66results about How to "Well matched thermal expansion" patented technology

A MEMS microphone system suited for harsh environments. The system uses an integrated circuit package. A first, solid metal lid covers one face of a ceramic package base that includes a cavity, forming an acoustic chamber. The base includes an aperture through the opposing face of the base for receiving audio signals into the chamber. A MEMS microphone is attached within the chamber about the aperture. A filter covers the aperture opening in the opposing face of the base to prevent contaminants from entering the acoustic chamber. A second metal lid encloses the opposing face of the base and may attach the filter to this face of the base. The lids are electrically connected with vias forming a radio frequency interference shield. The ceramic base material is thermally matched to the silicon microphone material to allow operation over an extended temperature range.

The invention discloses a solid oxide fuel cell with symmetrical electrodes and a preparation method and application thereof. The solid oxide fuel cell has the following symmetrical structure: an electrocatalysis membrane electrode deposited on the inner wall of the pore of a porous electrolyte, a compact electrolyte layer and another electrocatalysis membrane electrode deposited on the inner wall of the pore of the porous electrolyte. The preparation method comprises the following steps: preparing a porous electrolyte/compact electrolyte/porous electrolyte skeleton structure and an electrocatalysis membrane electrode infiltration precursor solution; infiltrating the prepared porous electrolyte/compact electrolyte/porous electrolyte skeleton structure in the electrocatalysis membrane electrode infiltration precursor solution by using an impregnation method; and carrying out heat treatment. The cell provided by the invention has the advantages of good thermal expansion coupling performance, good thermal shock resistance, low cost, a short preparation period, etc.; and when hydrocarbon is used as a fuel, carbon deposition on the positive electrode of the cell can be effectively prevented, and the cell can be used as an electrolytic bath and has commercialization prospects.

The invention discloses functionalized graphene-based solar back aluminum slurry and a preparation method thereof. The solar back aluminum slurry is prepared from the following raw materials in percentage by weight: 65-73 percent of aluminum powder, 1-3 percent of glass powder, functionalized graphene dispersion liquid containing 0.12-0.15 percent of functionalized pure graphene, 20-30 percent of organic carrier, 3-5 percent of auxiliary agent and the balance of diluent, wherein oxidized graphene is modified by using a coupling agent; the modified oxidized graphene is obtained through reaction of the coupling agent and the oxidized graphene and then is reduced to obtain the functionalized graphene; the functionalized graphene is dispersed into terpineol and butyl carbitol with a mass ratio of 5.5-6.5:1 after being subjected to ultrasonic treatment to form the functionalized graphene dispersion liquid. The preparation method comprises the steps of mixing, grinding and vacuum deformation of the raw materials. The solar back aluminum slurry has the advantages of high printing rate and good adhesion, conductivity, bending resistance and weathering resistance.

A carbon fiber toughened carbon-silicon carbide based composition with high thermal expansion match performance, low-temp antioxidizing performance, toughness and purity features that its reinforcing phase is carbon fiber, its basic body phase is the alternatively laminated 2-5 carbon-silicon carbide layers, and its external layer is silicon carbide for high antioxidizing performance. Its preparing process is sequential impregnation and thermodecomposing of boronphenolic aldehyde and polycarbonsilane.

A ferritic stainless steel having improved high temperature mechanical properties includes greater than 25 weight percent chromium, 0.75 up to 1.5 weight percent molybdenum, up to 0.05 weight percent carbon, and at least one of niobium, titanium, and tantalum, wherein the sum of the weight percentages of niobium, titanium, and tantalum satisfies the following equation: 0.4<=(% Nb+% Ti+½(% Ta))<=1. The coefficient of thermal expansion of the ferritic stainless steel is within 25 percent of the CTE of stabilized zirconia between 20° C. (68° F.) and 1000° C. (1832° F.), and the steel exhibits at least one creep property selected from creep rupture strength of at least 1000 psi at 900° C. (1652° F.), time to 1% creep strain of at least 100 hours at 900° C. (1652° F.) under load of 1000 psi, and time to 2% creep strain of at least 200 hours at 900° C. (1652° F.) under load of 1000 psi. The steel is particularly suited for high temperature applications including, but not limited to, current collecting interconnects in solid oxide fuel cells, furnace hardware, equipment for the chemical process, petrochemical, electrical power generation, and pollution control industries, and equipment for handling molten copper and other molten metals.

