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43results about How to "Prevent spheroidization" patented technology

Production method of multilayer ceramic electronic device

By a production method for producing a multilayer ceramic electronic device including dielectric layers and internal electrode layers comprising the steps of forming a green sheet to be said dielectric layer after firing, forming a pre-fired electrode layer to be said internal electrode layer after firing in a predetermined pattern on said green sheet by using a conductive material paste, forming a green chip by successively stacking said green sheets and said pre-fired electrode layers, and firing said green chip: wherein the conductive material paste for forming said pre-fired electrode layer is composed at least of conductive material particles, a first common material composed of ceramic powder and a second common material composed of ceramic powder having a larger average particle diameter than that of said first common material; an average particle diameter of said first common material is 1/20 to ½ of an average particle diameter of said conductive material particles; and the average particle diameter of said second common material is 1/10 to ½ of an average thickness of said internal electrode layers after firing; a multilayer ceramic electronic device, such as a multilayer ceramic capacitor, wherein arising of cracks is effectively prevented, having a low short-circuit defect rate, a low voltage resistance defect rate and high capacitance is produced.
Owner:TDK CORPARATION

Spheroidizing method of nodular cast iron

InactiveCN103433471ASolve the problem of moving up after meltingAdjust the amount added at any timeMelt-holding vesselsRare-earth elementFerrosilicon
The invention relates to a spheroidizing method for producing nodular cast iron. According to the spheroidizing method, a melted whole rare earth ferrosilicon magnesium alloy spheroidizing agent containing not more than 20% of Mg, not more than 70% of Si and not more than 3% of RE is put into a reaction chamber built in the spheroidizing ladle and carrying out an inter-ladle pouring process, wherein the addition amount of the spheroidizing agent is only 0.4%-0.8% of the weight of the melted iron to be processed; the spheroidizing reaction time is controlled accurately, the temperature of the melted iron in the spheroidizing and pouring processes is less reduced, absorption rates of Mg, RE and Si after spheroidization are high, the addition amount of the spheroidizing agent is only one third of that of the traditional process, and thus the spheroidizing cost can be reduced by 50%; the production environment in the production and use processes of the spheroidizing agent is improved, and the product quality is improved. Compared with the traditional rare earth ferrosilicon magnesium alloy spheroidizing agent with rare earth element RE of 2-8%, the use amount of the rare-earth element RE is reduced by 50-75% by using the spheroidizing method for producing nodular cast iron for spheroidization.
Owner:TIANJIN WANLU LTD CO OF SCI & TECH +2

Spheroidizing method

InactiveCN102690985APrevent the problem of moving up after meltingAvoid lostMelt-holding vesselsRare-earth elementBrick
The invention relates to a spheroidizing method for producing spheroidal graphite cast iron, and the method comprises the following steps: injecting rare earth magnesium silicon iron inoculant alloy fluid containing less than or equal to 20% of Mg, less than or equal to 65% of Si and less than or equal to 3% of RE into a square steel pipe for solidifying and cooling; fixing the whole rare earth magnesium silicon iron inoculant of the outer lining square steel pipe in a spheroidizing bag by using refractory bricks and wedge-type chocks at the bottom of the spheroidizing bag covered, and then carrying out spheroidizing by utilizing a bag injecting method. The time for controlling spheroidizing is accurate, the molten iron cooling is less in the spheroidizing and casting process, the absorption rate of Mg, RE and Si after the spheroidizing is high, degradated spheroidization is avoided 15min after spheroidizing, the environment for producing and using a spheroidizing agent is improved, the production cost is remarkably reduced and the quality of the product is improved. Compared with the traditional magnesium silicon iron spheroidizing agent with the rare-earth element RE content of 2-8%, the spheroidizing method can be used for reducing the use amount of the rare-earth element RE by 50-75%.
Owner:TIANJIN WANLU LTD CO OF SCI & TECH +2

Lithium battery spherical positive electrode material with lithium fluoride coating layer and preparation method

The invention relates to the technical field of lithium ion batteries, in particular to a lithium battery spherical positive electrode material with a lithium fluoride coating layer and a preparation method. The preparation method comprises the following steps of stirring a mixed solution formed by nickel sulfate, cobalt sulfate and manganese sulfate until the complete reaction is completed, and washing and drying solids to obtain NCM precursor powder; heating and stirring the NCM precursor powder, lithium carbonate and magnesium lithium silicate, pre-sintering at 200-300 DEG C, sintering in a fluidized bed, back-blowing the powder by hydrogen fluoride and argon, and filtering to obtain the lithium battery spherical positive electrode material with the lithium fluoride coating layer. According to the present invention, the problems of poor spheroidization control and transition metal element dissolution of the lithium battery positive electrode material in the prior art are solved. The lithium battery spherical positive electrode material with the lithium fluoride coating layer prepared by the preparation method has better spheroidized morphology, and the lithium fluoride serves as the coating layer, so that the cycle performance of the battery can be effectively improved.
Owner:CHENDU NEW KELI CHEM SCI CO LTD

