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30 results about "Dendrite (metal)" patented technology

A dendrite in metallurgy is a characteristic tree-like structure of crystals growing as molten metal solidifies, the shape produced by faster growth along energetically favourable crystallographic directions. This dendritic growth has large consequences in regard to material properties.

Rare earth metal electrolysis system and electrolysis furnace thereof

The invention discloses a rare earth metal electrolysis system and an electrolysis furnace thereof, and relates to the technical field of metallurgy, the rare earth metal electrolysis system is characterized by comprising a potential data acquisition and preprocessing module, a dendritic crystal feature extraction and quantification module, a dendritic crystal identification and intelligent determination module and an inverse pulse control and dynamic regulation module, in the electrolysis process, potential distribution original data of the surface of a rare earth metal cathode are detected and collected in real time, the obtained original data are preprocessed, and a preprocessed potential data set is established based on a time sequence. According to the method, intelligent, real-time and accurate inhibition of dendritic crystals in the rare earth metal electrolysis process is achieved, short circuit, splashing and electrode ablation are effectively prevented, the compactness and purity of metal deposition are improved, the current efficiency is remarkably improved, and compared with a traditional scheme, the method has the advantages of being high in real-time performance, good in inhibition effect, small in interference and high in adaptability, and the method is suitable for popularization and application. And efficient and safe preparation of the rare earth metal is ensured.
Owner:GANZHOU CHENXIN METAL MATERIALS CO LTD

Smelting and casting method of high-toughness regenerated aluminum alloy

PendingCN121911836AProcess efficiency improvementDie castingDendrite (metal)
The invention relates to the technical field of metal casting, and discloses a smelting and casting method of a high-toughness regenerated aluminum alloy, which comprises the following steps: measuring the iron content of a regenerated aluminum melt, regulating and controlling the manganese-iron ratio, heating the melt to 750-790 DEG C, and carrying out overheating treatment to eliminate a hereditary core; cooling to 630-645 DEG C, applying a mechanical shear flow field with the average shear rate not lower than 60s <-1 > in the interval, stripping a diffusion boundary layer on the surface of the iron-rich phase crystal nucleus by utilizing fluid drag force, breaking dendritic crystals, and separating out in a polyhedral or spherical manner; according to the method, through active intervention of a critical shear flow field, the problem of needle-like growth of an iron-rich phase caused by solute diffusion blocking in a traditional technology is solved, in-situ generation of the harmless iron-rich phase in the high-iron-content secondary aluminum is achieved, the obdurability of a die casting is improved, and dependence on the purity of raw materials is reduced.
Owner:HUNAN QIANYUAN ALUMINUM CO LTD

A carbon carrier material with sodium dendrite growth alleviation, rich in microporous and closed pore structure, and a preparation method and application thereof

The application discloses a carbon carrier material for relieving sodium dendrite growth, rich in micropores and closed pore structure, and a preparation method and application thereof, and belongs to the technical field of low-dimensional material energy storage devices. The preparation method comprises the following steps: SO1, cross-linking reaction of a phenol source, a cross-linking catalyst and a formaldehyde solution; SO2, obtaining an impurity-containing sample through a high-temperature carbonization reaction; and SO3, adding the impurity-containing sample into a solvent for soaking, suction filtration, washing and drying to obtain the carbon carrier material. The carbon carrier material prepared by the application is uniformly distributed, the selection and pore size of the pores are adjustable, can effectively provide rich sodium-philic sites for inducing uniform deposition of sodium, and can inhibit the dendrite growth of a sodium metal battery in a cycle process; the pores serve as three-dimensional Na + Transmission channels are beneficial to forming a good ion migration path, reducing the current density of a local material, reducing the possibility of forming dendrites, and improving the safety and service life of the energy storage device.
Owner:GUANGDONG UNIV OF TECH

A grid mapping method for pool dynamics and phase-field method dendrite growth calculation