The invention relates to a low-temperature solid oxide fuel cell and a making method thereof. The structure of the low-temperature solid oxide fuel cell comprises an anode film deposited on the inner wall of a porous perovskite structure oxide ceramic La1-xSrxGa1-yMgyO3-delta composite film, a cathode film deposited on the inner wall of the porous perovskite structure oxide ceramic La1-xSrxGa1-yMgXO3-delta composite film, and a compact perovskite structure oxide ceramic La1-xSrxGa1-yMgyO3-delta electrolyte film positioned between the anode film and the cathode film, wherein each of x, y and delta is equal to or more than 0 and equal to or lower than 0.2, and the perovskite structure oxide ceramic La1-xSrxGa1-yMgyO3-delta composite film is formed through a porous perovskite structure oxide ceramic La1-xSrxGa1-yMgyO3-delta substrate, the perovskite structure oxide ceramic La1-xSrxGa1-yMgyO3-delta and a porous perovskite structure oxide ceramic La1-xSrxGa1-yMgyO3-delta film. The invention also provides the making method of the low-temperature solid oxide fuel cell.

The invention discloses a glass sealing material for a thermal battery and a preparation method thereof. The invention is characterized in that the glass sealing material comprises the following components in percentage by mole : 60-80% of SiO2, 3-15% of BaO, 5-15% of Na2O, 4-15% of K2O, 0-6% of Al2O3, 0-6% of B2O3, 0-5% of Li2O, and 0-5% of La2O3. The glass sealing material disclosed by the invention basically comprises SiO2, Al2O3 and B2O3, is added with proper matching of alkali metal oxide (mixed alkali effect) so as to control a softening point and viscosity of glass, improve the flowability of the glass and improve the performance of glass powder by adding modified oxides such as La2O3 with certain content and auxiliary ingredients, so that the wetting property of the glass to a titanium battery cover is improved. In addition, the invention prepares the glass sealing material by reasonable manufacturing technologies such as smelting, clearing, pulverizing, granulating and the like, so that the leakage rate of a sealing cover of the thermal battery produced by the sealing material disclosed by the invention is less than 1.0 multiplied by 10-10Pa.m<3>/s, and the insulation resistance is improved by more than one times compared with that of the sealing cover produced by the prior art.

The invention discloses a boride modified glass ceramic based composite high-temperature oxidation resisting coating. The composite high-temperature oxidation resisting coating fired on the surface of a refractory metal matrix is prepared from boride and silicate glass, wherein the boride is at least one or two of HfB2, ZrB2 and TiB2; besides, the invention further discloses a preparation method of the coating. The method comprises steps as follows: 1, the surface of the refractory metal matrix is treated; 2, boride particle modified glass ceramic composite slurry is prepared; 3, a preset layer is obtained by presetting the slurry on the surface of the refractory metal matrix, and the boride modified glass ceramic based composite high-temperature oxidation resisting coating is obtained vacuum high-temperature firing. The composite high-temperature oxidation resisting coating is used for high-temperature protection of the refractory metal matrix and can continuously protect the refractory metal matrix at the protection temperature of 400-1,600 DEG C for 5 h or longer.

The invention discloses a preparation method for a fuel cell with an ordered porous structured electrode. The preparation method is characterized in that the electrode has an ordered columnar porous structure; and the battery structure comprises a porous electrolyte layer impregnated with an electrode catalyst/compact electrolyte layer/porous electrolyte layer impregnated with the electrode catalyst. The preparation method comprises the steps of (1) preparing ordered porous structured electrolyte layer paste, compact electrolyte layer paste and an electrode catalyst impregnation liquid; (2) preparing porous electrolyte layer/compact electrolyte layer/porous electrolyte layer framework; and (3) impregnating the porous electrolyte layer framework with the electrode catalyst. The fuel cell provided by the invention can provide high gas transmission channels and ionic and electronic conductive network, and has better performance compared with a conventional solid oxide fuel cell; and meanwhile, the fuel cell has the advantages of high thermal expansion matching performance, low preparation cost, simple preparation process and the like, can be used as the fuel cell and an electrolytic cell and has high development prospect.

