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52results about How to "Reasonable technical route" patented technology

Liquid sulfur collection method for sulfur recovery

The invention discloses a liquid sulphur collecting method suitable for a sulfur recovery device. Process gas of the sulphur recovery device enters a process gas condensate cooler to carry out gas-liquid separation; condensed and separated gas enters the next stage of reaction or condensate cooling system after a liquid sulphur catcher traps the liquid sulphur; the condensed liquid sulphur is collected by a liquid sulphur collector below the process gas condensate cooler; the collecting process is controlled by a process operation module; the collected liquid sulphur is directly delivered to a sealed liquid sulphur middle tank with pressure; the liquid sulphur is fed to a liquid sulphur treatment system after passing through a liquid sulphur degassing pump after gas-liquid secondary separation; and the separate gas is separated from the final stage of process gas condensate cooler and enters a tail gas treatment unit together with the tail gas which is further separated by a tail gas delivery tank. By adopting the technology, arrangement of a sulphur sealing tank, a sulphur sealing tank pond and a liquid sulphur pond is concealed; the technologic process is shortened; the investment on the equipment is reduced; and pollution of the liquid sulphur, the hydrogen sulfide and related treatment technologies on the soil, environment and ground water quality is partially removed.
Owner:SHANDONG SUNWAY PETROCHEMICAL ENGINEERING CO LTD

Rare-earth permanent magnet hydrogen storage device for hydrogen demolishing and hydrogen cyclic utilization and system and method thereof

ActiveCN106001582AStoring evenlyDehydrogenation can be controlledMagnetic materialsRare earthProcess engineering
The invention belongs to the technical field of rare-earth permanent magnet materials and relates to a rare-earth permanent magnet hydrogen storage device for hydrogen demolishing and hydrogen cyclic utilization and a system and method thereof. A rotary hydrogen storage tank body (10) of the device is made of a hydrogen storage alloy material. An output end (6) and an input end (7) which are symmetrical and communicate with each other are arranged on the rotary hydrogen storage tank body (10). The output end (6) and the input end (7) are each internally provided with a filter screen (1). A sealing rotating shaft (2) is arranged at the outer side of each filter screen (1), and the sealing rotating shafts (2) are mounted on a storage tank rotation driving mechanism. An exhaust opening (5) is formed in the output end (6). A spiral piece (9) is arranged inside the rotary hydrogen storage tank body (10). A heating device (3) and a cooling device (4) are arranged at the outer side of the rotary hydrogen storage tank body (10) in a manner that the heating device (3) and the cooling device (4) are close to but not in contact with each other. The rare-earth permanent magnet hydrogen storage device and the system and method thereof are reasonable in process flow and simple in equipment structure and have industrial application value and wide application prospect.
Owner:CENT IRON & STEEL RES INST

Daldinia childiae and application thereof in preparation of bacterium grain wood

The invention discloses Daldinia childiae L2Ma and application thereof in preparation of bacterium grain wood, belonging to the technical field of microorganisms. The strain is collected in China General Microbiological Culture Collection Center; the address is No.3, Yard 1, Beichen West Road, Chaoyang District, Beijing City; and the collection number is CGMCC No:5954. The strain has excellent impregnation capability for a wood-based material, the impregnation time is short, and the impregnation depth is large; beautiful colors and grains can be formed on the surface of the material; and the physical mechanical strength is not influenced. A method for preparing a bacterium grain wood by using the strain comprises the steps of strain activation, expanding propagation and inoculation culture; and the method comprises the following specific steps: inoculating the strain on an activation and expanding propagation culture medium, performing activation and expanding propagation at 22-30 DEG C for 7-15 days, sterilizing the wood-based material, enabling the wood-based material to be sufficiently in contact with the strain subjected to activation and expanding propagation, and culturing at 22-30 DEG C for 6-8 weeks. According to the invention, the method is reasonable in process and simple to operate; and the prepared bacterium grain wood has favorable decoration effect and has no influence on the physical mechanical property of the base material, thereby being beneficial to large-scale production and popularization.
Owner:SOUTHWEST FORESTRY UNIVERSITY

Preparation method and application of polypyrrole/phytic acid/graphene oxide composite anti-corrosion coating

The invention discloses a preparation method and application of a polypyrrole/phytic acid/graphene oxide composite anti-corrosion coating. The preparation method comprises the following steps: systematically adjusting and controlling the concentration and ratio of pyrrole monomer, phytic acid and graphene oxide dispersion liquid, and carrying out direct electro-deposition of the composite coatingmaterial on the surface of stainless steel through the convenient one-step galvanostatic method. The polypyrrole/phytic acid/graphene oxide composite anti-corrosion coating is applied to corrosion protection of stainless steel in an acid environment to solve the problems that an existing conducting polymer anti-corrosion coating has micropores and is poor in adhesive force and does not have high stability. The preparation method is simple and can realize direct, rapid and large-area deposition of the coating material on the surface of stainless steel; and in addition, the coating is dense in structure and stable in anti-corrosion performance, and has excellent application prospect in the stainless steel material used in an oil and gas well and acid soil and a metal bipolar plate of a fuelcell.
Owner:SUZHOU UNIV OF SCI & TECH

