Patents
Literature
Patsnap Eureka AI that helps you search prior art, draft patents, and assess FTO risks, powered by patent and scientific literature data.

47 results about "Sodium perborate" patented technology

Sodium perborate is chemical compound whose chemical formula may be written NaH₂BO₄, Na₂H₄B₂O₈, or, more properly, [Na⁺]₂·[B₂O₄(OH)₄]²⁻. Its name is sometimes abbreviated as PBS. The compound is commonly encountered in anhydrous form or as a hexahydrate (commonly called "monohydrate" or PBS-1 and "tetrahydrate" or PBS-4, after the early assumption that NaBO₃ would be the anhydrous form). They are both white, odorless, water-soluble solids.

Positive electrode lead paste for high-capacity and long-service-life storage battery and preparation method therefor

A positive electrode lead paste for a high-capacity and long-service-life storage battery and a preparation method therefor. The formula of the positive electrode lead paste comprises lead powder, dilute sulfuric acid, water and additives. In parts by mass, the additives added to every 1000 parts of the lead powder comprise: 1-3 parts of sodium perborate; 0.5-2 parts of 4BS; 1-3 parts of antimony trioxide; 1-3 parts of tin pyrophosphate; 2-4 parts of a polyolefin; 2-4 parts of a conductive carbon material; and 1-1.5 parts of a polyester staple fiber. By adding tin pyrophosphate and the polyolefin in the positive electrode lead paste, the capacity of a lead storage battery can be effectively increased and the service life thereof can be prolonged; and tin pyrophosphate and the polyolefin can work synergistically, and the addition of the two together achieves a better effect.
Owner:TIANNENG BATTERY GROUP

Preparation method of pyroxasulfone

The invention belongs to the technical field of organic synthesis, and particularly relates to a pyroxasulfone preparation method which specifically comprises the following steps: dissolving 3-(5-difluoromethoxy-1-methyl-3-trifluoromethyl-1H-pyrazol-4-ylmethylthio)-5, 5-dimethyl-2-isoxazoline serving as a raw material with a solvent, then adding a boron compound, finally dropwise adding hydrogen peroxide, and reacting at room temperature to obtain the pyroxasulfone. Reacting for several hours to obtain pyroxasulfone; the adopted boron compound is cheap and easy to obtain, so that the use of a transition metal catalyst is avoided, and the raw material cost is reduced; organic acid reagents with heavy odor are not used, waste water and solid waste are less, and the method has great advantages in the aspect of environmental protection; the method is simple to operate, free of complex treatment steps and suitable for industrial production, and when the boron compound is selected from sodium metaborate, sodium perborate or a mixture of borax and sodium metaborate, the yield and purity of the process are higher, and sulfoxide impurities are fewer.
Owner:JINGBO AGROCHEM TECH CO LTD

Washing machine tank cleaning agent and preparation method and application thereof

The invention provides a washing machine tank cleaning agent and a preparation method and application thereof. The washing machine tank cleaning agent comprises the following components in percentage by mass: 30-50% of peroxide, 3-10% of inorganic alkali, 15-20% of buffer alkali, 1-5% of lauryl sodium sulfate, 1-5% of protease and the balance of anhydrous sodium sulphate. Wherein the inorganic base is potassium hydroxide and / or sodium hydroxide, the buffer base is sodium carbonate and / or sodium bicarbonate, and the peroxide is sodium percarbonate and / or sodium perborate. According to the washing machine groove cleaning agent, in a specific peroxide system, the specific inorganic base and the specific buffer base are adopted, the synergistic interaction effect is achieved in the aspects of dirt removal, hair dissolution, bacteriostasis and the like, and compared with washing machine groove cleaning agents adopting other inorganic bases or other buffer bases, the washing machine groove cleaning agent has the advantages that the cleaning effect is good; according to the present invention, the effects of dirt removal, hair dissolution and bacteria inhibition are significantly excellent.
Owner:HANGZHOU HUICUI ZAOWU SUPPLY CHAIN MANAGEMENT CO LTD

