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121results about How to "Facilitate phase separation" patented technology

Method for extracting and separating molybdenum (VI) in aqueous solution

The invention discloses a method for extracting and separating molybdenum (VI) in an aqueous solution. The method is mainly characterized in that a non-ionic surface active agent, the molybdenum-containing aqueous solution, a saline solution and deionized water are mixed and stirred evenly, the concentration of the non-ionic surface active agent is 50-300 g/L, the concentration of molybdenum is 1-40 g/L, and the salt concentration is 50-300 g/L; the pH value is adjusted to 1-4, the mixture is subjected to still standing and phase separation after being stirred for 10-60 min at 25-80 DEG C, phase separation is conducted for 10-60 min, an aqueous two-phase system with the upper phase being a non-ionic surface active agent phase loading the molybdenum and the lower phase being an aqueous phase, and the concentration of the molybdenum in the non-ionic surface active agent phase loading the molybdenum is 2-80 g/L; the reextraction temperature is 25-80 DEG C, the time is 10-60 min, phase separation is conducted for 10-60 min, the phase ratio of the non-ionic surface active agent phase loading the molybdenum to an ammonium sulfate aqueous solution is 1 to 5, and the reextraction product is ammonium molybdate. According to the method, the extraction rate is high, good phase separation is achieved, the molybdenum extraction rate reaches 95% or above, and the molybdenum reextraction rate reaches 95% or above.
Owner:YANSHAN UNIV

Rapid method for production of cerium-containing oxide organic colloids

InactiveUS20130192122A1Simple and rapid and low temperature processDispersion stability can be increasedLiquid carbonaceous fuelsIron compoundsOctanoic AcidsEmulsion
Improved methods for producing colloidal dispersions of cerium-containing oxide nanoparticles in substantially non-polar solvents is disclosed. The cerium-containing oxide nanoparticles of an aqueous colloid are transferred to a substantially non-polar liquid comprising one or more amphiphilic materials, one or more low-polarity solvents, and, optionally, one or more glycol ether promoter materials. The transfer is achieved by mixing the aqueous and substantially non-polar materials, forming an emulsion, followed by a phase separation into a remnant polar solution phase and a substantially non-polar organic colloid phase. The organic colloid phase is then collected. The promoter functions to speed the transfer of nanoparticles to the low-polarity phase. The promoter accelerates the phase separation, and also provides improved colloidal stability of the final substantially non-polar colloidal dispersion. The glycol ether promoter reduces the temperature necessary to achieve the phase separation, while providing high extraction yield of nanoparticles into the low-polarity organic phase. In addition, use of particular amphiphilic materials, such as heptanoic acid or octanoic acid, enable efficient extractions at ambient temperatures without the use of a glycol ether promoter.
Owner:CERION

Method for treating chemical nickel plating concentrated waste liquid by solvent extraction method and ion exchange method

The invention discloses a method for treating a chemical nickel plating concentrated waste liquid by a solvent extraction method and an ion exchange method. The method comprises adjusting a chemical nickel plating concentrated waste liquid concentration to 6-7 by NaOH, fully mixing the waste liquid subjected to pH adjustment and an extractant, carrying out standing for two phase layering, separating the two phases to obtain organic and water phases, wherein the water phase is a nickel-free solution and the organic phase is a loading organic phase, fully mixing sulfuric acid and the above organic phase, carrying out standing for two phase layering, separating the two phases to obtain a water phase and an organic phase, wherein the water phase is a nickel sulfate solution and the organic phase is an extractant, treating the nickel-free solution by an alkalescent anion exchange resin column to remove hypophosphite, carrying out cooling to precipitate sodium sulfate crystals, and adding nickel sulfate and hypophosphite into the sodium sulfate crystals to obtain a regenerated chemical nickel plating liquid for direct chemical nickel plating. The method has the advantages of high extraction efficiency, environmental friendliness, simple operation, low cost and high economic value.
Owner:SOUTHEAST UNIV
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