Balling processing method of nodular cast iron

ActiveCN103874771ASolve the problem of moving up after meltingAdjust the amount added at any timeFerrosiliconRare earth
Disclosed is a balling processing method of nodular cast iron. A left vertical baffle plate (2) and a right vertical baffle plate (3) are laid at the bottom part of a balling processing bag (1). A semicircular reaction chamber upper cover plate (4) is horizontally laid on the top parts of the left vertical baffle plate (2) and the right vertical baffle plate (3). A vertical surface of the reaction chamber is provided with one or more reaction chamber material feed ports (5). The upper end of one reaction chamber material feed ports (5) is provided with a pressure reducing groove (6). The upper end of the pressure reducing groove (6) is at the same level as the semicircular reaction chamber upper cover plate (4). The finished balling processing bag is dried and then used for balling processing. The steps of balling processing are as follows: the required no-lining steel pipe overall rare earth magnesium ferrosilicon nodulizer (8) or low silicon or silicon-free nodulizer is put into the reaction chamber of the balling processing bag (1); the Ferrosilicon inoculants is put into the reaction chamber of the balling processing bag (1) and stacked at the material feed ports (5); melted iron flows into the balling processing bag (1) to carry out the balling reaction; and when the balling reaction is completed, the dross is removed, and the melted iron is coated by compound inoculants.
Owner:杭州合大铸造有限公司

Pure magnesium spheroidizing technology of lost foam ductile cast iron

ActiveCN106636870APrevent defects such as cold insulation wrinkle skinAvoid stickingSulfurFerrosilicon
The invention discloses a pure magnesium spheroidizing technology of lost foam ductile cast iron. The pure magnesium spheroidizing technology comprises the steps that a spheroidizing agent is placed into a lip-pour ladle reaction chamber, a cover of the reaction chamber is closed, and a conventional nucleating agent, ferrosilicon, is added into a lip-pour ladle; after molten iron in a heat-insulated furnace is subjected to deslagging, molten iron is added into the lip-pour ladle, and the temperature of molten iron is controlled to be 1520 DEG C to 1560 DEG C; then, the lip-pour ladle is overturned, and molten iron and the spheroidizing agent react for 60 s to 70 s; and pouring is carried out while stream inoculation is achieved, wherein the addition amount of the stream nucleating agent is 0.08% to 0.15% of the weight of molten iron; the spheroidizing agent is a mixture of pure magnesium ingots and calcium chloride; and the weight ratio of molten iron to the pure magnesium ingots to calcium chloride to ferrosilicon is 1000 to (1.4 to 2.0) to (0.2 to 0.5) to (4 to 8). According to the pure magnesium spheroidizing technology of lost foam ductile cast iron, the spheroidizing problem of high-sulfur high-silicon molten iron can be effectively solved, the spheroidizing grade is high, a required matrix structure can be obtained, the problems that the spheroidizing effect is poor, the quality of castings is not stable, and the rejection rate is high are solved, the technology does not require lip-pour ladle nucleating, the procedures can be decreased, and the labor intensity is reduced.
Owner:桃江新兴管件有限责任公司

Manufacturing method of ultra-large-section low-temperature high-toughness ferrite spheroidal graphite iron casting

The invention discloses a manufacturing method of an ultra-large-section low-temperature high-toughness ferrite spheroidal graphite iron casting. The spheroidal graphite iron casting is more than 50 tons in weight, is 400mm or more in wall thickness, and is prepared from the following components: 3.6 to 3.7 percent of C, 0.9 to 1.0 percent of Si<original>, 1.9 to 2.0 percent of Si<final>, less than or equal to 0.1 percent of Mn, less than or equal to 0.03 percent of P, less than or equal to 0.01 percent of S, 0.03 to 0.08 percent of Mg, 0.01 to 0.02 percent of RE, 0.6 to 0.8 percent of Ni and0.003 to 0.005 percent of Sb. During manufacturing, the technical measures of ''high-temperature pure base iron melt, water-cooled metal mold, cold iron, spheroidizing agent 5800, compound strengthening inoculation, alloying and low-temperature box beating'' are adopted, so that the prepared ultra-large-section low-temperature high-toughness ferrite spheroidal graphite iron casting can meet the quality standard of a spheroidal graphite iron casting of which the license number is QT400-18, and can meet the technical requirements of ultra-large-section spheroidal graphite iron castings applied to wind power, nuclear power and the like.
Owner:ZHENGZHOU RES INST OF MECHANICAL ENG CO LTD

