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58results about How to "Low concentration temperature" patented technology

Method for equivalent dialysis through directly adopting membrane treatment

The invention discloses a method for equivalent dialysis through directly adopting membrane treatment. The method comprises the following steps: S1: storing the filtrate of Acesulfame in a filtrate storage tank, which is taken as a stock solution; S2: adopting a hot water circulation system to increase the temperature of the stock solution in the filtrate storage tank, setting membrane ingress pressure and membrane egress pressure simultaneously, and through transmission and concentration of an organic membrane, allowing a clear membrane liquid to flow to a clear membrane liquid storage tank for recycle; S3: when the clear membrane liquid flux in the clear membrane liquid storage tank drops to 20-60L / PM, using the same amount of water to dialyze, and dialyzing the Acesulfame out and recycling; S4: discharging the residual liquid in a circulation tank to a liquid waste disposing center directly so as to have liquid waste disposal; and S5: washing and detecting membrane equipment. The method disclosed by the invention adopts the hot water circulation system for heating and omits the concentration treating and recycling process, so that the energy consumption is saved, the concentration temperature is low, the material is difficult to break down, the purposes of liquid decoloration and organic salt treatment are realized, the product obtained can be recycled directly, and the equipment has a simple structure and a low treatment cost.
Owner:ANHUI WEIDUO FOOD INGREDIENTS CO LTD

Tobacco extracting solution concentrating technology

The invention relates to a tobacco extracting solution concentrating technology, and belongs to the technical field of the tobacco extracting solution concentration. The technology comprises the following steps of: after performing primary purification on a tobacco water extracting solution, micro-filtering, performing positive permeation concentration on micro-filtering permeate, and recycling adiluted draw solution formed by the positive permeation concentration through using an electrodialysis or salt sun-drying mode. The technology has the advantages of low operating pressure, and high safety; low concentration temperature, and small temperature rising during a concentrating process, without heat-exchanging and cooling; and small membrane pollution, simple and convenient washing, andlow washing frequency. At the same time, the technology is high in concentration degree, and concentration of the concentrated tobacco extract can reach 60%. In a tobacco extracting solution concentrating working procedure of reconstituted tobaccos by a papermaking process, evaporation and concentration can be completely replaced. In the concentrating process, loss of materials, nicotine and volatile components is small, energy consumption is low, and popularization and application are easy.
Owner:CHINA TOBACCO YUNAN NEW MATERIAL

Continuous triple-effect falling-film concentration and vacuum crystallization system and method in potassium nitrate production through double-decomposition method

The invention relates to a continuous triple-effect falling-film concentration and vacuum crystallization system and method in potassium nitrate production through a double-decomposition method. The continuous triple-effect falling-film concentration and vacuum crystallization system comprises a mixing tank, a concentration preheater, a backflow triple-effect concentration device, an ammonium chloride crystallizer, a thickener and a centrifuge, which are sequentially connected. The continuous triple-effect falling-film concentration and vacuum crystallization method comprises the following steps: adding potassium nitrate mother liquid and ammonium nitrate into the mixing tank for uniformly mixing, subsequently conveying to the mixture to the concentration preheater for preheating, feeding into the backflow triple-effect concentration device for concentration, feeding into the ammonium chloride crystallizer for crystallization after concentration, further sequentially feeding into the thickener and the centrifuge, separating a solid ammonium chloride product from the centrifuge, and returning the separated solution as a circulating mother liquid to a potassium nitrate production process through the double-decomposition method for circulation. Under the condition that the number of concentration equipment is not increased, the continuous triple-effect falling-film concentration and vacuum crystallization system and method in potassium nitrate production through double-decomposition method, provided by the invention, can achieve large-scale and continuous production, and the production efficiency is improved.
Owner:KINGENTA ECOLOGICAL ENG GRP

Method for purifying high purity ammonium rhenate from liquid containing ammonium rhenate

