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51results about How to "The experiment takes a short time" patented technology

Core-shell structure catalyst for fuel cells and its pulse electrodeposition preparation method

The invention discloses a core-shell structure catalyst for fuel cells and its pulse electrodeposition preparation method. The active component of the catalyst is a nanoparticle with a core-shell structure, and an active metal is cladded in the form of an ultrathin shell on the surface of a carbon carrier loaded metal or alloy nanoparticle serving as a core. The catalyst takes a non-platinum noble metal or transition metal as the core, and adopts more than one of Pt, Ir or Au as the shell. The preparation method includes: preparation of the nanoparticle serving as the core, making of a working electrode for pulse electrodeposition, and preparation of the catalyst by pulse electrodeposition. The catalyst can be used as an anode or cathode catalyst of a low temperature fuel cell. The obtained catalyst has very high stability. Compared with underpotential deposition, the method is simple to operate, has no need for inert atmosphere protection, and is more suitable for large-scale industrial production, also can greatly reduce the noble metal consumption of fuel cells, and greatly reduce the cost of fuel cells, thus having great significance in promoting the commercialization process of fuel cells.
Owner:SOUTH CHINA UNIV OF TECH

SSR molecular marker method of brassica allohexaploid and primers thereof

The invention discloses an SSR molecular marker method of a brassica allohexaploid and primers thereof. The SSR molecular marker method of the brassica allohexaploid comprises the steps: hybridizing a brassica allohexaploid parent, and performing microspore culture on the obtained filial generation to obtain a DH colony; extracting genome DNAs of the brassica allohexaploid parent and the DH colony, and performing PCR amplification with all genome DNAs as a template by using the primers; constructing a genetic map of the brassica allohexaploid parent according to a PCR amplification result, wherein 217 pairs of primers are included, with base sequences respectively shown in SEQ ID No. 1 / 2-433 / 434. According to the SSR molecular marker method, a first genetic map of the brassica allohexaploid is constructed, and the basis is provided for further performing QTL location and molecular marker assistant breeding.
Owner:ZHEJIANG UNIV

Method for detecting hemoglobin by liquid chromatogram-triple tandem quadrupole mass spectrometer

The invention discloses a method for detecting hemoglobin by a liquid chromatogram-triple tandem quadrupole mass spectrometer. The method comprises the following steps that 1, a standard substance solution and a sample needing to be detected respectively pass through a solid phase extraction column so that a sample needing to be detected is obtained; 2, the sample needing to be detected is detected by the liquid chromatogram-triple tandem quadrupole mass spectrometer, wherein the chromatographic conditions comprise that a C18 chromatographic column is adopted and a mobile phase A (acetonitrile) and a mobile phase B (formic acid aqueous solution) are used for gradient elution; and 3, through the detection result, hemoglobin content of the detected sample is obtained. Compared with the method recommended by IFCC, the method provided by the invention shortens the whole detection time to 12min, reduces spectrometer operation time by 50%, guarantees good singularity and accuracy, improves a spectrometer utilization rate, and can be used as a reference method for detecting hemoglobin.
Owner:BEIJING CHAOYANG HOSPITAL CAPITAL MEDICAL UNIV

Thermal treatment production stimulating device and experimental method

The invention relates to the field of aluminum alloy thermal treatment equipment and process stimulators, in particular to a thermal treatment production stimulating device and experimental method. The thermal treatment production stimulating device comprises a solid solution furnace, an aging oven and a cooling device, wherein the solid solution furnace is connected with the cooling device; and the aging oven is separately connected with the solid solution furnace and the cooling device. The thermal treatment production stimulating experimental method utilizes the device to perform simulation experiment, and comprises the following experimental steps of: S1, performing solid solution on an aluminum alloy material slice; S2, performing cooling or aging treatment on the aluminum alloy material slice subjected to solid solution; and S3, performing ageing treatment on the cooled aluminum alloy material slice. According to the thermal treatment production stimulating device and experimental method disclosed by the invention, various aluminum alloy sheet and strip thermal treatment key equipment such as solid solution equipment, cooling equipment and aging equipment are integrated onto one set of devices, so that experimental test is convenient, flexibility is strong, experimental cost is low, experiment can be repeatedly performed, experimental parameters can be precisely controlled, experimental repeatability is good, experimental time consumption is short and experiment can be performed at any time. While a great deal of investment is saved, cost and time of experiment are also saved.
Owner:NORTHEASTERN UNIV