The invention discloses an iron-based coating material for heat insulating protection and a coating preparation method thereof and belongs to the technical field of surface coatings. Raw materials selected include alloy blocks and pure metal blocks, and specifically are ferroboron, ferroniobium, ferrosilicon, pure chromium and pure iron; a high-temperature nitrogen gas atomizing method is adopted to prepare alloy powder, and the alloy powder of 20-45 um in degree of sphericity and granularity; a hypersonic flame spraying method is adopted to prepare an iron-based noncrystalline or nanocrystalline coating. The coating prepared by the method has relatively low heat conductivity and can be used for heat insulating protection of heat-end parts of automobile engines.

The invention provides a cermet composite material and a coating preparation method thereof, belongs to the field of thermal spraying in composite materials and surface engineering, and particularly relates to a preparation method for metal-based composite powder with low thermal conductivity and a coating thereof by atmospheric plasma spraying. The method comprises the following steps that iron-based amorphous powder prepared by the high pressure nitrogen gas atomization method is mixed with zirconia powder prepared by the agglomeration sintering method according to a certain mass ratio, andfinally the composite powder with a better sphericity and a particle size of 25-75 [mu]m is obtained. The iron-based-ceramic composite coating is prepared by adopting the atmospheric plasma spraying mode, and the composite coating prepared has relatively low thermal conductivity, and can be used for insulation protection for hot end parts of a diesel engine.

The invention relates to a non-cobalt IT-SOFC (Intermediate-Temperature Solid Oxide Fuel Cell) stable anode material and application thereof and belongs to the technical field of fuel cells. The A site of SrFeO3-delta is doped with Nd, and the B site of the SrFeO3-delta is doped with Cu, so that the prepared (Nd1-xSrx)a (Fe1-yCuy)bO3-detal (NSCFu) anode material has high oxygen reduction catalytic activity, and the electrochemical performance is greatly improved. The anode material has long-term stability, and meanwhile has the advantages of high electronic conductivity, and high chemical compatibility and thermal expansion compatibility with cerium-oxide-based electrolytes. Thus, the SOFC anode material is potential.

The invention relates to a preparation method of a high-temperature resistant metal sealing material for a compact mixed conductor oxygen permeable ceramic membrane and a sealing application method of the material, in particular to a preparation method of the sealing material between a compact mixed conductor oxygen permeable ceramic membrane piece and a supporting component thereof and an application method of the sealing material, belonging to the technical field of a special ceramic welding material. The high-temperature resistant metal sealing material comprises the following components in weight percentage: 92-95% of Cu, 4-7% of Sn, 0-0.005% of Al, 0.1-0.3% of Zn, 0-0.05% of Fe, 0.04-0.2% of Pb, 0.1-0.3% of Ni and 0.1-0.5% of P. The preparation method comprises the following steps: weighing raw materials according to the formula for blending; placing the mixed materials in a vacuum induction furnace the vacuum degree of which is less than 2Pam for smelting at the temperature of 1100-1150 DEG C for 3-5 minutes until the materials are molten; and cooling to room temperature, and then taking out molten blocks to finally obtain the high-temperature resistant sealing material. The sealing material obtained by the method of the invention has very high sealing tightness as well as good chemical stability on the oxygen permeable ceramic membrane.

The invention discloses a full-carbon fiber composite material reflecting mirror substrate and a preparation method thereof. The full-carbon fiber composite material reflecting mirror substrate comprises a first panel, a first adhesive film, a honeycomb core, a second adhesive film and a second panel, wherein the first panel is adhered to one side of the first adhesive film; the second panel is adhered to one side of the second adhesive film; and the other side of the first adhesive film and the other side of the second adhesive film are adhered to two sides of the honeycomb core. By designing the first panel, the honeycomb core and the second panel, properties of a carbon fiber composite material are effectively utilized and the problems of a traditional reflecting mirror that the weight is great, the coefficient of thermal expansion is high and the thermal performance is not matched are solved; and layering angles and sequences of the honeycomb core are designed so that the specific modulus of the reflecting mirror is improved and the defect that the honeycomb vertical performances of the traditional reflecting mirror are poor is overcome.