Method for eliminating casting shrinkage cavity defect by using petroleum coke carburant

The invention discloses a method for eliminating a casting shrinkage cavity defect by using a petroleum coke carburant. The method comprises the following steps that a first batch of carbon steel scrap is added into the petroleum coke carburant for being mechanically stirred uniformly, and then added into the middle-lower part of a medium-frequency smelting furnace; a second batch of carbon steel scrap is added into the middle-upper part of the medium-frequency smelting furnace, and heating is carried out until the carbon steel scrap is completely molten into molten steel; after the molten steel is completely melted down, magnetic stirring is carried out, and after carbon components in the furnace are uniform, sampling is carried out for spectrum sample component analysis; and the components are adjusted after sampling, and various elements are added according to requirements. The petroleum coke is added at the initial stage of the smelting furnace, so that the dissolving speed of the petroleum coke can be guaranteed, graphite carbon is effectively prevented from forming graphite floating in a casting, spheroidizing recession of graphite is effectively prevented, graphitizing expansion in a matrix is fully exerted, shrinkage porosity and shrinkage cavity defects of a hot spot part in the casting are effectively prevented, raw material waste is reduced, and the production cost is reduced.
Owner:临清市金光机械制造有限公司

V-method casting process for nodular cast iron casting

The invention belongs to the technical field of spheroidal graphite cast iron casting processing, particularly relates to a V-method casting process for a spheroidal graphite cast iron casting, and provides the following scheme aiming at the problem that the shrinkage porosity tendency of a shrinkage cavity is relatively large when a thick and large-section casting is subjected to casting processing: S1, material selection; s2, core making and modeling; s3, smelting and pouring; s4, opening the box and taking the package; s5, fine processing; according to the method, the thick and large-section ductile iron casting is cast through V-method negative pressure, during casting of the casting, by controlling the sand mold, the compactness, the number of sprues, the number of dead heads and the number of chilling blocks and selecting the proper pouring temperature, the graphitization expansion force of the casting in the solidification casting process can effectively avoid shrinkage cavity and shrinkage porosity defects, and the casting quality is improved. The negative pressure pipe is pressurized at the thick and large part of the casting, so that the cooling speed is accelerated to prevent spheroidizing recession, and meanwhile, the graphitization expansion force is reduced, so that the phenomena of shrinkage cavities and shrinkage porosity of the casting are greatly reduced.
Owner:山东宇信铸业有限公司

High Strength Gas Cylinder Head and Its Production Technology

The invention discloses a high-strength fuel gas cylinder cover and a production technology thereof. The production technology comprises the following steps that step (1), furnace burdening is prepared, low-S nodular cast iron pig iron and pure carbon waste steel are selected, a medium-frequency induction electric furnace is adopted for smelting, wherein the smelting temperature is controlled to be 1500-1550 DEG C, argon is blown into molten iron, the blowing depth is 20-40% at the depth of the furnace, the blowing time is 5-8 minutes, and then the molten iron is discharged; step (2), spheroidizing and first inoculation treatment are carried out, and a pour over method is adopted; step (3), pouring and a second inoculation treatment are carried out, the pouring temperature of the molten iron is not lower than 1400 DEG C, the second inoculation is carried out by adopting a second nucleating agent during the pouring, and the second inoculation is a metal-stream instantaneous inoculation;step (4), after the pouring is completed, the waste heat of a casting is used for carrying out heat treatment until the room temperature is reached. The technology is reasonable in design, the heat treatment process of the technology is omitted, so that the production cost is reduced, environmental pollution is reduced; and the mechanical property of the fuel gas cylinder cover obtained by the technology is improved correspondingly.
Owner:宁波力古机械制造有限公司

Electron beam selective melting forming method for pure tungsten metal parts

The invention discloses a method for electron beam selective melting and forming of pure tungsten metal parts. In the method, a three-dimensional model of the pure tungsten metal part is firstly established by software and sliced ​​to obtain slice data, and then according to the slice data of the three-dimensional model Electron beams are used to melt tungsten powder into selected areas to obtain pure tungsten metal parts. The invention uses electron beams to melt tungsten powder into shape, which improves the energy of the heat source, ensures complete melting of tungsten powder with high melting point, avoids spheroidization during the melting process of tungsten powder, and separates the forming bottom plate and tungsten powder before scanning the melting selection area. The high-temperature preheating treatment of the powder reduces the temperature gradient during the forming process of pure tungsten metal parts, slows down the cooling rate of the micro-melt pool, avoids the spheroidization of tungsten powder droplets caused by rapid cooling, and reduces the spheroidization of pure tungsten metal parts. Cracking greatly improves the forming quality of pure tungsten metal parts and increases the density of pure tungsten metal parts.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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