Asphalt adhesive power test device and method

The invention discloses an asphalt adhesive power test device and method. The test device comprises a base, an adhesive belt and a support plate, wherein a vertical back plate is arranged on the base;the top end of the adhesive belt is fixed to the back plate; the bottom end of the adhesive belt is used for sticking a sample in a sample box; the support plate is arranged horizontally; the supportplate can slide longitudinally along the back plate; a horizontal slide bar is fixed to the support plate; and the horizontal slide bar is in sliding fit with the sample box; and the bottom of the support plate is connected with a weight box. The invention also discloses a test method. Through adoption of the test device and method, the experiment steps of the asphalt adhesive power are simplified; the experiment time is shortened; and the experiment process becomes easier and more convenient.
Owner:HOHAI UNIV

Method for extracting bacterium genomic DNA by using magnetic nanoparticles

The invention discloses a method for extracting bacterium genomic DNA by using magnetic nanoparticles, belonging to the technical field of nanomaterials and molecular biology. The method comprises the steps of: preparing a magnetic nanoparticle aggregate, preparing a bacterium lysing solution, preparing and adding an absorption buffer solution, absorbing with a magnet, rinsing with 70 percent alcohol, and eluting with a TE buffer solution to obtain a bacterium genomic DNA solution. Compared with the traditional phenol / chloroform DNA extracting method, the method for extracting the bacterium genomic DNA by using magnetic nanoparticles has the advantages of short experiment time, simpleness in operation, high extraction efficiency, rapidness, convenience, sensitivity, high yield and the like; and the extracted bacterium genomic DNA can be completely used for subsequent experiments, such as DNA hybridization, PCR (Polymerase Chain Reaction), and the like, and provides the basis for the subsequent research and analysis.
Owner:JIANGNAN UNIV

Method for indirectly measuring dry deposition velocity of PM2.5 on surface of plant

The invention provides a method for indirectly measuring the dry deposition velocity of PM2.5 on the surface of a plant. The method comprises the following steps: preparing simulated PM2.5 with the particle size of 2.5 [mu]m; determining the initial concentration and measurement time length of the PM2.5 in a smog chamber in a testing process, wherein a concentration time-varying rule of the PM2.5 is consistent with a stable exponential decaying rule; measuring concentration time-varying rules of the PM2.5 in the smog chamber under an empty condition and a condition of existence of a leaf sample respectively, and performing data fitting to calculate decaying velocity constants j and k of two curves respectively; calculating the dry deposition velocity Vd of the PM2.5 on the leaf sample to be measured according to formula (I) (specified in the original document) on the basis of the above data. According to the method, the formula obtained by observation data fitting is adopted for calculation, so that system errors can be greatly reduced, the measurement accuracy can be improved, and moreover, the method is low in experimental cost and experimental time consumption and more convenient and easier to operate.
Owner:SHANGHAI JIAO TONG UNIV

Sample fixing platform and freeze scanning electron microscope containing same

The invention relates to the technical field of sample fixing devices, and specifically relates to a sample fixing platform. The sample fixing platform comprises a base and a cylinder arranged on the base, wherein a plurality of sample placing positions are arranged at the upper end of the cylinder; and fixing parts for fixing samples are arranged on the sample placing positions. The invention also relates to a freeze scanning electron microscope containing the sample fixing platform. According to the sample fixing platform and the freeze scanning electron microscope containing the sample fixing platform provided by the invention, a plurality of fixing parts are arranged at the upper end of the cylinder, and a plurality of samples such as blades can be fixed simultaneously, so that the consumed time for experiments is short, the experiment efficiency is greatly improved, and the economic cost in the experimental process is also reduced.
Owner:INST OF GENETICS & DEVELOPMENTAL BIOLOGY CHINESE ACAD OF SCI

Femtosecond time-resolved multi-channel lock-in fluorescence spectrometer based on optical parametric amplification

The invention provides a femtosecond time-resolved multi-channel lock-in fluorescence spectrometer based on optical parametric amplification. The spectrometer includes a laser light source and a light beam splitting sheet; a sample excitation light generating part for frequency conversion of fundamental frequency light outputted by the laser light source; a sample excitation light focusing device and a sample-fixing sample pool; a sample fluorescence collecting and condensing system; a generating part of pumping light required by fluorescence optical parametric amplification; an optical parametric crystal for allowing the pumping light and fluorescence to generate a non-collinear optical parametric process; a time-resolved fluorescence spectrum data acquisition system; and a light path delay system for changing time delay of the optical parametric pumping light and the sample excitation light. The data acquisition system is a data acquisition system based on a multi-channel lock-in amplifier. Time-resolved fluorescence spectra without super fluorescent background interference can be obtained by single measurement.
Owner:INST OF PHYSICS - CHINESE ACAD OF SCI