Sodium perborate drying equipment

The utility model discloses sodium perborate drying equipment, which belongs to the technical field of sodium perborate drying, and comprises a filter cartridge for placing sodium perborate, and the side edge of the filter cartridge is rotatably connected with a first spraying pipe which is provided with a spraying port and is used for drying sodium perborate; the end, away from the first spraying pipe, of the second spraying pipe is fixedly connected with a cleaning brush, the end, away from the filter cartridge, of the first spraying pipe is connected with a third gas conveying pipe, and the side edge of the third gas conveying pipe is fixedly connected with a second gas conveying pipe. In the filtering process, a second air pump is started, cold air in an air tank is conveyed through a third air conveying pipe and sprayed through a first spraying pipe and a second spraying pipe, sodium perborate in a filtering cylinder is air-dried, meanwhile, the cold air is conveyed into the third spraying pipe through the third air conveying pipe, and filtered sodium perborate is air-dried.
Owner:浙江洁华新材料股份有限公司

Positive electrode lead paste of lead storage battery and preparation method of positive electrode lead paste

The invention provides a lead storage battery positive electrode lead paste and a preparation method thereof. The invention provides a rare earth-carbon-based composite lead storage battery positive electrode additive formula which comprises the following components in parts by weight: 25-35 parts of a carbon material, the carbon material comprises a carbon nanotube, graphene and expanded graphite, and the mass ratio of the carbon nanotube to the graphene to the expanded graphite is 1: 2: 3; 20 to 30 parts of a binder; the rare earth comprises a Ce element, and the molar ratio of the Ce element to the Sn element is 1: (8-10); 30 to 40 parts of a 4BS seed crystal; 50 to 80 parts of nano red lead powder; 1 to 1.5 parts of polyester fiber; and 5-10 parts of sodium perborate. According to the invention, a multi-dimensional conductive network is constructed through the combination of the carbon nanotubes, the graphene, the expanded graphite and the conductive binder, a stable three-dimensional network is formed, the problem of conductive anisotropy of traditional lead paste is solved, heterojunctions are formed through the SnO2-rare earth mixture, oxygen evolution overpotential is reduced, grains are refined, and corrosion of a positive grid is inhibited.
Owner:TIANNENG BATTERY GROUP

A single-component luminol chemiluminescent substrate solution and a preparation method thereof

The application belongs to the field of detection reagents, and particularly relates to a single-component luminol chemiluminescence substrate liquid and a preparation method thereof. The single-component luminol chemiluminescence substrate liquid comprises the following components: sodium acetate, sodium perborate, N-N dimethylacetamide, beta-cyclodextrin, luminol, 4-morpholinopyridine, p-acetylaminophenol, 4-hydroxyphenylacetic acid, phenothiazine-10-yl-propyl sulfonic acid sodium salt and isothiazolinone. The purpose of the application is to solve the technical defects that the luminol chemiluminescence substrate liquid in the prior art must be packaged in two components due to the instability of the luminous agent and the oxidizing agent in the liquid phase, leading to inconvenient use and easy introduction of operation errors, so as to provide a single-component luminol chemiluminescence substrate liquid and a preparation method thereof, which have high storage stability, high luminous performance and convenient use.
Owner:HEXU (ZHENGZHOU) BIOTECHNOLOGY CO LTD

A ramie degumming method combining pretreatment with composite enzymes and its application

