The invention discloses a preparation method of a high-performance composite 
carbon felt, and particularly relates to the technical field of 
fiber products. The preparation method comprises the specific steps of material cleaning, PAN (
polyacrylonitrile) precursor preparation, pre-oxidation, 
carbonization, graphitization, surface treatment and 
coating treatment. According to the invention, a material cleaning step is added to the composite 
carbon felt process, impurities in the finished 
carbon felt can be effectively eliminated from the source, and the influence of the impurities upon the quality of the finished carbon felt is prevented; 
polyacrylonitrile is dissolved using n-butyl 
alcohol, the characteristics of the carbon 
fiber and the carbon felt of the subsequent 
branch are ensured accordingly, the parts of the carbon felt are stressed uniformly so that the fracture caused by uneven stress at 
impurity positions in the traditional process is avoided, the stretching effect of the finished carbon felt in the using process is effectively improved, and the service life of the carbon felt is ensured; volatilized n-butyl 
alcohol vapor can be liquefied again after being cooled for secondary use, and therefore, the production cost of a manufacturer is guaranteed.