Microstructure parameter-based clay consolidation coefficient prediction method

The invention provides a microstructure parameter-based clay consolidation coefficient prediction method, which comprises the steps of: conducting clay consolidation experiments under different pressures, and measuring the void ratio according to conventional geotechnical experiments; calculating the consolidation coefficients of different consolidation experiments; employing a scanning electron microscope technique to obtain a microstructure photo of a corresponding sample section; carrying out granule area and void area segmentation on the clay microstructure photo, and extracting the information of granule unit sum, unit direction, total area, total circumference, and area ratio; analyzing the granules and establishing a main component expression with an accumulative contribution rate of over 95%; and establishing the relationship between the main components and the clay consolidation coefficient. The method provided in the invention links the consolidation coefficient of clay with its microstructure parameters to obtain corresponding consolidation coefficient indexes under different pressures according to the clay void ratio and micro-parameter main components. The method can effectively shorten the experiment time at a civil engineering investigation phase.
Owner:TIANJIN URBAN CONSTR COLLEGE

Suspension device and suspension method

InactiveCN109512542ASuspension is safe, fast and non-destructiveCause damageAnimal fetteringEngineeringExperimental animal
The invention discloses a suspension device and a suspension method, and belongs to the technical field of animal experiments. The suspension device includes a tail tying belt, a suspension rope and an inflation mechanism; the tail typing belt includes a cloth bag and an air bag; the cloth bag includes a first side and a second side, the first side is opposite to the second side, and the first side is bonded to the second side; the air bag is arranged in the cloth bag; both ends of the suspension rope are respectively connected with the first side; and the inflation mechanism is communicated with the air bag. The suspension device and the suspension method can realize safe, fast and lossless suspension of an experimental animal.
Owner:JIANGHAN UNIVERSITY

Testing system, method and device for satellite electric propulsion system

The invention discloses a test system, method and device for a satellite electric propulsion system, and the system comprises a vacuum tank which is used for providing a vacuum environment for the satellite electric propulsion system; a satellite electric propulsion system which is arranged in the vacuum tank and comprises a power supply processing unit and an electric thruster, wherein the powersupply processing unit is used for supplying power, and the electric thruster is used for generating thrust; a load simulator which is used for simulating load characteristics of the electric thrusterin at least one state; and a simulation access conversion device which is arranged between the satellite electric propulsion system and the load simulator and is used for connecting the power supplyprocessing unit with the load simulator or the electric thruster. The technical problem that in the prior art, an electric propulsion system thermal vacuum experiment consumes long time is solved.
Owner:CHINA ACADEMY OF SPACE TECHNOLOGY

Method for analyzing trace substances in to-be-tested sample by utilizing electrospray ionization-mass spectrometry of molecularly imprinted membrane

The invention provides a method for analyzing trace substances in a to-be-tested sample by utilizing an electrospray ionization-mass spectrometry of a molecularly imprinted membrane. The method comprises the following steps: 1) modifying and activating the surface of a microfiltration membrane; 2) soaking the modified and activated microfiltration membrane into a reactive solvent containing template molecules, functional monomers, a crosslinking agent and an initiator, deoxygenizing and reactively synthesizing a molecularly imprinted membrane; 3) soaking the molecularly imprinted membrane synthesized in the step 2) into an elution solvent, shaking at room temperature to remove the template molecules; and 4) adding the molecularly imprinted membrane in the step 3) into the to-be-tested sample, shaking for 10-30min at room temperature, taking out, and detecting the molecularly imprinted membrane by adopting a molecularly imprinted membrane electrospray ionization device. According to the method, sample pretreatment is not needed, the real-time rapid analysis of the practical sample under high sensitivity can be realized, and the method has extremely high application values in the fields of food safety, plasma concentration, antibiotic residues and pesticide residues, and has wide application prospects.
Owner:ICDC CHINA CDC +1