InactiveCN103172122ALow concentration temperatureReduce the loss of rheniumRhenium compoundsIonHydrogen peroxide
The invention relates to a method for purifying high purity ammonium rhenate from a liquid containing ammonium rhenate. The method comprises the following steps of: a, concentrating the liquid containing ammonium rhenate and adding a hydrogen dioxide liquid into the concentrated liquid; stirring and removing surface foam of the mixed liquid and filtering; b, cooling the filtrate obtained in the step a, then, filtering and taking out crystallized substances and performing centrifugal dewatering treatment, and placing the crystallized substances again to an oven to dry to prepare the high purity ammonium rhenate; and c, mixing the filtrate obtained by the step b with the liquid containing ammonium rhenate and repeating the step a and the step b to prepare a high purity ammonium rhenate product. According to the invention, the concentration temperature is reduced, the loss of rhenium entrained in vapor volatilization is reduced, and the rhenium recovery rate is improved. Compared with the prior art, the method is free from ammonia or ammonia water, and environment-friendly in the production process, and meanwhile, low valence metal ions which are difficult to remove are converted into high valence metal ions which are easy to remove by the hydrogen peroxide liquid. The low valence rhenate is converted into the high valence rhenate, so that the purity of the ammonium rhenate product is ensured.
Owner:JIANGXI COPPER

Method for extracting total alkaloid in stem bark and leaves of nauclea offcinalis

The invention relates to a method for extracting total alkaloid in stem bark and leaves of nauclea offcinalis, which comprises the steps of (1) performing filtering extraction by utilizing acid water solution of alcohol, (2) preparing total alkaloid concentrated liquid, (3) preparing total alkaloid dry powder or dry extraction, and (4) measuring total alkaloid content. The method for extracting the total alkaloid in the stem bark and the leaves of the nauclea offcinalis has the advantages of (1) reducing extraction temperature and concentration temperature, reducing heated time of the extraction, saving energy consumption, improving leaching efficiency, leaching ratio and leaching amount of active components of the alkaloid, avoiding or reducing damage or deterioration of the alkaloid with poor stability, and being capable of effectively obtaining the total alkaloid extraction or the total alkaloid dry powder of the nauclea offcinalis; (2) reducing preparation procedures and loss of the total alkaloid; (3) enabling the density of the total alkaloid obtained by the acid water solution of the alcohol to be improved by one third and enabling the types of active alkaloid to be increased by over one time; and (4) providing a simple measurement method for measuring the total alkali in the extraction of the nauclea offcinalis, and selecting wavelength scope of measurement of the total alkaloid.
Owner:海南制药厂有限公司

Preparation process of formaldehyde alcoholic solution for polymethoxy dimethyl ether production

InactiveCN107652169ARealize the controllability of the degree of aggregationReduce decompositionOrganic chemistryOrganic compound preparationHigh concentrationDecomposition
Aiming at the problem that the acquisition of formaldehyde with low water content decides the feasibility of DMMn synthesis and directly influences the product synthesis conversion rate, aldehyde canbe concentrated to 85 percent through a vacuum concentration system, the water content in the formaldehyde is dewatered to 0.5 to 3 percent in a dewatering tower, methyl alcohol with a low boiling point is condensed with the formaldehyde, the polymerization degree controllability of the formaldehyde in a liquid phase is realized, and a formaldehyde alcoholic solution with a polymerization degree nbeing equal to 3 to 10 is obtained, so that the most suitable reaction raw material-the formaldehyde alcoholic solution with a low water content is found for polymethoxy dimethyl ether synthesis. Theformaldehyde vacuum concentration system is combined with a stripping tower principle, so that the formaldehyde alcoholic solution with the low water content is prepared, the water content in the reaction system is reduced, the product decomposition is avoided, the DMMn synthesis conversation rate is efficiently improved, meanwhile, the risk of polymerization during a high-concentration formaldehyde concentration process is avoided due to the introduction of the formaldehyde, the concentration temperature is reduced, the generation of formic acid is reduced, and an advantageous effect is achieved on separating a follow-up polymethoxy dimethyl ether product.
Owner:无锡赫利邦化工科技有限公司

Method and device for continuously concentrating glyoxylic acid

The invention relates to a method and a device for continuously concentrating glyoxylic acid. A glyoxylic acid solution is concentrated by adopting a method of continuously adding a stock solution and extracting a concentrated solution. The method comprises the following steps: a switch-on vacuum debugging process, an early feeding concentration stabilizing process, a continuous feeding and extraction adjusting process, a normal continuous concentration process, a distillate intermittent transfer process and a concentration ending halt process. The device comprises an evaporator, a heater, a demister, a condenser, a receiving tank, a buffer tank, a scrubber tank, a high vacuum unit, a stock solution container, a concentrated solution container, a distillate container, an extracting pump, a distillate delivery pump, a stock solution feeding flow meter, a concentrated solution extraction flow meter and the like. The method and the device can realize continuous production of concentrated glyoxylic acid, the concentration efficiency is high, the equipment capacity can be obviously improved, the materials are short in heating time and low in temperature, the product is high in quality, high in yield and low in energy consumption, the service life of glassed steel equipment can be prolonged, and the labor intensity of workers is reduced.
Owner:HUBEI HONGYUAN PHARMA