The invention discloses a ramie degumming method and application of a pretreatment combined with a composite enzyme, and relates to the field of ramie fiber degumming. Before enzymatic degumming of the ramie fiber, the invention first mechanically rolls and boils the ramie fiber, and then performs pretreatment degumming. Borax decomposed by sodium perborate makes the inside of the fiber loose, and degrades the hemicellulose and lignin components of the ramie fiber, destroys the colloid combination, opens the inner wall supported by pectin, and causes the hemicellulose and lignin components to fall off and be removed. The hydrogen peroxide decomposed by sodium perborate in the pretreatment agent at high temperature decolorizes the pigment in the wood cellulose, bleaches the ramie, and can save the subsequent bleaching process for ramie degumming. At the same time, after oxidative degumming, the internal molecules of the ramie fiber are arranged loosely, and the aperture channels are opened, which increases the action sites for the enzyme molecules in the subsequent composite enzyme treatment and improves the reaction efficiency.
Owner:JIANGNAN UNIV

Long-acting oxygen producer for aquaculture water as well as preparation method and application of long-acting oxygen producer

The invention provides a long-acting oxygen producer for aquaculture water and a preparation method and application thereof, and belongs to the technical field of aquaculture, the long-acting oxygen producer comprises the following components by weight: 5-20 parts of sodium percarbonate, 65-85 parts of sodium perborate, 5-15 parts of sodium tetraborate pentahydrate, 0.5-2 parts of polyethylene glycol, and 0.2-0.5 part of magnesium stearate. Sodium perborate is rapidly dissolved to release oxygen to achieve a quick-acting oxygenation effect, the solubility of sodium tetraborate pentahydrate is higher than that of sodium perborate, sodium tetraborate pentahydrate is rapidly dissolved in water and hydrolyzed to form boric acid with a certain concentration, the dissolution and hydrolysis processes of sodium perborate are inhibited to a certain extent, and the oxygen release speed of sodium perborate is delayed. The oxygen release time and the use effect of the oxygen producer are greatly improved, the oxygen release time is prolonged to 16-36 hours, the oxygen producer does not need to be added again by workers at night, the breeding cost is reduced, the stability and sustainability of a breeding system are improved, and the economic benefits of the breeding industry are improved.
Owner:YUEYANG YUMEIKANG BIOTECHNOLOGY CO LTD

Bleaching agents containing percarbonates or perborates and persulfates

A composition for the oxidative color change of keratinous fibers, comprising – based on its total weight – (a) one or more per compounds from the group consisting of sodium percarbonate, potassium percarbonate, sodium perborate and potassium perborate in a total amount of 0.5 to 14.0 wt.%, and (b) one or more persulfates from the group consisting of ammonium persulfate, potassium persulfate and sodium persulfate in a total amount of 5.0 to 60.0 wt.%, and (c) less than 10.0 wt.% water, characterized in that it contains 3.0 to 12.0 wt.% sodium percarbonate, and contains 7.0 to 16.0 wt.% ammonium persulfate, and contains 20.0 to 45.0 wt.% potassium persulfate, and contains 1.0 to 6.0 wt.% sodium persulfate.
Owner:HENKEL KGAA

Preparation method of fire-resistant special crucible

PendingCN121318464ACarbide siliconCrucible
The invention belongs to the technical field of refractory materials, and particularly relates to a preparation method of a special refractory crucible. During preparation, the alpha-silicon carbide powder, the metal silicon powder, the fluoride powder, the sodium perborate, the precursor and the kaolin are subjected to dry mixing, and deionized water is added for stirring; adding the sol and the coupling agent, continuously stirring, mixing to form wet slurry, drying, crushing to obtain coarse particles, and aging to obtain an aged material; performing isostatic pressing on the aged material, and demolding to obtain a crucible green body; and pre-sintering the crucible green body, and sintering at high temperature to obtain the fire-resistant special crucible. The large holes are filled with the formed flowing glass phase, and the closed micropores are formed under the wrapping of the glass phase through fluoride reaction, so that a permeation channel of high-temperature molten metal is fundamentally blocked, the eroded depth of the crucible during use is reduced, the technical defect that open pores are easily formed after alpha-silicon carbide powder is sintered is overcome, and the service life of the crucible is prolonged. And the compact fire-resistant special crucible is prepared.
Owner:JIAXING HOT ADVANCED CERAMICS CO LTD

