This invention discloses a high-efficiency and energy-saving
distillation separation process for
privet aldehyde, belonging to the field of fragrance preparation and
distillation separation technology. The specific process includes the following steps:
Privet aldehyde crude product is pretreated by alkali washing and
water washing, and then fed into a partition column for
distillation separation; the overhead vapor of the partition column is compressed and heated by an MVR compressor, and then fed into the
reboiler of the partition column as a heat source; the
side stream of the partition column collects the crude
privet aldehyde product, which is then sent to a refining column for final refining to obtain the finished
privet aldehyde product; the operating pressure of the refining column is higher than that of the partition column, and the overhead vapor of the refining column serves as a supplementary heat source for the
reboiler of the partition column; during the distillation
separation process,
nitrogen gas is independently introduced into the partition column and the refining column for protection, and the
nitrogen pressure in each column is 2-5 mmHg higher than the operating pressure of that column. Through the synergistic effect of MVR
heat pump distillation, partition column technology, and
differential pressure heat
coupling, significant energy savings are achieved in the privet aldehyde distillation
separation process.