Preparation method of semen armeniacae amarae and thunberg fritillary bulb oral liquid for relieving cough and resolving phlegm

ActiveCN103393923AAvoid the problem of loss of active ingredientsFast evaporationPharmaceutical delivery mechanismRespiratory disorderAdditive ingredientSemen
The invention discloses a preparation method of a semen armeniacae amarae and thunberg fritillary bulb oral liquid for relieving cough and resolving phlegm. The preparation method is characterized by comprising the following steps of: jointly decocting sweet root bark of white mulberry, fried semen armeniacae amarae, thunberg fritillary bulb and liquorice to reserve an extracting liquid, obtaining clear paste through three-effect decompression concentration, sinking the clear paste by water and centrifugalizing and reserving a clear liquid; independently decocting sweet polygala tenuifolia, independently storing the extracting liquid, and combining the extracting liquid with the clear liquid; adjusting the pH twice when the volume is fixed and before filling; sterilizing for 40 minutes at 103 DEG C and filling. The preparation method disclosed by the invention has the beneficial effects that 1, the polygala tenuifolia is independently decocted to avoid the problem that the polygala tenuifolia is bubbled to lead to loss of effective components when the extracting liquid is concentrated; 2, three-effect decompression concentration is adopted, so that not only can the concentration temperature be low, the moisture is quick to evaporate, the concentration time is short and the energy consumption is reduced, but also the effective components of the product are effectively prevented from being damaged by high temperature foremost; 3, the pH value is adjusted twice to ensure the stability of product quality; 4, insulative overnight aging at 70-80 DEG C can be used for effectively preventing the liquid medicine from rancidity; 5, the oral liquid is sterilized for 40 minutes at 103 DEG C, and the temperature is moderate, so that the effective components of the liquid medicine are effectively protected.
Owner:BEIJING SHOUER PHARMA FACTORY

Deerskin glue and production process thereof

The invention provides deerskin glue. According to the formula, the glue contains the following raw materials: 90%-95% of cultured deerskin serving as the main raw material, 0.1%-0.5% of added or not-added flavor ingredients, 3%-10% of rock candy, 3%-10% of rice wine, 0.1%-0.5% of soybean oil. A production process of the deerskin glue comprises the following steps: cleaning; cutting; sterilizing at a high temperature; cooking at a high temperature; adding the flavor ingredients and cooking; filtering the glue solution; adding trypsin and hydrolyzing; concentrating; adding the flavor ingredientextract; continuing to concentrate the glue solution; heating and stirring; cooling; naturally drying cut glue pieces; and finally packing. The deerskin glue and the production process thereof, whichare provided by the invention, have the advantages that the flavor ingredients are added at a specific temperature and time to enhance the mouthfeel of the deerskin glue; the processes of dehairing and impurity removing are increased before processing and the sterilization process is increased to improve the product purity; the trypsin is added and hydrolysis is carried out to ensure that the product is more transparent and the protein molecules are more uniform; and the concentration temperature is reduced and the glue is prevented from overcooking to ensure that the production quality is increased and the product quality is finally improved.
Owner:苏州红冠庄国药股份有限公司

Low-nicotine paper-making process reconstituted tobacco and preparation method and application thereof

The invention provides low-nicotine paper-making process reconstituted tobacco and a preparation method and application thereof. The preparation method of the low-nicotine paper-making process reconstituted tobacco comprises the following steps of: mixing tobacco fibers, wood pulp fibers and filler, then adding water, and performing heating extraction; centrifuging the leaching solution to obtaina tobacco extracting solution; pulping the solid matter according to a papermaking process, and forming to obtain a substrate; concentrating the tobacco extracting solution under reduced pressure to obtain water paste; adding ammonia water into the water paste, performing uniform stirring, mixing with an organic solvent, and performing extracting; separating the solution after extraction to obtainan organic phase and a water phase; mixing the water phase with an ethanol solution, performing uniform stirring, and performing concentrating under reduced pressure to obtain a coating solution; andcoating a substrate with the coating solution, and performing drying to obtain the low-nicotine paper-making process reconstituted tobacco. The low-nicotine paper-making method reconstituted tobaccoprepared through adoption of the method is low in nicotine content, can replace part of tobacco raw materials to be added into traditional or novel cigarettes, can effectively reduce tar, nicotine andother harmful substances in smoke, and reduces harm to the human body.
Owner:贵州黄果树金叶科技有限公司