The application discloses a grid mapping method for finite element method or finite volume method and phase field method dendrite growth calculation. The application relates to the technical field of welding simulation. Specifically comprises the following steps: step 1, obtaining the field variable distribution in the numerical simulation calculation of the finite element method or the finite volume method welding process; step 2, exporting the coordinates and field variable data of the nodes with the temperature greater than the metal melting point; step 3, performing triangular partitioning on the melting area according to the node coordinates; step 4, drawing the Voronoi diagram of the melting area according to the circumcenters of the Delaunay triangles; step 5, setting the phase field method nodes; step 6, sequentially processing the units in the Voronoi diagram, taking the base point of the unit and the base point directly connected with the base point as known points, and obtaining the field variable value of the phase field method nodes by the interpolation method; and step 7, using the obtained field variable value for the calculation of the phase field method grain growth.
Owner:SHENZHEN AMBER DIGITAL TECHNOLOGY CO LTD

A method for inhibiting dendrite growth on a zinc foil surface

This invention provides a zinc foil surface treatment method for inhibiting dendrite growth, comprising: immersing a zinc foil with ultrasonically cleaned surface in an acidic mixture to obtain a zinc foil with a preferred zinc (002) crystal facet under acid etching; immersing the zinc foil with the preferred zinc (002) crystal facet in a mercaptosilane coupling agent solution, and through hydrolysis, forming a nanostructured zinc-silane composite layer on the zinc foil surface; and drying the zinc foil with the zinc-silane composite layer to obtain a zinc foil that can inhibit dendrite growth. The zinc foil surface treatment method for inhibiting dendrite growth described in this invention can generate a zinc-silane composite layer and zinc with (002) crystal facet orientation on the zinc foil surface. This composite layer has a strong zinc ion adsorption capacity, which can improve ion kinetics, promote uniform zinc plating and peeling, and the preferred (002) crystal facet can induce parallel growth of zinc metal and resist electrolyte corrosion, thereby effectively inhibiting zinc dendrites and stabilizing the electrode / electrolyte interface.
Owner:HEBEI UNIV OF TECH

Preparation method of dendrite-free gel electrolyte and application thereof

The application discloses a preparation method of dendrite-free gel electrolyte and application thereof, and comprises the following steps: synthesizing a porphyrin-based covalent organic framework (PPCOF); preparing a gel precursor solution; and preparing an in-situ polymerized PMMA-based gel electrolyte. The electrolyte has the characteristics of simple preparation method, cheap and easily available raw materials, good electrode interface contact (in-situ polymerization), and the like, and can solve the problems of poor PMMA-based GPE electrode contact, low lithium ion transference number and easy growth of lithium dendrites, thereby providing guidance for the development of dendrite-free solid-state lithium metal batteries.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

A method for preparing carbide microspheres

The application provides a preparation method of metal carbide microspheres, and belongs to the technical field of micro-nano materials. The method comprises the following steps: alloy powder smelting, alloy powder preparation, alloy powder screening, a metal matrix corrosion process, a cleaning process and a screening process, so that a metal carbide micro-nano spherical material is obtained. The metal carbide microspheres can be applied in the fields including but not limited to nuclear materials, energy materials and metal matrix composites. The size of the metal carbide microspheres prepared by the application can be customized in the range of 10-300 um through screening, the average thickness of metal carbide dendrites is 1-20 nm, the average dendrite spacing of the carbide is 1-5 um, and the composition of the metal carbide microspheres can be controlled by alloy composition.
Owner:CHINA MASCH INST OF ADVANCED MATERIALS (ZHENGZHOU) CO LTD

A method of laser powder bed fusion forming of a directional columnar grain structure alloy

