The invention discloses an in-situ
attenuated total reflection Fourier transform infrared spectrum detection method based on
microwave heating, and belongs to the technical field of spectrum detection and analysis. According to the method, a
design strategy that
microwave heating and an
infrared spectrum
system are arranged separately is adopted, and a high-refractive-index
infrared reflection
crystal is used as a unique
coupling detection area, so that real-time infrared spectrum monitoring of a
reaction system is realized. The detection method disclosed by the invention is particularly suitable for in-situ monitoring of hydrogenation,
cracking and
conversion reaction of an
oxygen-containing or unsaturated
substituent compound on a
furan ring or a
benzene ring, and is compatible with
microwave and catalytic
reaction mechanism research, material interface reaction analysis and spectroscopic characterization of a
biomass derivative conversion process; the method has the advantages of being accurate in
temperature control, high in response speed, high in
signal stability and good in data
repeatability, dynamic spectrum tracking can be conducted on a complex
reaction system, a traditional external heating detection mode is compatible, and the space matching degree and the
time resolution of microwave field in-situ characterization are remarkably improved.