The invention provides a preparation method of a
spectral analysis standard sample, and the preparation method comprises the steps of sieving the steel class, confirming the element and the initial value of the steel class, preparing the standard sample, testing the uniformity, analyzing the constant value and confirming the standard value, identifying, packaging and making
certificate, scrutinizing the stability, and contrasting the standard steel. The invention has the advantages that the analyzing speed can be improved by using the standard steel, the duration of heat is saved, and the benefit is quite impressive. The problem of on-line analysis of the five harmful elements can be solved, and the
smelting is monitored in real time, to stop the situation of
scrap steel or steel class changing caused by the over limited five harmful elements happening. A piece of standard steel can control the major elements and the residual elements, monitor the five harmful elements and the acid-soluble
aluminium in the
liquid steel in real time, without the analyzing time increased. The method can be popularized, and the
spectral analysis controlling standard steel is necessary for the prior steel-making corporation. By using
continuous casting semi finished
metal to develop the
spectral analysis controlling standard steel, the process is simplified, and the developing cost is reduced.