PendingCN122644604ATransient heat transferGrain structure
The present application belongs to the technical field of metal additive manufacturing and solidification structure regulation, and particularly relates to a laser powder bed fusion forming method of a directional columnar grain structure alloy. The present application adopts a flat-top beam or a point-ring beam as a forming laser beam, inputs a single-channel three-dimensional transient heat transfer solidification model, obtains a molten pool width, a molten pool depth, a temperature gradient, a solidification rate and a columnar grain-equiaxed grain transition determination result, screens laser power and scanning speed according to the molten pool morphology with a width-depth ratio W / D>3; sets a scanning interval according to the deviation area of the molten pool side temperature gradient vector relative to the preset columnar grain growth direction, so that the overlapping area of adjacent melt channels covers different orientation dendrites or grains on the side; sets the powder layer thickness according to the sensitive area of the columnar grain-equiaxed grain transition at different heights, so that the remelting of the subsequent layer molten pool eliminates the mixed crystals, equiaxed crystals or non-target oriented grains on the top of the previous layer molten pool, and a columnar grain structure metal alloy component is obtained through continuous directional growth across the melt channel and across the layer.
Owner:SHANGHAI UNIV

A conductive dendritic composite gel, its preparation method and application

ActiveCN119591906BSensorsDiagnostic recording/measuringDendrite (metal)Nanotechnology
This invention discloses a conductive dendritic composite gel, its preparation method, and its applications. The invention uses a hydrogel as a matrix, leveraging the hydrophilicity of the hydrogel framework to attract tin ions. Furthermore, by in-situ deposition of metal dendrites within the gel, a highly efficient conductive pathway is constructed. The conductive dendritic composite gel of this invention achieves simultaneous improvement in both mechanical and electrical properties. In addition, the sensor prepared based on this conductive dendritic composite gel exhibits high sensitivity and a wide detection range, effectively monitoring and identifying changes in limbs, demonstrating broad application potential in the field of wearable devices.
Owner:ZHEJIANG UNIV OF TECH

Yb and Tb co-doped alloy brazing filler metal, preparation method and brazing process

The invention relates to the technical field of brazing, and discloses Yb and Tb co-doped alloy brazing filler metal, a preparation method and a brazing process. The Yb and Tb co-doped alloy brazing filler metal comprises, by mass, 12%-13% of chromium, 3%-4% of boron, 3%-4% of silicon, 4%-5% of iron, 0.5%-2% of terbium, 0.5%-1.5% of ytterbium and the balance nickel. Yb and Tb co-doping effectively inhibits growth of dendrites, rare earth elements are easily enriched at the grain boundary to form a fine isometric crystal structure, the prepared Yb and Tb co-doped alloy brazing filler metal brazed diamond is smaller in thermal damage degree, the brazed surface is smooth and free of accumulation, and the phenomena of wrinkles and holes are reduced to a great extent. The rare earth co-doping is beneficial to improving the wettability of the brazing filler metal, the brazing filler metal and the diamond are subjected to violent chemical metallurgy, the interface bonding strength of the brazing filler metal and the diamond is improved, and therefore the machining performance of a diamond tool is improved.
Owner:ANHUI POLYTECHNIC UNIV

Dendritic-free anodes and current collectors for lithium metal and lithium ion batteries

The disclosed concept relates to lithium-ion and lithium-metal batteries including methods of preparing a multi-component alloy (MCA) system having a body-centered cubic (bcc) crystal structure as a negative electrode and current collector, where the lithium-ion or lithium-metal battery is dendritic-free throughout the charging and discharging process of the battery. The MCA system includes an alloy composition of (i) 40 at% iron, 40 at% aluminum or gallium, and 20 at% magnesium, or (ii) 10 at% iron, 40 at% aluminum or gallium, and 50 at% magnesium, or (iii) 50 at% iron, 40 at% aluminum or gallium, and 10 at% magnesium.
Owner:UNIV OF PITTSBURGH OF THE COMMONWEALTH SYST OF HIGHER EDUCATION