A method for efficiently degrading bisphenol compounds by using UV-LED combined with sodium perborate

The application discloses a method for efficiently degrading bisphenol compounds by using UV-LED combined with sodium perborate, and relates to the technical field of water treatment. The method adds sodium perborate into a bisphenol compound solution to be treated, and irradiates the water body by using UV-LED, so that the bisphenol compounds can be efficiently removed. The application utilizes the activated sodium perborate to efficiently degrade bisphenol compounds, and has the advantages of simple operation, low cost, excellent performance and high application value.
Owner:XIAMEN UNIV

Dental care and cleansing composition

ActiveUS12419828B2Cosmetic preparationsInorganic boron active ingredientsBiotechnologyPsidium guajava leaf extract
The present invention discloses a novel dental care composition comprising combination of various ingredients majorly includes natural ingredients which acts synergistically to treat various dental related disorders. The natural ingredients herein includes a synergistic composition of guava leaf extract, sodium perborate and honey. The said composition exhibits anti-oxidant, anti-microbial, anti-inflammatory and anti-septic properties.
Owner:GRP PHARMA LTD

Preparation method of novel chiral bipyridine and application thereof in catalytic reaction

The application belongs to the technical field of chemical industry and relates to a preparation method of a novel chiral bipyridine and application of the chiral bipyridine in catalytic reaction. Various benzyl bromides with 4,5-diazofluorene as a skeleton are reacted to generate a series of chiral bipyridine ligands, then under the participation of the ligands, indolines and quinoline nitrogen-containing heterocyclic compounds are reacted with pinacol diboronic acid under the catalysis of [IrOMe(COD)2] as a metal catalyst, and then a series of phenol compounds are obtained through oxidation of sodium perborate. The novel chiral bipyridine ligand developed by the method has the advantages of good site selectivity and excellent reaction yield without using strong acid and strong base in the process of C-H bond selective boronation.
Owner:DALIAN UNIV OF TECH

Method for sterilizing and decontaminating post-consumer absorbent sanitary products polluted with organic compounds derived from human metabolism

A method for sterilizing and decontaminating post-consumer absorbent products polluted with organic compounds derived from human metabolism including drug residues, the post-consumer absorbent sanitary products comprising fractions of plastic, super-absorbent polymers (SAP), and optionally cellulose, the method including at least the steps of: sterilizing (SR) the absorbent sanitary post-consumer products by heating to a temperature equal to or less than 140° C., and to a pressure lower than 4 bar, decontaminating (DC) the post-consumer absorbent sanitary products of organic compounds by treating with an oxidizing composition comprising at least one compound selected from the group consisting of hydrogen peroxide, sodium percarbonate, potassium percarbonate, sodium perborate, potassium perborate, potassium monopersulfate, ammonium persulfate, sodium persulfate, potassium persulfate, and ozone. The at least one compound is contained in the oxidizing composition in an amount equal to or greater than 2% by weight with respect to the dry weight of the post-consumer absorbent sanitary products.
Owner:PROCTER & GAMBLE CO

Synthetic method of minoxidil

The invention belongs to the field of organic synthesis, and particularly relates to a minoxidil synthesis method, which comprises the following steps: by taking 2, 4-diamino-6-chloropyrimidine as a starting material, oxidizing the starting material by sodium perborate tetrahydrate, and carrying out synergistic catalysis by adopting piperidine and ionic liquid. According to the invention, sodium perborate tetrahydrate and EDTA are adopted to inhibit the occurrence of peroxidation by-products; the ionic liquid is adopted, decomposition of oxides caused by high temperature is avoided, and the ionic liquid effectively inhibits side reactions; the dosage ratio of piperidine to 2, 4-diamino-6-chloropyrimidine-3-oxide is reduced, so that complete reaction is ensured, and side reaction caused by excessive piperidine is avoided; according to the method, the safety of the oxidation process is high, side reactions are effectively avoided, post-treatment is simple, and the method is green and environmentally friendly.
Owner:SHANDONG CAICAL MEDICAL TECHNOLOGY CO LTD