Preparation method for separating and purifying silicon dioxide and cerous chlorate from seeing stone waste material

The invention relates to a preparation method of separating and purifying silicon dioxide and cerous chloride from crystal stone wastes, belonging to the field of resource reuse, and is characterized by the following steps: 1) removing impurity: the crystal stone wastes is added with phosphoric acid as an impurity-removing agent and stirred to obtain a mixture of silicon dioxide and cerium oxide; and 2) separation: the mixture is added with concentrated hydrochloric acid as a separation agent, treated by water bath and filtration, the filtrate is evaporated and crystallized to fully precipitate cerous chloride heptahydrate crystals, which is oxidized to obtain cerium oxide crystals; the filter residues are dried at a temperature of <150 DEG C for 1 to 3 hours to obtain silicon dioxide. The preparation method achieves maximum utilization of resources of solid wastes, can transform trash into treasure and obtain phosphate by-products of high economic value and cerous chloride of high purity and high price, and also has advantages of low processing costs, highly pure target composition and significant economic benefits. The purification process follows the idea of clean production, energy saving and reducing emission so as to avoid the problem of environmental pollution.
Owner:INNER MONGOLIA UNIV OF SCI & TECH

Method for obtaining 2-alkyl anthracene through anthracene alkylation and preparing 2-alkyl anthraquinone through catalytic oxidation

The invention relates to the field of preparation of 2-alkyl anthraquinone. The invention specifically discloses a method for obtaining 2-alkyl anthracene through anthracene alkylation and preparing 2-alkyl anthraquinone through catalytic oxidation. The method comprises the following steps: anthracene makes contact with an alkylation reagent for an alkylation reaction, a reaction product containing alkyl anthracene is prepared, and an alkylation reaction solvent is a combination of a solvent A with the dielectric constant being 1-10 at the temperature of 20 DEG C and a solvent B with the dielectric constant being larger than 10 and smaller than or equal to 50 at the temperature of 20 DEG C; the anthracene is separated from the reaction product containing the alkyl anthracene through melt crystallization, and the 2-alkyl anthracene is separated through distillation; the 2-alkyl anthracene is contacted with an oxidizing agent for oxidation reaction. The alkylation combined solvent and the catalyst are adopted, so that the selectivity of the 2-alkyl anthracene is high; the adopted separation method can significantly reduce the separation operation difficulty, and the product purity ishigh; the adopted oxidation system is simple and efficient, and the catalyst is low in cost and easy to recycle.
Owner:CHINA PETROLEUM & CHEM CORP +1

Xylaria venosula fungi and application of the same in preparation of fungi pattern wood

The present invention discloses a strain of Xylaria venosula J22QIU and an application of the Xylaria venosula J22QIU in preparation of fungi pattern wood, and belongs to the technical field of microorganisms. According to the present invention, the strain is preserved in the China General Microbiological Culture Collection Center, the address is Institute of Microbiology, Chinese Academy of Sciences, 3# Court No.1, Beichen West Road, Chaoyang District, Beijing, and the preservation number is CGMCC No:5964; the strain provides excellent dip dyeing ability for the wood base material, the dip dyeing time is short, the dip dyeing depth is high, beautiful color and texture can be formed on the material surface, and the physical and mechanical strength is not affected; the method for preparing the fungi pattern wood by using the strain comprises strain activation and propagation, and fungi inoculation culture, wherein the strain is inoculated on an activation and propagation culture medium, activation and propagation is performed for 10-15 days at a temperature of 22-30 DEG C, the wood base material is sterilized and completely contact the obtained strain, and culture is performed for 4-8 weeks at a temperature of 22-30 DEG C; and the method has characteristics of reasonable process and simple operation, the prepared fungi pattern wood has a good decorative effect, the physical and mechanical property of the substrate is not affected, and the method is suitable for large-scale production and promotion application.
Owner:SOUTHWEST FORESTRY UNIVERSITY

Method for separating 2-alkyl anthracene from anthracene through reaction and preparing 2-alkyl anthraquinone through catalytic oxidation