Electrolyte for inhibiting growth of zinc dendrites and application thereof

The invention relates to the technical field of energy storage batteries, and particularly discloses an electrolyte for inhibiting zinc dendrite growth and application thereof. The electrolyte consists of electrolyte zinc salt, sodium lactate and water, and is beneficial to inhibiting Zn dendritic crystals and reducing the reaction rate of hydrogen precipitation. Besides, lactic acid anions (SC-) are more easily combined with water, so that a solvation shell structure of Zn < 2 + > is destroyed, deposition of Zn < 2 + > is more uniform, side reactions are reduced, and the zinc metal electrode can stably circulate for more than 500 hours under the condition of 5 mA cm <-2 >. Growth of zinc dendrites can be remarkably inhibited, the service life of the zinc metal negative electrode is prolonged, and the method has the advantages of being simple in preparation process, low in cost and good in application prospect.
Owner:HUBEI UNIV OF AUTOMOTIVE TECH

Method for calculating stress on nitride dendrite in forced convection during solidification of molten steel

The application provides a method for calculating stress of nitride dendrites under forced convection in a steel liquid solidification process, and relates to the technical field of metal solidification. The composition of the steel grade and the involved thermodynamic and kinetic parameters and complex F-H boundary conditions are collected. The free boundary condition is added to the right side along the x direction velocity, and the stress growth model of Fe-C-M-N quaternary alloy steel in the flow field is established by coupling D2Q9 and cellular automaton model. Finally, the visual processing module is used to analyze the shape, size and flow field distribution of the nitride dendrites during solidification. The application optimizes the solidification technology, predicts the stress analysis of the nitride dendrites under forced convection, and provides theoretical guidance for improving the quality of the casting blank.
Owner:NORTHEASTERN UNIV CHINA

Automatic control method and system for precious metal purification process

The invention relates to the technical field of precious metal purification, and discloses an automatic control method and system for a precious metal purification process. The method comprises the following steps: constructing a quadrant acoustic monitoring coordinate system to obtain a real-time acoustic energy vector, establishing an acoustic energy entropy increase coordinate system, defining an entropy increase polygon, and executing a multi-stage judgment mechanism to output an entropy increase directivity report; starting an optical information conversion mechanism to generate an optical shadow map, converting the optical shadow map into a resistance value distribution map by using a photoresistor array, and executing a gating gain modulation rule to output a local suppression field instruction; and formulating a directional intervention strategy based on the report, constructing a resonance cooperative shielding mechanism, and realizing dendritic crystal removal through a reverse current pulse and sine cleaning pulse sequence. According to the method, the problems of local dendritic crystal risk perception lag and extensive intervention in electrolytic refining are solved, self-organization growth of dendritic crystals is effectively blocked through acousto-optic fusion monitoring and grading synergistic inhibition, and the product purity and the process stability are remarkably improved.
Owner:SHENZHEN BOYUAN PRECIOUS METAL TECH CO LTD

Continuous high-phosphorus electroless nickel plating method capable of reducing crystallization of plating solution

The present application provides a continuous high-phosphorus electroless nickel plating method capable of reducing the crystallization of the plating solution, comprising the following steps: preparing a plating solution containing nickel sulfate as the main salt, sodium hypophosphite as the reducing agent, sodium citrate as the complexing agent, a buffer, and a crystallization inhibitor according to a predetermined concentration ratio, wherein the crystallization inhibitor is one or more of a composite of an organic polyphosphonate and nano-titanium dioxide, a nitrogen-containing heterocyclic compound, or a polymer having a comb-like structure; controlling the plating temperature, the pH value of the plating solution, and the flow rate of the plating solution within a preset range, and performing continuous plating operations. By adding a crystallization inhibitor to the components of the plating solution, the crystallization inhibitor can form a complex with metal ions such as Ni²⁺ in the plating solution and be uniformly dispersed, regulating the release rate of nickel ions and avoiding local crystallization; these crystallization inhibitors can also provide a three-dimensional barrier effect, reducing the formation of dendrites and abnormal grain growth, thereby achieving the effect of reducing the crystallization of the plating solution and improving the stability and production efficiency of the plating solution.
Owner:SHENGZHEN KINHU ELECTROPLATING CO LTD