Novel synthesis method of dutasteride

PendingCN121270644ASteroidsIodideBoronic acid
The invention discloses a novel synthesis method of dutasteride, which is characterized in that sodium perborate is used as an oxidizing agent, and a proper solvent system and pH value are designed, so that efficient oxidation of hydrogenated dutasteride carboxylic acid iodide is realized, toxic reagents are prevented from being used, and impurities can be reduced; the high-purity dutasteride can be obtained through simple refining, the operability is high, and the method is suitable for industrial mass production.
Owner:HUANGGANG HUMANWELL PHARMACEUTICAL CO LTD

Method for preparing potassium peroxoborate by recovering sodium peroxoborate mother liquor with modified potassium type resin

This invention discloses a method for preparing potassium perborate from sodium perborate mother liquor using modified potassium-form resin, belonging to the field of resource comprehensive utilization technology. The method includes: pretreating a 732 type strong acid cation exchange resin to convert it to the potassium form, then modifying it with a 15-crown ether-5 ethanol solution to obtain a crown ether-modified potassium-form resin; passing the sodium perborate mother liquor through an exchange column packed with this resin, and performing ion exchange at 20-30℃, utilizing the specific selectivity of the crown ether for sodium ions to efficiently replace Na ions in the mother liquor with K ions in the resin, obtaining a pure potassium perborate solution; cooling the solution at -5~5℃ for crystallization, separation, and drying to obtain a high-purity potassium perborate product. This invention directly utilizes waste mother liquor as raw material, with a mild process, and produces a product with high active oxygen content (>16%), uniform particles, and good stability. It solves the problems of high cost, heavy pollution, and poor product quality associated with traditional processes, achieving green and high-value utilization of waste resources.
Owner:浙江洁华新材料股份有限公司

Multi-layer copper-molybdenum etching solution for LED field and preparation method of multi-layer copper-molybdenum etching solution

The invention relates to the technical field of etching solutions, and discloses a multilayer copper-molybdenum etching solution for the LED field, which comprises the following components by mass percent: 5.5-7.5% of sodium perborate; 6%-8% of hydrogen peroxide; 6%-7% of triammonium phosphate; 1%-2% of citric acid; 1%-2% of sodium citrate; 1.0% to 1.5% of iminodiacetic acid; 0.05%-0.1% of tin sulfate; 0.30%-0.45% of a dipotassium hydroxyethylidene-1, 1-diphosphonate solution; 0.08%-0.10% of sodium nitrite; 0.2% to 0.4% of water-soluble mercaptobenzothiazole; 0.02% to 0.05% of ethoxylated acetylene glycol; 0.02% to 0.05% of diethylene triamine pentamethylene phosphonate; and the balance of ultrapure water. A combination of sodium perborate and hydrogen peroxide is adopted as an oxidation system, a composite additive, a novel metal complexing agent and a surfactant matched with the etching solution are adopted, and the multilayer copper-molybdenum etching solution which is moderate in etching rate, good in anisotropy, high in substrate material selectivity and good in chemical stability is prepared.
Owner:SUZHOU BOYANG CHEM

Method for preparing N-phenyl phenylenediamine compound through structural reforming of imidazole compound

The invention relates to the technical field of organic synthesis, in particular to a method for preparing an N-phenyl phenylenediamine compound through structural reforming of an imidazole compound. According to the method for preparing the N-phenyl phenylenediamine compound through structural reforming of the imidazole compound, the borane compound serves as a reducing reagent, the imidazole compound is reduced to generate a boron-nitrogen heterocyclic ring compound, then the boron-nitrogen heterocyclic ring compound is further subjected to ring-opening oxidation through sodium borate tetrahydrate to generate the N-phenyl phenylenediamine compound, and the N-phenyl phenylenediamine compound is prepared. In the reaction process, by-products are few, the N-phenylphenylenediamine compound is high in selectivity and yield, and subsequent separation and purification are simple. Moreover, the method provided by the invention is simple in process, green and environment-friendly, simple to operate, low in cost, high in safety and suitable for industrial production.
Owner:LANZHOU INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES

