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68results about How to "Stable at room temperature" patented technology

Unsymmetrical fragrant diamine containing fluorine, preparation and application in synthesizing polyimide thereof

The present invention relates to fluorine-containing asymmetric aromatic diamine, a preparation method and an application thereof in the synthesis of polyimide. The compound has a constitutional formula as shown in the right. The preparation method comprises the following steps: (1) 2, 6-dimethyl phenol, paranitrobensoyl chloride and alchlor have catalytic reaction in an organic solvent to prepare (4'-hydroxy-3', 5'-dimethyl benzene)-(4-nitrophenyl) ketone; (2) the (4'-hydroxy-3', 5'-dimethyl benzene)-(4-nitrophenyl) ketone reacts with 2-chlorine-5-nitro trifluorotoluene with alkaline, to prepare (3', 5'-dimethyl-4'-(4''-nitro-2''-trifluoromethyl phenoxy) benzene)-(4-nitrophenyl) ketone; (3) the prepared product in the second step is reduced by reducing agent with organic solvents and catalysts; thus the fluorine-containing asymmetric aromatic diamine can be prepared. The fluorine-containing asymmetric aromatic diamine can be used for preparing fluorine-containing polyimide. The fluorine-containing asymmetric aromatic diamine prepared in the method has high purity and can keep stable at the room temperature; the polyimide made of the fluorine-containing asymmetric aromatic diamine has excellent solubility, film forming capability, optical transparency, mechanical properties and heat resistance.
Owner:DONGHUA UNIV

Mesoporous titanium dioxide material and preparation method thereof

The invention relates to the field of a mesoporous material, and in particular relates to a mesoporous titanium dioxide material and a preparation method thereof. According to the mesoporous titanium dioxide material disclosed by the invention, an aperture is 10-30nm, a specific surface area is 63-235m<2>/g and a pore volume is 0.55-1.02cm<3>/g. Compared to a current mesoporous titanium dioxide material, the mesoporous titanium dioxide material disclosed by the invention greatly improves specific surface area, aperture and pore volume; the preparation method comprises the following steps: preparing titanium peroxide acid sol through titanic acid and hydrogen peroxide, forming an self-assembling system through titanium oxide acid sol and a surfactant, and drying and baking the self-assembling system to obtain the mesoporous titanium dioxide material; the method is simple and easy to implement; moreover, the entire preparation process is free from other organic chelating agents or inorganic additives and mineral acids; the preparation system is a pure water system which is independent from any other non-polar or weak-polar solvents; and in addition, the titanium peroxide acid sol prepared is relatively stable at room temperature, and control process is relatively simple.
Owner:NORTHEASTERN UNIV

Polycondensation type single-component silicon rubber capable of being vulcanized at room temperature and under heating condition, and preparation method thereof

ActiveCN103265814AFast vulcanizationShortened deep vulcanization cycleRubber materialPolymer science
The invention discloses polycondensation type single-component silicon rubber capable of being vulcanized at room temperature and under a heating condition, and belongs to the field of silicon rubber materials. The polycondensation type single-component silicon rubber is prepared from the following raw materials: a reactive basic polymer, a filler, a crosslinking agent, a coupling agent, a catalyst and an inorganic compound with crystal water. A preparation method of the polycondensation type single-component silicon rubber comprises the following steps of: (1) uniformly stirring the reactive basic polymer, the dry filler and the inorganic compound with the crystal water under a moisture-insulating condition to obtain a mixture; and (2) adding the crosslinking agent, the coupling agent and the catalyst into the mixture, and stirring and mixing uniformly under the moisture-insulating condition to obtain the polycondensation type single-component silicon rubber. The polycondensation type single-component silicon rubber can be stored in a rubber pipe at room temperature for not less than half a year and is stored at room temperature very stably; and after being extruded out of the rubber pipe, the rubber material can be dried superficially at room temperature within half an hour, can be completely vulcanized for 7 days and can be vulcanized deeply and quickly within several hours under a proper heating condition, so that the deep vulcanization cycle of the rubber material is effectively shortened.
Owner:XIAMEN JINTAIXIANG NEW TECH

Control method and device for air conditioner compressor and air conditioner

The invention relates to the technical field of intelligent control, and discloses a control method for an air conditioner compressor. The control method comprises the following steps that a first correction temperature is obtained according to the first actual temperature of an inner coil pipe and an amplitude reduction correction value; when the first correction temperature is larger than the first preset temperature, the compressor is controlled to operate at a first frequency reduction speed in a frequency reduction mode; a second correction temperature is obtained according to the second actual temperature of the inner coil pipe and the amplitude reduction correction value; a second temperature difference is acquired; and when the second temperature difference is smaller than or equal to the first set temperature difference, the compressor is controlled to operate at a second frequency reduction speed in a frequency reduction mode. In the frequency reduction operation stage of the compressor, the temperature rise amount within the set detection interval duration is used as a switching parameter of fast frequency and slow reduction, the lag degree between the temperature of the inner coil pipe and the frequency rise of the compressor is reduced, and the phenomenon of dead halt caused by too fast reduction of the frequency of the compressor is avoided; On the basis, the actual temperature of the inner coil pipe can be subjected to amplitude reduction correction, and the stability of the compressor is improved. The invention further discloses a control device and the air conditioner.
Owner:CHONGQING HAIER AIR CONDITIONER CO LTD +3

Vertical monomolecular film field effect transistor based on two-dimensional laminated heterostructure and preparation method of vertical monomolecular film field effect transistor

The invention discloses a vertical monomolecular film field effect transistor based on a two-dimensional laminated heterostructure and a preparation method of the vertical monomolecular film field effect transistor, and belongs to the field of new materials and molecular field effect transistors. The vertical monomolecular film field effect transistor is composed of the two-dimensional material template layer, the ultra-flat metal electrode, a two-dimensional material insulating support layer, a self-assembled monomolecular film, a two-dimensional material drain terminal electrode, an insulating two-dimensional material dielectric layer and a conductive two-dimensional material gate electrode layer. According to the invention, a novel two-dimensional material is adopted to replace the gridand dielectric layer materials in a traditional field effect transistor, a two-dimensional material insulating layer is introduced to accurately control the atomic-scale thickness of the electrode spacing, and the two-dimensional material thin layer is introduced to improve the flatness of the metal electrode, so that the device achieves the atomic-scale flatness and controllable atomic layer thickness; the vertical molecular field effect transistor which has room temperature stability, is regulated and controlled by the solid-state grid and is provided with the ultra-flat metal electrode isrealized, and the stability of the device and the possibility of large-scale integration are greatly improved.
Owner:NANKAI UNIV
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