A metallurgical process for reducing the point segregation of GCr15SiMn bearing steel ingot

The application discloses a metallurgical process for reducing point segregation in GCr15SiMn bearing steel ingot, and the obtained ingot has high cleanliness, and meanwhile, the ingot has a composite inclusion with MgO-Al2O3 oxide as a core and MnS as a peripheral wrapping. The ingot cleanliness requires that the oxygen content in the steel is controlled to be 6-10 ppm, and the titanium content is less than or equal to 25 ppm. The composite inclusion has a core oxide with a size of 0.1-2 microns, and a peripheral wrapping MnS inclusion, and the total size is controlled to be less than 5 microns, and the number density is greater than or equal to 10 per mm 2 . The composite inclusion is spontaneously formed in the solidification process of the molten steel and serves as a nucleation core of early austenite, thereby inhibiting the enrichment of solute elements such as C and Si between the solidification front dendrites, and achieving the purpose of reducing the point segregation of the ingot. The EAF-LF-VD-VC process route is adopted, and the methods such as strictly controlling the end composition of the electric furnace tapping, the Al content in the whole process, the composition of the refining slag and the double vacuum process are adopted to realize the purpose.
Owner:UNIV OF SCI & TECH BEIJING

Intelligent method for rapidly measuring dendritic crystal thickness and lamellar spacing in metal material

The invention discloses an intelligent method for rapidly measuring dendritic crystal thickness and lamellar spacing in a metal material, and the method comprises the steps: carrying out the preprocessing of a neodymium iron boron rapid hardening sheet, obtaining a flat and smooth cross section, collecting a BSE image through a scanning electron microscope, and marking the dendritic crystal thickness and dendritic crystal lamellas, and obtaining a training data set; an image segmentation network U-Net is built, training is carried out by using the training set, evaluation is carried out by combining the verification set, and a feature recognition extraction model is obtained; based on the structural characteristics of dendritic crystal lamellas, a measurement algorithm of the dendritic crystal thickness and the lamellar spacing is constructed by combining various methods; and acquiring a back scattering electron image of a sample to be measured, inputting the back scattering electron image into the feature recognition extraction model to obtain a binarization segmentation result, and outputting a quantization result of the dendritic crystal thickness and the lamellar spacing through a constructed measurement algorithm. According to the method, machine learning, image processing and mathematical statistics technologies are combined, rapid characterization of the thickness, the spacing and the distribution of the branch wafer layer in the metal material is realized, and the method has the characteristics of accuracy, automation and rapidness.
Owner:NCS TESTING TECHNOLOGY CO LTD +1

High corrosion-resistant high-aluminum zinc-aluminum-magnesium-silicon plated steel sheet and method for manufacturing the same

ActiveCN116904898BHot-dipping/immersion processesDendrite (metal)Corrosion
The present application relates to a kind of high corrosion resistance high-aluminum zinc-aluminum magnesium silicon coating steel plate and its manufacturing method, in coating, in the multi-component phase of aluminum-zinc dendrite gap, according to the total area occupied by aluminum-zinc dendrite gap: MgZn2 intermetallic compound accounts for 10%~20%, Mg2Si intermetallic compound accounts for 2%~5%, Zn-Al-Mg ternary eutectic structure accounts for more than 60%.The present application aims to improve the surface and edge corrosion resistance of high-aluminum zinc-aluminum magnesium silicon coating steel plate.By component optimization and process parameter setting, form reasonable coating organization and form, further improve the corrosion resistance of coating.
Owner:ANGANG STEEL CO LTD

