The invention relates to a treatment process for organic silica mud. The treatment process comprises the following steps of: disilane hydrolysis, copper chloride leaching, pressing and backwashing, copper replacement, silicon slag roasting and tail gas treatment. According to the treatment process, hydrogen chloride gas generated by hydrolysis is effectively utilized, so that hydrogen chloride gas realizes zero discharge; a stirring reaction kettle is adopted for stirring and leaching, so that a leaching rate of copper is as high as 99%, copper content of sponge copper is 70% or higher, and iron chloride content is 30% or higher, and therefore, the economical value is increased; hydrolysis residues are roasted through a rotary kiln, so that silicon oxide content is greater than 98%, and therefore, the whole process route is free of wastewater and waste residue discharge, the waste gas is only carbon dioxide, harms on environment are reduced to be the lowest, the products are metal copper and silicon powder, and the economical value is high. Throughout the process, zero discharge of wastewater and waste residues is realized, so that the environmental benefits are remarkable; hydrolysis and leaching are performed under normal pressure at a temperature lower than 90 DEG C, requirements on the material and strength of equipment are not high, and a roasting temperature of the rotary kiln ranges from 500 DEG C to 850 DEG C; and moreover, silicon powder does not contain corrosive hydrogen chloride, and requirements on the material of the rotary kiln are not high.