The invention relates to the technical field of batteries, in particular to a negative
electrode material preparation method based on a negative
electrode aged hard carbon material, which comprises the following steps: firstly, crushing and grading an aged hard carbon precursor to obtain particles with a preset particle size; the preparation method comprises the following steps: performing pretreatment such as
acid washing, alkali washing,
water washing and
ethanol washing, mixing a purified precursor with a
coating material in proportion to form a uniform
coating layer, pre-
sintering in a protective
atmosphere, and preliminarily stabilizing a
material structure by controlling parameters such as a heating rate; and carrying out specific surface area detection on the pre-sintered primary product, and dynamically adjusting pre-
sintering process parameters according to the specific surface area detection to ensure that the pore structure of the material reaches the standard. And performing high-temperature
carbonization treatment on the material meeting the standard so as to repair the
carbon layer structure and improve the
conductivity. And finally, performing quality judgment by detecting the first coulombic efficiency of a finished product. According to the invention, the first coulombic efficiency, the specific capacity and the
cycling stability of the regenerated hard carbon material are improved, and the recycling of the aging material is realized.