Yttrium-treated H13 die steel and preparation method thereof

The present invention belongs to the technical field of metal materials and specifically relates to an yttrium-treated H13 die steel and a preparation method thereof. The yttrium-treated H13 die steel is characterized by comprising the following components, calculated by mass fraction: C: 0.30-0.40%, Si: 0.90-1.10%, Mn: 0.30-0.50%, P < 0.010%, S ≤ 0.050%, Cr: 4.50-6.50%, Mo: 1.20-1.50%, V: 0.80-1.20%, N ≤ 0.010%, Y: 0.006×([%C]+[%N])-0.042×([%C]+[%N])%, with the remainder being Fe and unavoidable impurities. The inclusion type in the yttrium-treated H13 die steel of the present invention is Y2O3, the inclusions and primary carbides are small in size, and the primary carbides are spheroidized from large-sized long strips, fishbone shapes or large blocks to small-sized blocks or granules. The secondary dendrite spacing is reduced from 50 μm to 23 μm, the equiaxed crystal ratio is increased from 0 to about 25%, and the structure is significantly refined.
Owner:SUZHOU UNIV

Corrosion and impact resistant alloy material and processing thereof

PendingCN122446086AProduction lineMolten bath
The application relates to the technical field of alloy materials, in particular to a corrosion-resistant and impact-resistant alloy material and a processing technology thereof. The Y-La-Ce ternary rare earth is used for synergistic modification, alloy bath deep deoxidization and desulfurization and high-efficiency purification of grain boundary impurities are realized, and the segregation of harmful elements such as S, P and O at the grain boundary is significantly reduced. The application also adopts a whole-process process synergistic regulation and control of high-temperature rolling, grading aging and low-temperature stress relief. The high-temperature rolling can crush the as-cast dendrite, eliminate the loose shrinkage and realize the densification of the structure. The grading aging can accurately control the size and distribution of the nano precipitated phase, balance the strength and toughness and stabilize the grain boundary structure. The low-temperature stress relief annealing can completely release the residual stress generated in the rolling and aging processes, avoid the cracking in subsequent processing and service deformation, guarantee the size stability and structure uniformity of the material, has strong process compatibility, can be directly adapted to the existing metallurgical production line, realizes the stable mass production of large-size plates and bars, and is high in production efficiency and controllable in cost.
Owner:JIANGXI HAOTAI METALLURGICAL TECH

Dendrite-free anodes and current collectors for lithium metal batteries and lithium-ion batteries

The disclosed concept relates to lithium-ion and lithium metal batteries comprising methods of preparing multi-component alloy (MCA) systems with body-centered cubic (bcc) crystal structures as anodes and current collectors, wherein the lithium-ion or lithium metal battery is dendrite free throughout the charge and discharge processes of the battery. The MCA systems include the following alloy compositions: (i) 40 atom % iron, 40 atom % aluminum or gallium, and 20 atom % magnesium, or (ii) 10 atom % iron, 40 atom % aluminum or gallium, and 50 atom % magnesium, or (iii) 50 atom % iron, 40 atom % aluminum or gallium, and 10 atom % magnesium.
Owner:UNIV OF PITTSBURGH OF THE COMMONWEALTH SYST OF HIGHER EDUCATION

Nano lanthanum oxide modified Inconel 625 nickel-based superalloy and preparation method thereof

PendingCN121250164ACarbideDendrite (metal)
The invention discloses a nano lanthanum oxide modified Inconel 625 nickel-based superalloy and a preparation method thereof, and belongs to the technical field of metal additive manufacturing and superalloy materials.La2O3 particles with the particle size being 30-50 nm and Inconel 625 alloy powder with the particle size being 53-105 [mu] m are evenly dispersed through a ball-milling powder mixing technology, and then the nano lanthanum oxide modified Inconel 625 nickel-based superalloy is prepared through laser directional energy deposition forming; wherein the addition amount of La2O3 particles is 0.3 wt.%-0.9 wt.%, and the addition of a proper amount of La2O3 can promote grain refinement of a gamma-Ni matrix in the solidification process, relieve segregation of Nb / Mo among dendritic crystals and remarkably reduce formation of Laves phases and MC carbides, so that a microscopic structure is more uniform, the tensile strength and the ductility are both superior to those of a control sample without addition of La2O3, and synergistic improvement of strength and toughness is achieved. The method has the advantages of being small in addition amount, simple in process and remarkable in performance improvement, and a new technical approach is provided for structure regulation and performance optimization of the nickel-based high-temperature alloy in the field of additive manufacturing.
Owner:JILIN UNIVERSITY