The invention relates to the field of preparation of 2-alkyl anthraquinone, and particularly discloses a method for preparing 2-alkyl anthraquinone by performing reaction on anthracene, performing separating to obtain 2-alkyl anthracene and performing catalytic oxidation on the 2-alkyl anthracene. The preparation method comprises the following steps: (1) preparing a reaction product containing the2-alkyl anthracene from the anthracene; (2) separating the anthracene from the reaction product containing the alkyl anthracene through melt crystallization and performing distillation seperation toobtain the 2-alkyl anthracene; and (3) under an oxidation condition and in the presence of an oxidation reaction solvent and a catalyst, contacting the 2-alkyl anthracene with an oxidizing agent for an oxidation reaction, wherein the oxidizing agent is tert-butyl hydroperoxide, the catalyst contains a carrier and an active component loaded on the carrier, and the active component is selected fromone or more of VA group elements and transition metals. The method is a green preparation method of the 2-alkyl anthraquinone, the separation method can significantly reduce the separation operation difficulty, and the product yield and purity are high; the developed oxidation system is high in activity, the conversion rate is as high as 96.29%, and the selectivity is 98.67%.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for separating 2-alkyl anthracene from product containing alkyl anthracene and preparing 2-alkyl anthraquinone by adopting catalytic oxidation process

The invention relates to the field of preparation of 2-alkyl anthraquinone, and particularly discloses a method for separating 2-alkyl anthracene from a product containing alkyl anthracene and preparing 2-alkyl anthraquinone by adopting a catalytic oxidation process. The method comprises the following steps: (1) preparing the reaction product containing the alkyl anthracene from anthracene; (2) subjecting the reaction product containing the alkyl anthracene to melt crystallization to separate the anthracene and distillation to separate the 2-alkyl anthracene; (3) under an oxidation condition and in the presence of an oxidation reaction solvent and a catalyst, contacting the 2-alkyl anthracene with an oxidizing agent for an oxidation reaction, wherein the oxidizing agent is hydrogen peroxide, the catalyst contains a carrier and a metal active component loaded on the carrier, and the metal active component is selected from one or more of alkaline earth metals, transition metals and lanthanide metals. According to the method, the separation operation difficulty of the reaction product containing alkyl anthracene can be remarkably reduced, the oxidation system is green and efficient, the conversion rate is as high as 90.12%, and the selectivity is as high as 99.02%.
Owner:CHINA PETROLEUM & CHEM CORP +1

A fungus of the genus Congcha and its application in the preparation of fungi-grained wood

The invention discloses Nectria rigidiuscula J12WU and application thereof in preparation of bacterium grain wood, belonging to the technical field of microorganisms. The strain is collected in China General Microbiological Culture Collection Center; the address is No.3, Yard 1, Beichen West Road, Chaoyang District, Beijing City; and the collection number is CGMCC No:5963. The strain has excellent impregnation capability for a wood-based material, and the impregnation time is short; beautiful colors and grains can be formed on the surface of the material; and the physical mechanical strength is not influenced. A method for preparing a bacterium grain wood by using the strain comprises the steps of strain activation, expanding propagation and inoculation culture; and the method comprises the following specific steps: inoculating the strain on an activation and expanding propagation culture medium for expanding propagation, performing activation and expanding propagation at 22-30 DEG C for 7-15 days, sterilizing the wood-based material, enabling the wood-based material to be sufficiently in contact with the strain subjected to activation and expanding propagation, and culturing at 22-30 DEG C for 1 week or more than 1 week. According to the invention, the method is reasonable in process and simple to operate; and the prepared bacterium grain wood has favorable decoration effect and has no influence on the physical mechanical property of the base material, thereby being beneficial to large-scale production and popularization.
Owner:SOUTHWEST FORESTRY UNIVERSITY

Preparation method for separating and purifying silicon dioxide and cerous chlorate from seeing stone waste material

InactiveCN101343064BMaximum utilization of resourcesHigh economic valueSilicaRare earth metal compoundsWater bathsFiltration
The invention relates to a preparation method of separating and purifying silicon dioxide and cerous chloride from crystal stone wastes, belonging to the field of resource reuse, and is characterized by the following steps: 1) removing impurity: the crystal stone wastes is added with phosphoric acid as an impurity-removing agent and stirred to obtain a mixture of silicon dioxide and cerium oxide;and 2) separation: the mixture is added with concentrated hydrochloric acid as a separation agent, treated by water bath and filtration, the filtrate is evaporated and crystallized to fully precipitate cerous chloride heptahydrate crystals, which is oxidized to obtain cerium oxide crystals; the filter residues are dried at a temperature of <150 DEG C for 1 to 3 hours to obtain silicon dioxide. The preparation method achieves maximum utilization of resources of solid wastes, can transform trash into treasure and obtain phosphate by-products of high economic value and cerous chloride of high purity and high price, and also has advantages of low processing costs, highly pure target composition and significant economic benefits. The purification process follows the idea of clean production, energy saving and reducing emission so as to avoid the problem of environmental pollution.
Owner:INNER MONGOLIA UNIV OF SCI & TECH
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