Modified hard carbon negative electrode material and preparation method and application thereof

This invention discloses a modified hard carbon anode material, its preparation method, and its application, belonging to the field of electrode material technology. The preparation method provided by this invention includes the following steps: pre-treating barbecue charcoal material, immersing it in a sodium perborate solution, washing and drying it, then performing an oxidation treatment, followed by carbonization under inert gas, and finally cooling to obtain the final product. The hard carbon anode material prepared by this invention is beneficial for increasing the C=O content in the material, improving the sodium storage specific capacity, and optimizing its rate performance and cycle performance. It is an ideal anode material for sodium-ion batteries. The sodium-ion battery assembled in this application exhibits high initial discharge specific capacity and high initial coulombic efficiency, excellent rate performance, and good stability.
Owner:SOUTHWEST JIAOTONG UNIV

A lead-acid battery lead paste, a preparation method thereof, and a construction process

The present invention relates to the field of lead-acid battery plate preparation, and particularly to a lead-acid battery lead paste, a preparation method and a construction process thereof. Among them, a lead-acid battery lead paste includes a positive plate lead paste and a negative plate lead paste. The positive plate lead paste comprises the following components in parts by weight: 2.5-3 parts of sodium perborate, 1-2 parts of graphite, 0.8-1 part of glass fiber, 950-1050 parts of lead powder, 80-90 parts of deionized water, 110-120 parts of dilute sulfuric acid, and 10-20 parts of alcohol powder. The present invention mixes alcohol powder into the lead paste, and the alcohol powder uniformly fills the inside of the lead paste. In this way, when constructing the surface of the plate, only by melting the alcohol powder with water mist can the lead paste layer have uniform and fine micropores. In this case, not only the stability of the lead paste layer is ensured, but also the porosity of the plate is increased with more micropores.
Owner:ANHUI LEOCH POWER SUPPLY

Dry preparation method of sodium perborate and preparation device thereof

The invention discloses a dry preparation method of sodium perborate and a preparation device thereof, and belongs to the field of dry preparation of sodium perborate. The preparation method comprises the following steps: S1, hydrogen peroxide pretreatment: adding a stabilizer into a hydrogen peroxide solution; s2, preparing a reactant precursor, putting solid borax pentahydrate and solid sodium hydroxide into a horizontal reactor according to a certain molar ratio, and stirring; titanium dioxide is added, and an ultraviolet light beam emitter is turned on; then adding a weakly alkaline pH buffer regulator to obtain a reactant precursor; s3, spraying the hydrogen peroxide solution added with the stabilizer in the step S1 into the reactant precursor in the step S2, stirring, and increasing the power of an ultraviolet beam emitter when spraying begins; and after the reaction is finished, drying to obtain a sodium perborate solid. According to the method, solid-liquid separation is not needed, and the process link of centrifugation is omitted, so that a large amount of production time is saved, and the overall production efficiency is improved by more than 30%.
Owner:浙江洁华新材料股份有限公司

Preparation method of solid peracetic acid

The invention relates to the technical field of disinfectant preparation, and particularly discloses a preparation method of solid peracetic acid. Firstly, hydrogen peroxide and acetic anhydride are subjected to an oxidation reaction to prepare anhydrous peracetic acid, and then sodium perborate and anhydrous peracetic acid are subjected to an esterification reaction to prepare solid peracetic acid. Compared with the prior art, the method has the advantages that the use of high-concentration hydrogen peroxide is avoided, the solid peracetic acid is obtained by a safer, simpler and more convenient method, and the method is suitable for industrial production.
Owner:HUZHOU BAITE BIOLOGICAL TECH CO LTD