System and method for forming directional crystal microstructure

PendingCN122319048AScan lineCrystal structure
3D-printed metal objects with large-size cubic crystal structures are produced by controlling the infill distance and molten pool depth. A molten pool is moved within a first powder layer along a first scan pattern to create a first patterned layer. The scan pattern has parallel scan lines spaced apart by an infill distance along an infill direction perpendicular to the scan lines. As the molten pool cools, dendrites grow in their dendrite growth direction. This infill distance promotes dendrite growth in directions orthogonal to the scan lines and suppresses dendrite growth in directions with a directional component opposite to the infill direction. A second patterned layer is created by moving the molten pool within a powder layer on top of the first patterned layer. The pool depth suppresses dendrite growth in the first patterned layer at an angle of less than 45 degrees relative to the top surface of the molten pool.
Owner:HONEYCOMB IND LTD

Quantitative analysis method for columnar crystal spacing of neodymium iron boron rapid hardening sheet

The invention discloses a neodymium-iron-boron rapid hardening sheet columnar crystal spacing quantitative analysis method which comprises the following steps: S1, sample preparation: cutting a neodymium-iron-boron rapid hardening sheet along the thickness direction to obtain a cross section in the thickness direction, and grinding and polishing the cross section to obtain a sample to be detected; s2, image acquisition and processing: using a BSE detector to acquire backscattered electron images of the sample cross section and splicing the backscattered electron images to obtain a panoramic view containing thickness; performing binarization processing on the panoramic view, and identifying a neodymium-rich phase at the grain boundary of the columnar crystal to obtain a binarization image; and S3, calculating the spacing: measuring the dendritic crystal spacing on the binarized image by using a straight line method, and solving the average value of the dendritic crystal spacing of each straight line, namely the columnar crystal spacing of the neodymium iron boron rapid hardening sheet. According to the method, the whole process of mechanical polishing, electron microscope imaging and image analysis is integrated, the problems of time consumption, low resolution and large artificial error of a traditional metallographic method for preparing a sample are solved, and rapid, objective and high-precision quantitative analysis is realized.
Owner:NCS TESTING TECHNOLOGY CO LTD

A method for determining dendrite channel permeability

The present invention belongs to the technical field of metal alloy casting, and specifically relates to a method for determining the permeability of dendrite channels. The present invention includes the steps of: corroding the surface of the alloy, performing a polishing process to obtain a low-magnification tissue image with a clear dendrite interface outline, and using a two-dimensional imager to obtain a high-definition low-magnification tissue image of the metal; measuring the primary and secondary dendrite arm spacings and the segregation area ratio by image processing software, extracting the dendrite outline by image processing software, and calculating the fractal dimension of the dendrite outline morphology according to the box counting method; and calculating the permeability of the columnar crystal region, the columnar crystal to equiaxed crystal transition region (CET), and the dendrite channel in the equiaxed crystal region. The permeability of the dendrite channel can quantitatively predict the flow resistance of the liquid phase between dendrites during the solidification process of the metal, thereby achieving control of the liquid phase flow rate and flow direction during the solidification process. This provides guidance for regulating the three-dimensional density of the actual solidification structure of the metal and thereby finely controlling segregation.
Owner:WESTERN METAL MATERIAL