Marine acoustic phase center calibration method

The invention discloses a marine acoustic phase center calibration method, and relates to the field of marine surveying and mapping. The problems that according to an existing acoustic phase center calibration method, a pool experiment needs to be carried out in advance to calibrate the acoustic phase center of an acoustic array, the experiment time consumption is long, and the efficiency is low are solved. The method comprises the following steps: S1, enabling a workboat to sail around a seabed beacon according to a preset track, and collecting data; S2, calculating the installation position deviation DX of a seabed beacon coordinate matrix and an acoustic array in a geodetic coordinate system by using the data collected in S1; S3, calculating coordinates of each element on an acoustic array in the workboat coordinate system according to the sum DX; and S4, calculating the length of each base line according to the coordinate of each element on the acoustic array in the workboat coordinate system, and calibrating the acoustic phase center of each element through each base line length. The method is mainly used for calibrating the element acoustic phase center.
Owner:HARBIN ENG UNIV

Method for extracting total DNA (Deoxyribonucleic Acid) of microorganisms from pile-fermentation Pu-erh tea

The invention relates to a method for extracting total DNA (Deoxyribonucleic Acid) of microorganisms from pile-fermentation Pu-erh tea. The method comprises the following steps of: 1) taking Pu-erh tea samples in different fermentation processes; 2) pretreating the Pu-erh tea samples to be extracted; 3) extracting the total DNA of the microorganisms from the pretreated samples; 4) carrying out agarose gel electrophoresis detection on the extracted total DNA of the microorganisms; 5) carrying out PCR (Polymerase Chain Reaction) amplification under the guidance of special primers by using the extracted total DNA as a template; and 6) carrying out the agarose gel electrophoresis detection on the fragments subjected to the PCR amplification.
Owner:TIANJIN TASLY GROUP

Method for calculating dislocation density of deformed crystal material based on single diffraction peak

The invention discloses a method for calculating dislocation density of a deformed crystal material based on a single diffraction peak. The method comprises the following steps of: utilizing a synchrotron radiation energy scanning X-ray diffraction technology to obtain an experimental intensity distribution curve of diffraction intensity of the deformed crystal material relative to a diffraction vector mode and a reference intensity distribution curve of diffraction intensity of a non-deformed crystal material relative to the diffraction vector mode; introducing a dimensionless variable M, andcalculating a standard intensity distribution curve of a diffraction peak after dislocation density normalization; calculating a specific M value of the experiment intensity distribution curve according to the experiment intensity distribution curve and the standard intensity distribution curve, and recording the specific M value as M'; and calculating the dislocation density of the deformed crystal material according to the full widths at half maximum of the experimental intensity distribution curve, the standard intensity distribution curve and the reference intensity distribution curve. The dislocation density of the deformed crystal material can be obtained by analyzing the intensity distribution curve of the single diffraction peak, and the experiment time is shortened.
Owner:XI AN JIAOTONG UNIV

Method for extracting total RNA of microalgae cells

InactiveCN109652407AReduced volume requirementsReduce grinding timeDNA preparationRNA extractionTotal rna
The invention discloses a method for extracting the total RNA of microalgae cells. The method has the advantages that microalgae is placed in a plant RNA extraction auxiliary fluid containing silica sand to be grinded, thereby achieving that grinding and polysaccharide removal treatment of the microalgae is rapidly completed through one step, greatly reducing the demands for the microalgae thallusamount, greatly simplifying the experimental operation, reducing the experimental time consumption. According to the method, breaking of the microalgae cell wall is combined with the removal of the microalgae so that the cell wall breaking and polysaccharide removal are completed within 5 min; through the innovation and improvement of the whole extraction method, the extraction time of the microalgae RNA is shortened to less than 30 min; on this basis, it is achieved that all the operations of the extraction of the microalgae RNA can be carried out in a general laboratory environment, and a special extraction environment of RNA enzyme removal is not needed; all experimental supplies do not need DEPC water for RNA enzyme removal treatment; the DEPC water is not harmful to the health of researchers while the early-stage preparation work is reduced, and the safety of experimenters is protected.
Owner:SOUTH CHINA UNIV OF TECH

Dot-matrix multi-thread high-temperature experiment system

The invention discloses a dot-matrix multi-thread high-temperature experiment system. The dot-matrix multi-thread high-temperature experiment system comprises a dot-matrix electric heating furnace, a plurality of groups of sample reactors, a plurality of gas paths and a plurality of gas supply devices. Wherein a plurality of heating holes are formed in the upper end of the dot-matrix electric heating furnace; each group of sample reactors comprises a plurality of sample reactors which are connected in series, metal samples are placed in cylinders of the sample reactors, air inlet and outlet pipes are arranged on top covers, valves are arranged on the air inlet and outlet pipes of the sample reactors, and the sample reactors are independently arranged in the heating holes respectively; the plurality of gas paths are connected with the plurality of groups of sample reactors in a one-to-one correspondence manner; the multiple gas supply devices are connected with the multiple gas paths in a one-to-one correspondence mode, and each gas supply device supplies different gas sources. Therefore, the system can carry out experiments under various working conditions at the same time, multiple threads can operate at the same time to complete a large number of repeated experiments, different reaction time can be controlled, experiment time is saved, experiment cost is reduced, and the system is suitable for various high-temperature experiments.
Owner:TSINGHUA UNIV +1