Ferrous sulfide cleaning passivator as well as preparation method and application thereof

The invention relates to the technical field of equipment cleaning agents, and particularly discloses a ferrous sulfide cleaning passivator. The ferrous sulfide cleaning passivator comprises, by weight, 0.5-2 parts of an oxidizing agent, 0.3-1 part of a chelating agent, 0.5-5 parts of a stabilizer, 0.2-1 part of a pH regulator and 90-100 parts of water. The oxidizing agent is one or more of sodium perborate, peracetic acid, potassium peroxymonosulfonate, butanedione and nitrobenzoic acid; the chelating agent is selected from one or more of ethylene diamine tetraacetic acid disodium salt, 1-hydroxyethylidene-1, 1-diphosphonic acid, amino trimethylene phosphonic acid, diethylene triamine penta (methylene phosphonic acid), glutamic acid tetrasodium diacetate and methylglycine trisodium diacetate. The ferrous sulfide cleaning and passivating agent provided by the invention has efficient cleaning and passivating effects, is environment-friendly and has a good application prospect.
Owner:JINAN HUICHENGDA TECH CO LTD

Method for cleaning reverse osmosis membrane

The invention relates to the technical field of cleaning of environmental protection equipment, in particular to a cleaning method of a reverse osmosis membrane. The cleaning method comprises the following steps: carrying out bubbling treatment on reverse osmosis membrane produced water to obtain a backflushing medium; carrying out first cleaning on the reverse osmosis membrane by using a backwashing medium to obtain a first cleaned membrane; the primary cleaning film is soaked with a cleaning agent, and a second cleaning film is obtained; wherein the cleaning agent is prepared from the following raw materials: citric acid, polyaspartic acid, sodium perborate, cellulase and tannic acid; performing second cleaning on the second cleaning film at preset pressure to obtain a third cleaning film; and performing third cleaning on the third cleaning membrane to obtain the regenerated reverse osmosis membrane. According to the cleaning method, the membrane flux recovery rate and the salt barrier rate recovery rate are synchronously improved from two core dimensions of pollutant removal thoroughness and membrane structure protection integrity through the progressive design of physical pre-cleaning, chemical targeted cleaning and multi-stage deep purification and in combination with the synergistic effect of all components of the cleaning agent.
Owner:武汉钢铁有限公司

A method for preparing an amido phenethyl alcohol compound by structural reorganization of an indole compound

The present application relates to the technical field of organic synthesis, and in particular to a method for preparing amido phenethyl alcohol compounds by structural reorganization of indole compounds. The method for preparing amido phenethyl alcohol compounds by structural reorganization of indole compounds provided by the present application uses borane compounds as a reducing agent, reduces indole compounds to generate benzazaborinine, and then further opens the ring and oxidizes to generate amido phenethyl alcohol compounds by sodium borate tetrahydrate. The structural reorganization of indole compounds successfully realizes the efficient synthesis of a series of amido phenethyl alcohol compounds, and the reaction process has few by-products, high selectivity and high yield of amido phenethyl alcohol compounds, and simple subsequent separation and purification. Moreover, the method provided by the present application is simple in process, green and environmentally friendly, simple in operation, low in cost, high in safety, and suitable for industrial production.
Owner:LANZHOU INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES

Single-component luminol chemiluminescent substrate solution and preparation method thereof

The invention belongs to the field of detection reagents, and particularly relates to a single-component luminol chemiluminescent substrate solution and a preparation method thereof. The single-component luminol chemiluminescent substrate solution is prepared from the following components: sodium acetate, sodium perborate, N, N-dimethylacetamide, beta-cyclodextrin, luminol, 4-morpholinopyridine, acetamidophenol, 4-hydroxyphenylacetic acid, phenothiazine-10-yl-propyl sodium sulfonate and isothiazolinone. The invention aims to solve the technical defects that in the prior art, a luminol chemiluminescent substrate solution must be packaged by two components due to instability of a luminescence agent and an oxidizing agent in a liquid phase, so that the luminol chemiluminescent substrate solution is inconvenient to use, and operation errors are easy to introduce. Therefore, the invention provides the single-component luminol chemiluminescent substrate solution with high storage stability, high luminescent property and convenience in use and the preparation method thereof.
Owner:HEXU (ZHENGZHOU) BIOTECHNOLOGY CO LTD

