The application provides a resource treatment method of waste
palladium catalyst. The method first carries out
microwave carbon removal,
plasma etching and N-TiO2 light catalyst loading on the waste
palladium catalyst to complete carrier loosening modification; then in a supercritical extraction kettle with an embedded
ultraviolet LED lamp, a gradient strategy of 'weak complexing agent pre-washing
impurity removal + strong complexing agent main
palladium extraction' is adopted, combined with light
catalysis-super critical synergistic effect to strengthen palladium
desorption and selective extraction; then the
impurity metal and weak complexing agent are recovered through reduced pressure condensation, and the palladium complex fluid is purified through a
silica gel adsorption column; then the purified fluid is introduced into a loading kettle to mix with a carrier precursor suspension,
hydrogen is introduced for in-situ reduction, and
palladium nanoparticles are loaded, and a palladium-based catalyst applicable to industrial application is directly obtained through
drying and
calcination; finally, the waste carrier is
microwave activated (
active carbon carrier is additionally steam activated) to realize deep reuse.