Method for evaluating adherence strength of cells by utilizing cell detachment agent

The invention relates to a method for evaluating the adherence strength of cells by utilizing a cell detachment agent. The method is technically characterized in that the adhesive effect between the cells and a substrate is weakened by using the cell detachment agent serving as a common experimental agent in cell biology, the cells are fixed later, the number of the adherent cells of each treatedconcentration gradient treatment group is detected, a detection value of a phosphate buffer solution (PBS) treatment group is used as a standard value and normalization analysis is performed, a curvegraph which takes NA as horizontal coordinates and takes D as vertical coordinates is drawn, and the adhesion strength of the cells is characterized by dilution multiples D50 percent corresponding to1 / 2NA(PBS). Compared with the prior art, the method has the advantages that time consumed in experiments is reduced, experimental steps are simplified, automated batch treatment is easy to realize, and the measuring accuracy and the parallelity of the results are improved.
Owner:北京泰盛生物科技有限公司

Method for measuring solid content of catalytic slurry oil

The invention discloses a method for measuring the solid content of catalytic slurry oil, which comprises the steps of slurry oil heat treatment, solvent dilution, centrifugal treatment, filtration and enrichment, drying and weighing and the like, can accurately measure the solid content of the slurry oil, and can obtain a certain amount of solid fine powder sample for property characterization at the same time. According to the method, the problem of reading errors in calculation of the solid content volume by a traditional centrifugal method is solved, neglect of the ash content in measurement of the coke powder content is avoided, the time for measuring the solid content by a single filtering method is shortened, the measurement of the solid content of the oil slurry is more accurate, stable and rapid, meanwhile, a certain amount of solid content can be obtained for analysis of properties such as particle size and composition. Technical support is provided for investigation of oil slurry solid content and other properties and safe and stable operation monitoring of refinery plant devices.
Owner:PETROCHINA CO LTD

Mammal oocyte quality evaluation method based on optical property detection

The invention provides a mammal oocyte quality evaluation method based on optical property detection. The method comprises the following steps: oocytes are collected from a mammal, and the oocytes donot need any biochemical treatment; a Mueller matrix type full-field OCT system is combined with a Mueller matrix decomposition and transformation technology to represent the polarization characteristics of each biological structure of oocytes; a full-field OCT system is combined with a Fourier analysis technology to characterize backscattering spectrum characteristics of all biological structures of oocytes; and the backscattering intensity characteristics of each biological structure of the oocyte are characterized by analyzing the gray scale distribution characteristics and the frequency spectrum characteristics of the OCT image of the oocyte. The method has the characteristics of no damage, no labeling, high resolution, three-dimensional chromatography, simplicity in operation, shortexperimental time, easiness in implementation and the like, and can be used for effectively evaluating the development quality and development potential of the mammal oocytes.
Owner:SHENYANG NORMAL UNIV

Method for Calculating Dislocation Density of Deformed Crystal Materials Based on Single Diffraction Peaks

The invention discloses a method for calculating dislocation density of a deformed crystal material based on a single diffraction peak. The method comprises the following steps of: utilizing a synchrotron radiation energy scanning X-ray diffraction technology to obtain an experimental intensity distribution curve of diffraction intensity of the deformed crystal material relative to a diffraction vector mode and a reference intensity distribution curve of diffraction intensity of a non-deformed crystal material relative to the diffraction vector mode; introducing a dimensionless variable M, andcalculating a standard intensity distribution curve of a diffraction peak after dislocation density normalization; calculating a specific M value of the experiment intensity distribution curve according to the experiment intensity distribution curve and the standard intensity distribution curve, and recording the specific M value as M'; and calculating the dislocation density of the deformed crystal material according to the full widths at half maximum of the experimental intensity distribution curve, the standard intensity distribution curve and the reference intensity distribution curve. The dislocation density of the deformed crystal material can be obtained by analyzing the intensity distribution curve of the single diffraction peak, and the experiment time is shortened.
Owner:XI AN JIAOTONG UNIV