Photocatalytic material for degrading dye as well as preparation method and application of photocatalytic material

The invention discloses a preparation method of a photocatalytic material, which comprises the following steps: adding ferric trichloride into a dopamine aqueous solution to obtain a mixed solution, immersing a copper wire mesh into the mixed solution, keeping the temperature at 30-60 DEG C for 5-30 minutes, adding sodium perborate into the mixed solution, and continuously reacting for 30-60 minutes to obtain a dopamine modified copper wire mesh; adding bismuth oxychloride powder into a hydrochloric acid aqueous solution, and dispersing to obtain a composite solution; the dopamine modified copper mesh is immersed in the composite solution for 10-60 min at the temperature of 25-50 DEG C, and after being taken out, the dopamine modified copper mesh is placed for 10-30 min at the temperature of 25-60 DEG C; and repeating the dipping and standing, and naturally drying at room temperature to obtain the photocatalytic material. According to the preparation method disclosed by the invention, Cu2 (OH) 2CO3 / Cu2O can be generated on the surface of the copper mesh in situ, so that relatively firm combination is formed. The flaky composite material can be simply and conveniently recycled after the dye is degraded, and the prepared composite material has high photocatalytic degradation performance and can be used for removing organic colored pollutants generated in the printing and dyeing industry and the like.
Owner:NANTONG LOVER APPL +1

Reaction kettle for preparing sodium perborate

The utility model discloses a sodium perborate preparation reaction kettle, relates to the technical field of reaction kettles, and specifically comprises a kettle body and a filter box, the kettle body is located above the filter box, a motor is fixedly installed on the upper surface of the kettle body, one side of the kettle body is fixedly connected with a feeding port, the output end of the motor is fixedly connected with a connecting rod, and the connecting rod is fixedly connected with the filter box. The outer surface of the connecting rod is fixedly connected with a stirring rod, one side of the stirring rod is fixedly connected with a connecting block, and one side of the connecting block is fixedly connected with a scraping plate. According to the sodium perborate preparation reaction kettle, clean water is pumped into a fixed pipe through a water inlet pipe, then the water is pumped out through a plurality of water outlet heads and a water outlet, then a motor is started to drive a connecting rod to rotate, then the interior of the kettle body is cleaned with the clean water, and then residual additives on the inner wall of the kettle body are scraped off through a scraping plate; therefore, the cleaning effect is achieved, and the purpose of cleaning is achieved.
Owner:HEBEI JIUHAO ECOLOGICAL AGRI TECH CO LTD

Method for efficiently degrading common dyes in wastewater by using UV222 in combination with sodium perborate

The invention discloses a method for efficiently degrading common dyes in wastewater by using UV222 in combination with sodium perborate, and relates to the technical field of water treatment. UV222 (wavelength of 222nm) released by a plasma generator is combined with sodium perborate to form a synergistic oxidation system, high-activity free radicals are generated through photochemical activation, and efficient degradation of common dye pollutants in a water body is realized. A UV222 light source with a specific wavelength is adopted, so that the activation efficiency and the free radical yield of sodium perborate can be remarkably improved. Experiments show that the 30 min degradation rate of the method to methylene blue (MB) can reach 95% or above, and the method is suitable for various common dyes such as rhodamine B, malachite green, methyl orange and methyl violet. Compared with a conventional dye treatment technology, the method has the advantages of being higher in efficiency, lower in cost, simpler and more convenient to operate and remarkable in application value.
Owner:XIAMEN UNIV