The invention discloses an agilawood and ant nest fruit mask liquid with pure natural ingredients, a mask and a preparation method of the mask liquid. The mask liquid is prepared from the following raw materials in parts by weight: 30-50 parts of agilawood, 30-50 parts of ant nest fruits, 1-6 parts of saffron crocus, 1-6 parts of lantana camara, 1-6 parts of ginseng, 1-4 parts of orchid grass, 1-6 parts of malay ardisia japonica, 1-4 parts of garden balsam stem, 1-8 parts of angelica sinensis, 1-8 parts of betel nut, 1-4 parts of actinolite, 1-8 parts of musk gumbo, 1-4 parts of radix sophorae flavescentis, 1-8 parts of hongdawen xili (Chinese character), 1-8 parts of fructus cnidii, 1-8 parts of manjia kani (Chinese character), 1-8 parts of gastrodia elata and 0.1-1 part of borneol, wherein the pH value of the mask liquid is 3.5-5.5; and adjustment is carried out through volcanic spring of which the pH is 2.5. The mask liquid disclosed by the invention is capable of protecting the skin, also has the efficiencies of cleaning and sterilizing, and can play a good effect of nourishing the skin through coordination of unique efficacies of the agilawood, the ant nest fruits and special volcanic spring in Indonesia.