Method for treating high-salt organic wastewater

The invention discloses a method for treating high-salt organic wastewater. According to the method, concentrated extracted salt is combined with biochemical treatment, and inorganic matters and organic matters are removed step by step, so that up-to-standard emission of the wastewater is realized. The method comprises the specific steps: adding a dehydrating agent into the wastewater which is heated to be 40 DEG C to 80 DEG C until the wastewater is saturated; cooling the saturated wastewater to be -5 DEG C to 5 DEG C; separating out mixed salt crystals; centrifuging and separating crystal separation wastewater to obtain the mixed salt crystals and a concentrated mother solution containing high organic matter content; washing the mixed salt crystals to obtain dehydrating agent hydrate crystals; evaporating a washing mother solution and carrying out concentration and salt extraction; heating the dehydrating agent hydrate crystals to be 95 DEG C to 150 DEG C; carrying out crystal transformation dehydration to obtain a regenerated dehydrating agent and condensed water; carrying out 3 to 5 times of the concentration and salt extraction on the concentrated mother solution containing the high organic matter content to obtain a salt-containing concentrated mother solution containing the high organic matter content; diluting the salt-containing concentrated mother solution containing the high organic matter content with the condensed water and carrying out the biochemical treatment to obtain up-to-standard wastewater. The method disclosed by the invention has moderate process conditions; the dehydrating agent can be circularly utilized; the energy consumption is low, the treatment cost is low and the emission standards of the wastewater are met.
Owner:自然资源部天津海水淡化与综合利用研究所

Preparation method of high-purity ethyl 4-chloro-3-hydroxybutyrate

The invention belongs to the field of drug preparation and particularly relates to a preparation method of high-purity ethyl 4-chloro-3-hydroxybutyrate. Ethyl 4-chloroacetoacetate is used as a raw material to carry out reacting with ethanol as a solvent and sodium borohydride as a reducing agent; the reacted liquid is dewatered, neutralizing with glacial acetic acid is performed until neutrality,filtering is performed to remove salts, vacuum concentration is performed, a solvent is added to carry out dissolving, washing with water is carried out to remove salts, concentrating is performed, and vacuum distillation is performed to obtain the high-purity ethyl 4-chloro-3-hydroxybutyrate. The ethyl 4-chloro-3-hydroxybutyrate is an intermediate of oxiracetam, a drug to treat senile dementia; as registration of new medicines in China requires research on impurities of pharmaceutical intermediates, namely research on impurity whereabouts and influence of impurities on products, the existingpreparation method of ethyl 4-chloro-3-hydroxybutyrate causes many impurities and low purity, only 84.9%; the preparation method has a reasonable ratio of materials, has good simplicity and low cost,and enables the purity to reach 99.5% and above and the yield to reach 90% and above, and the prepared samples may meet the requirements for medicine registration.
Owner:SHANDONG XINHUA PHARMA CO LTD

Preparation process of blueberry concentrated juice with high content of anthocyanin

The invention provides a preparation process of blueberry concentrated juice with high content of anthocyanin. According to the preparation process provided by the invention, pectase is adopted for performing enzymolysis on blueberry pulp, chitosan is adopted as a clarifying agent for obtaining clear blueberry juice, a decompression concentration process is adopted for preparing the blueberry concentrated juice, and microwave sterilization is adopted for sterilizing the blueberry concentrated juice. The preparation process comprises the following steps of: selecting blueberry fruits in vaccinium ashei gardenblue species; extracting the blueberry juice, and adding the pectase to perform the enzymolysis on the blueberry pulp; clarifying the blueberry juice, and adding the chitosan as the clarifying agent for obtaining the clear blueberry juice; concentrating the blueberry juice, and adopting the decompression concentration to obtain the blueberry concentrated juice; and performing sterile filling on the blueberry juice, and adopting the microwave sterilization to sterilize the blueberry concentrated juice, wherein the content of soluble solids in the blueberry concentrated juice is 60%-75%, and the content of the anthocyanin is 1.925g / L-3.384g / L. The preparation process provided by the invention can not only effectively prevent the loss of the anthocyanin in the blueberry concentrated juice, but also shorten the concentration time, control the production cost of the preparation process and effectively protect color, luster, fragrance and other sensory qualities of the blueberry juice.
Owner:ANHUI AGRICULTURAL UNIVERSITY
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