Method for fast and simple enrichment of trace quantity of animal tissue mitochondrial DNAs

The invention provides a method for fast and simple enrichment of trace quantity of animal tissue mitochondrial DNAs. The method comprises that trace quantity of an animal sample (of which the minimum quantity is 10mg) is subjected to alkaline cracking and nuclear genome DNAs are selectively precipitated; and the precipitated nuclear genome DNAs are subjected to multiple purification processes so that fast and simple enrichment of the mitochondrial DNAs is realized. The method is simple and feasible and has short operation time, a low cost and low equipment requirements. The DNAs enriched by the method can be directly used as reliable templates for follow-up PCR amplification molecule identification. The method can be used for pre-treatment on trace quantity of animal samples in a small identification laboratory and especially is suitable for specie identification, individual analysis and paleontology research. The method is suitable for almost all of trace quantity of animal tissue comprising hard and soft animal tissue.
Owner:ZHEJIANG UNIV

Prediction Method of Clay Consolidation Coefficient Based on Microstructural Parameters

The invention provides a microstructure parameter-based clay consolidation coefficient prediction method, which comprises the steps of: conducting clay consolidation experiments under different pressures, and measuring the void ratio according to conventional geotechnical experiments; calculating the consolidation coefficients of different consolidation experiments; employing a scanning electron microscope technique to obtain a microstructure photo of a corresponding sample section; carrying out granule area and void area segmentation on the clay microstructure photo, and extracting the information of granule unit sum, unit direction, total area, total circumference, and area ratio; analyzing the granules and establishing a main component expression with an accumulative contribution rate of over 95%; and establishing the relationship between the main components and the clay consolidation coefficient. The method provided in the invention links the consolidation coefficient of clay with its microstructure parameters to obtain corresponding consolidation coefficient indexes under different pressures according to the clay void ratio and micro-parameter main components. The method can effectively shorten the experiment time at a civil engineering investigation phase.
Owner:TIANJIN URBAN CONSTR COLLEGE

A high-precision electronic multi-activity isothermal adsorption experimental device

ActiveCN106092812BControl adsorptionControlled Adsorption EnvironmentWeighing by absorbing componentWater circulationData recording
The invention relates to a high-precision electronic multi-activity isothermal-adsorption experimental apparatus. The experimental apparatus consists of an external case and a single-activity weighing unit and is characterized in that the external case comprises an isothermal water cycle temperature control system, adjustable foot pads, a glass door, a level gauge, a data recording system and a control panel; the isothermal water cycle temperature control system consists of a water tank, a temperature control component, an electric heating wire, a water pump, a water-circulation pipeline and a temperature control system; the single-activity weighing unit consists of a shell, high-precision electronic weighing units, a dynamic atmosphere circulator, a working area, a sample cabinet, a water cistern and a weighing bottle; the shell is a rectangular hollow shell, five high-precision electronic weighing units are arranged in the shell, and the sample cabinet and the water cistern are separately placed at an upper half part and a lower half part of the shell. According to the high-precision electronic multi-activity isothermal-adsorption experimental apparatus, an adsorption environment can be effectively controlled indoors, data of a plurality of samples of multiple activities are accurately and simultaneously measured and are continuously recorded under different temperatures, and a continuous sample quality changing process is obtained.
Owner:SOUTHWEST PETROLEUM UNIV

A rapid measurement method for coal caking index and colloidal layer index

A coal caking index and gelatinous layer index rapid measurement method comprises the following steps: collecting spectral data of a calibration sample by using a laser-induced breakdown spectroscopysystem, and selecting spectral lines in two modes: 1, selecting related elements and spectral lines according to the physical background of coal properties; 2, establishing a regression equation amongthe caking index, the gelatinous layer index and the spectral line intensity by using a partial least square method, and selecting a partial spectral line with the lowest relative standard deviationof the regression coefficient; and then, establishing a partial least square calibration model by taking a union set of spectral lines selected by the two modes as input. For a sample to be detected,a laser-induced breakdown spectroscopy system is used for collecting spectral data, and the spectral data is substituted into the calibration model to obtain the caking index and the gelatinous layerindex of the sample. According to the method, the measurement accuracy is improved through a novel spectral line selection means, the measurement speed is obviously higher than that of a national standard method, and online and in-situ measurement can be achieved.
Owner:TSINGHUA UNIV
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