The invention discloses an OLED display device and a packaging technology thereof. The technology concretely comprises the steps that a packaging glass cover plate and a substrate are cut, and glass material is heated to the molten state of glass water for standby application; the packaging glass cover plate is arranged on the substrate; and glass water is coated on the end surface, which is contacted with the substrate, of the packaging glass cover plate and then naturally cooled to room temperature so that the preparation process is completed. The size of the packaging glass cover plate is less than that of the substrate so that a circle of bare peripheral part of the substrate is formed outside the external edge of the packaging glass cover plate, and glass water is coated on the bare peripheral part of the substrate. According to the packaging technology of the OLED display device, packaging glass is processed in advance so that maximization of a display region can be realized and packaging speed can also be enhanced.

The invention provides a solid oxide electrolysis cell cathode material as well as a preparation method and an application thereof. The method comprises the following steps: (1) providing gel; (2) heating the gel to be combusted, thereby obtaining a combustion product; (3) grinding the combustion product, thereby obtaining combustion powder; (4) pre-sintering the combustion powder, thereby obtaining pre-sintered powder; and (5) calcining the pre-sintered powder, thereby obtaining the solid oxide electrolysis cell cathode material. According to the method, the solid oxide electrolysis cell cathode material with the chemical composition of Sr2Fe(1-x)MxO6-delta can be rapidly and effectively prepared, and due to the two-section calcining method, the Sr2MoO3 mixed phase can be effectively eliminated, a single perovskite phase product is obtained, and the obtained product is small in particle size and high in electrical conductivity. In addition, the thermal expansion coefficient of the obtained solid oxide electrolysis cell cathode material is close to LSGM and is well matched with thermal expansion of an electrolyte material with excellent performance.

The invention discloses a complex protective coating of a sink roll used for hot dip coating and a preparation method. The complex protective coating comprises a bottom layer, a transition layer and a working layer; the bottom layer is a CoCrW coating, the transition layer is a coating of a mixture formed by CaO-SiO2 and CoCrW according to a proportion, and the working layer is a CaO-SiO2 coating; and a thermal expansivity relation among the coatings and a thermal expansivity relation among the coatings and a roll body are set. Coating is performed on the bottom layer by means of high velocity oxygen-fuel equipment, coating is performed on the transition layer and the working layer by means of plasma spraying equipment, corresponding technological parameters are set in the coating forming processes, and accordingly the complex protective coating on the surface of the sink roll is obtained. According to the complex protective coating provided by the invention, through design on the coating structure, good thermal expansion matching between the complex protective coating and base metal of the roll is achieved, and the purpose that the complex protective coating can be applied to practical production stably in a long term is achieved; and the preparation method is easy to operate, and the complex protective coating on the surface of the roll can be prepared and obtained.

The invention belongs to the technical field of hard alloy materials, and in particular relates to a hard alloy surface treatment method and an application. According to the hard alloy surface treatment method provided by the invention, as surface carburizing treatment or surface nitriding treatment is carried out on a hard alloy, the obtained hard alloy has a surface Co poor layer and can inhibitdiffusion of Co in the hard alloy to a coating effectively. The thermal expansion matching property of the coating and the hard alloy is improved, so that the mechanical property of the coating at ahigh temperature is improved. The service performance of the coating is improved obviously, and the service life of an AlTiN coating is prolonged. A product is high in mechanical property, good in wear resistance and excellent in cutting performance at a high temperature.

The invention discloses a solid oxide fuel cell based on proton conduction type electrolyte and a preparation method of the solid oxide fuel cell. An electrolyte material in a traditional SOFC single cell is replaced by a CD<1-x>M<x>O<3-delta> type perovskite structure proton conduction type electrolyte material; acathode material of an AA'B2O6-delta type double-layer perovskite structure is also adopted; the anode layer and the cathode layer of the SOFC single cell are both prepared from a metal oxide target material containing a pore-forming agent through magnetron sputtering; and an electrolyte layer is prepared from the metal oxide target material without the pore-forming agent through magnetron sputtering. The method is wide in material selection and simple in preparation process; organic solvents, binders, plasticizers, activators, other organic auxiliaries and the like are not used in the whole process; and the method belongs to environment-friendly processing preparation means and technological processes.