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40results about How to "Control size" patented technology

Method for preparing pyramid array on monocrystalline silicon substrate

The invention relates to a method for preparing a pyramid array on a monocrystalline silicon substrate, and belongs to the technical field of manufacture of photovoltaic and semiconductor devices. The method comprises the following steps of: covering microballons in periodic arrangement on the surface of a monocrystalline silicon piece, and annealing near the glass transition temperature point of the microballoon; in oxygen atmosphere, obtaining a microballoon array in separation arrangement after etching by use of inductive coupling plasma; depositing a metallic titanium membrane on the monocrystalline silicon piece uniformly by a physical vapor deposition manner; and putting a silicon wafer with a masking film into an alkaline solution containing a surfactant for corrosion so as to obtain the pyramid array in order arrangement. The method is simple in process, short in preparation period and mature in technology; and three structures such as a positive pyramid array, an inverted pyramid array and a positive and inverted pyramid combined array can be obtained by a method for preparing a template through selecting and fine turning. The method has wide application value in the fields of photovoltaic, magnetic memory devices, nano photoelectric devices, nano sensors, surface raman enhancement and surface plasma effect and the like.
Owner:HUANGSHAN AKENT SEMICON TECH

Preparation method for metal organic framework-derived tricobalt tetroxide-modified titanium dioxide nanotube array

The invention discloses a preparation method for a metal organic framework-derived tricobalt tetroxide-modified titanium dioxide nanotube array. The method comprises the following steps: firstly performing pretreatment on a titanium sheet substrate material; performing electrochemical treatment on the treated titanium substrate material by using an ethylene glycol solution containing ammonium fluoride and water as an electrolyte, and performing calcination by using a muffle furnace to change a titanium dioxide crystal form; secondly, performing cobalt hydroxide electrodeposition by means of athree-electrode electrochemical workstation and by using cobalt nitrate hexahydrate as an electrolyte, a titanium dioxide nanotube array as a working electrode, a platinum sheet as a negative electrode and silver/silver chloride as a reference electrode; performing hydrothermal treatment on the titanium dioxide nanotube array to form ZIF-67 in situ; and finally, performing secondary calcination byusing a muffle furnace to obtain the ZIF-67-derived porous tricobalt tetroxide-modified titanium dioxide nanotube array. The method disclosed by the invention can effectively improve absorption capacity of TiO2 on visible light, promote separation of electron hole pairs, and improve photocatalytic degradation efficiency of organic pollutants.
Owner:SUZHOU UNIV

Process for producing nanostructured tin dioxide lithium ion battery negative pole material

The invention belongs to the preparation field of the anode material of a lithium ion battery, and in particular relates to a method for preparing metal oxide electrode material with a nanometer structure by utilizing the in-situ synthesis method. The internal structure and the dimension of a hollow micro-sphere obtained are controlled through adjusting the pH value of a system by utilizing hydrochloric acid. Raw materials in the invention are common and are easy to obtain; an organic solvent is not required during the preparation process; the preparation process is simple; the synthesis of template materials and the participation of a surface active agent are not required during the synthetic process; the requirements to the device are low, the time consumption is less and the preparation process is simple; and a main by-product during the preparation process is water and carbon dioxide and is environment-friendly. The raw materials used in the invention are common; and the preparation conditions are not restricted by areas. The hollow tin dioxide micro-spheres have higher application prospect in the filed of electrode material, catalyst carriers and the like. The method has the advantages of cheap and easily obtained raw materials, simple preparation process, and unrestricted preparation conditions by areas, and is suitable for massive industrial production.
Owner:JILIN UNIV

SSZ-13 molecular sieve, method for regulating crystal morphology of SSZ-13 molecular sieve and application of SSZ-13 molecular sieve

The invention belongs to the technical field of molecular sieve preparation, and relates to an SSZ-13 molecular sieve, a method for regulating and controlling the crystal morphology of the SSZ-13 molecular sieve and application of the SSZ-13 molecular In order to solve the technical problems that the SSZ-13 molecular sieve is large in particle size and uneven in particle size distribution due to the fact that the SSZ-13 molecular sieve morphology control technology is difficult to control in the prior art, the method for controlling the SSZ-13 molecular sieve crystal morphology is provided, a silicon source, an aluminum source, alkali and a structure-directing agent are added into pure water to be mixed evenly, then a crystal morphology control agent is added for further treatment, and the SSZ-13 molecular sieve crystal morphology is obtained. According to the method, the crystal morphology and size of the SSZ-13 molecular sieve can be effectively controlled, the SSZ-13 molecular sieve of a cubic, polyhedral or spherical crystal can be prepared, the grain size of the crystal is small and can be adjusted within a certain range, and the grain size distribution is uniform. When being used as an SCR (selective catalytic reduction) denitration catalyst to be applied to the field of automobile exhaust treatment, the catalyst shows high denitration catalytic performance, high hydrothermal aging stability and wider effective working temperature range.
Owner:安徽纳蓝环保科技有限公司
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