The invention discloses a preparation method of a 2xxx series aluminum
alloy transmission
electron microscope sample, and belongs to the technical field of transmission
electron microscope sample preparation. The method comprises the following steps: selecting a double-spraying liquid formed by mixing
nitric acid and
methanol with a certain concentration according to a volume ratio of 1:3, controlling the double-spraying
voltage to be 18-22V and the double-spraying temperature to be 5-10 DEG C, and
thinning a sample on a double-spraying electrolytic
thinning instrument. Due to the selection ofproper double-spraying liquid, double-spraying
voltage and double-spraying temperature, the surface of a sample is bright, the
potential difference between a second phase and a base body is reduced,
sieve pores are effectively avoided, uniform
thinning is achieved, the thinning effect can be achieved within 10-20 s, the efficiency is greatly improved, no stress or heat is input in the thinning process, and the invention provides a rapid and reliable
sample preparation method. By utilizing the method, the transmission sample without
sieve pores and with a larger thin area can be conveniently and simply prepared, and the method has important reference significance for preparing the
metal material transmission sample containing the thick second phase.