Apparatus for anti-dendritic electrolytic deposition

PendingCN120603990ACellsPhotography auxillary processesElectrolysisDendrite (metal)
The invention relates to a device for reducing or even eliminating edge dendrites formed on a metal deposition plate (6) by electrolytic reduction in a metal extraction process, comprising a non-conductive part (1), which, in use, at least along a first surface (2) and a respective second surface (3), at least along the respective edges (8 ', 8' ') of an anode (4) and a cathode (5), the non-conductive component (1) further has a groove (9) connecting the first and second surfaces (2, 3), the groove (9) being positioned in the direction of electrolyte flow to increase the width of the electrolysis channel (7) between the anode (4) and the cathode (5).
Owner:JOHN COCKERILL RENEWABLES SA

Zinc battery electrolyte additive

An electrolyte additive is provided. The additive is a quaternary ammonium or phosphonium salt effective to suppress hydrogen evolution and metal dendrite formation during operation of a zinc electrochemical cell such as a zinc-air battery. A zinc battery cell is also provided, which contains an effective amount of the electrolyte additive.
Owner:OCTET SCIENTIFIC INC

A method of ultrasonic-assisted preparation of single crystal alloys

The application belongs to the technical field of single crystal alloy preparation, and particularly relates to a method for ultrasonic-assisted preparation of single crystal alloy. The application introduces an ultrasonic-induced sound field and flow field in a directional solidification process, effectively controls the solute boundary layer thickness near a solidification interface, successfully realizes controllable conversion of high-temperature alloy from cellular crystal to steady-state dendrite under columnar crystal conditions, and significantly refines dendrite primary arm spacing. The application breaks through the limitation of traditional directional solidification on solidification structure size, provides a new technical path for preparation of high-performance high-temperature alloy, and comprehensively improves the application performance of metal materials.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Method for manufacturing a tc4 alloy

ActiveCN116770114BIngotDendrite (metal)
The application provides a preparation method of TC4 alloy and relates to the field of metallurgy. The preparation method comprises the following steps: ingredients are prepared according to the Ti-6Al-4V ratio, the ingredients are uniformly mixed, and then the ingredients are pressed into electrode blocks, vacuum plasma welding is performed, and a consumable electrode is obtained; after furnace centering, first, second and third vacuum arc melting is sequentially performed, and a TC4 alloy ingot is obtained after cooling; the first vacuum arc melting and the second vacuum arc melting perform arc starting stage control and stable melting stage control, and the third vacuum arc melting performs arc stage control, stable melting stage control and hot sealing stage control. The preparation method of the TC4 alloy provided by the application controls the stable melting pool morphology in the stable melting stage, reduces the melting pool depth, provides good conditions for the solidification of the ingot, ensures the smooth operation of the melting pool in the melting stage and the hot sealing stage, makes the liquid phase temperature and the composition uniform, reduces the dendrite spacing, and improves the uniformity of the ingot.
Owner:UNIV OF SCI & TECH BEIJING

A method for improving slab segregation

ActiveCN116274908BDendrite (metal)Molten metal
The application discloses a method for improving slab segregation, and belongs to the technical field of continuous casting. The method comprises the following steps: performing dynamic pressing on a slab with the mass fraction of Ni being greater than or equal to 3%, wherein the pressing amount is 0.5-3 mm when the slab is in the interval of fs=1.0-1.1. According to the method, dynamic light pressing is performed on the slab of high-nickel steel in the interval of fs=1.0-1.1 during continuous casting, and the pressing amount is controlled to be 0.5-3 mm, so that the molten metal of the slab can be fully pressed into the peripheral dendrites near the position of one fourth and three fourths, solute redistribution is realized, shrinkage holes are pressed together, the segregation and porosity problems of the slab of high-nickel steel near the position of one fourth and three fourths are reduced, and the internal quality of the slab of high-nickel steel is improved.
Owner:SHOUGANG GROUP CO LTD