative pressure mash tower degassing, aldehyde-discharging and acid-discharging device for fuel ethanol and edible alcohol. The device comprises a negative pressure mash tower. A first tower plate is arranged in the negative pressure mash tower; a degassing section is arranged above the negative pressure mash tower, a second tower plate is arranged in the degassing section, an aldehyde discharging section is arranged above the degassing section, and fillers are arranged in the aldehyde discharging section. The invention also discloses a production method for improving the alcohol quality by using the device. Compared with the traditional mash tower, the relatively pure crude wine steam rising from the negative pressure mash tower is used for degassing fermentedmash and discharging aldehyde from crude alcohol without increasing steam consumption, pre-impurity removal of the fermented mash and the crude alcohol is achieved, carbon dioxide in the fermented mash and most low-boiling-point aldehydes and volatile acids in the crude alcohol are removed in the degassing section and the aldehyde discharging section, the aldehyde content and the acidity of the crude alcohol are reduced, the subsequent tower impurity discharging load is effectively reduced and the comprehensive quality of the alcohol is improved.
Owner:肥城金塔酒精化工设备有限公司

Purification method for preparing ethylene glycol from coal-based synthesis gas

The invention relates to the technical field of ethylene glycol production, and provides a purification method for preparing ethylene glycol from coal-based synthesis gas. According to the present invention, ethylene glycol is purified by using a 1# resin tower and a 2# resin tower, the resin filled in the 1# resin tower is SQYJ-2 enhanced ultraviolet resin, and the resin filled in the 2# resin tower is SQYJ-1 dealdehyding catalyst resin; and the SQYJ-2 resin can improve the ultraviolet light transmittance of ethylene glycol and has a slight dealdehyding effect, and the SQYJ-1 resin can reduce the aldehyde content of ethylene glycol. According to the specific condition of the ethylene glycol extracted from the side line of the product tower, the ethylene glycol is selectively introduced into the 1# resin tower or the 2# resin tower, or the ethylene glycol is introduced into the 1# resin tower and then into the 2# resin tower, so that the purification of the ethylene glycol is realized. The ethylene glycol purified by the method disclosed by the invention is high in ultraviolet light transmittance and low in aldehyde content, and can reach the standard of superior products in GB/T4649-2008.
Owner:JIANGSU SUQING WATER TREATMENT ENG GROUP
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