The invention discloses a section
scanning electron microscope sample suitable for a
metal micro guide wire and a preparation method of the section
scanning electron microscope sample. Belongs to the technical field of material microscopic analysis. The preparation method comprises the following steps: fixing the
metal micro
guide wires by constructing conductive rigid clamps, filling conductive adhesives among the conductive rigid clamps, and arranging a plurality of
metal micro
guide wires among the conductive adhesives; the metal micro
guide wires are exposed out of the two ends of the conductive rigid clamp by 0.5-1.5 cm; and the
diameter of the metal micro guide wire is 45-500 microns. The invention provides a preparation scheme of a metal microwire section
scanning electron microscope sample, which is simple to operate and does not need any large equipment, and provides a rigid and conductive
support system capable of performing directional electrolytic
polishing for a soft and fine metal wire on the premise of not introducing external stress, not polluting the sample and not using expensive equipment. Therefore, the scanning
electron microscope samples are efficiently prepared in batches at low cost, and the high-resolution characterization requirement is met.