The invention relates to a
potassium tetracyanopalladate synthesis method, which comprises: S1,
acid dissolution oxidation: carrying out a
dissolution reaction on a
metal palladium powder raw material to generate a
palladium nitrate-containing aqueous phase solution; s2,
precipitation: carrying out
precipitation reaction on the aqueous phase solution containing
palladium nitrate prepared in the step S1 to generate a palladium
cyanide solid intermediate; s3, washing: washing the palladium
cyanide solid intermediate generated in the step S2 to remove
impurity ions; and S4, reactive
crystallization: reacting the palladium
cyanide intermediate purified in the step S3 with
potassium cyanide, and crystallizing to obtain a
potassium tetracyanopalladate product. According to the method, synthesis of potassium tetracyanopalladate can be achieved through a simple and rapid method, and the obtained product is high in purity, uniform in
crystal form, good in
solubility and suitable for application scenes with high requirements for plating quality in the industries of semiconductors, PCBs,
aerospace and the like; the potassium tetracyanopalladate is used as a key
raw material of a palladium plating process and is used in the field with high requirements on material performance and appearance.