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33results about How to "Mild working conditions" patented technology

Extraction and preparation method for licorice effective ingredients

InactiveCN103965152AHigh yield of active ingredientsHigh yieldSugar derivativesSteroidsWater dischargeLicorice acid
The invention relates to an extraction and preparation method for licorice effective ingredients, mainly to a method for simultaneously extracting effective ingredients like glycyrrhizic acid, glycyrrhiza flavonoid and a licorice flavoring agent from licorice. The method comprises the following steps: with glycyrrhizic acid as a raw material, carrying out extraction so as to obtain licorice residue and extract liquid and subjecting the licorice residue to ethanol extraction so as to obtain a crude glycyrrhiza flavonoid product; removing impurities in the licorice extract liquid by using an ultrafiltration membrane device, carrying out concentration by using a nanofiltration membrane device, subjecting a nanofiltration membrane concentrate to acid precipitation and drying a precipitate so as to obtain glycyrrhizic acid; and subjecting a supernatant produced after acid precipitation to concentration with the nanofiltration membrane device and carrying out drying so as to obtain the licorice flavoring agent. The method adopts membrane separation technology for impurity removal and concentration of the extract liquid, so working conditions are mild, product purity and quality are guaranteed, and yield of licorice effective ingredients is high; the method has the advantages of simple production flow, low cost, small pollution, reusability of a nanofiltration membrane filtrate generated in production process, reduction in consumption of raw water and great decrease of waste water discharge.
Owner:武汉普赛特膜技术循环利用有限公司

Method for producing purely natural monosodium glutamate by using low-value marine fishes

The invention relates to a method for producing purely natural monosodium glutamate by using low-value marine fishes, which comprises the following steps of: adding water in an amount which is 1 to 3 times the weight of low-value marine fishes, and 0.01 to 0.03 weight percent of antioxidant into the low-value marine fishes; raising the temperature to 60 to 80 DEG C, stirring at the pH of 7 to 9 for 1 to 3 hours, adding 0.3 to 0.5 weight percent of alkaline protease and performing enzymolysis at the temperature of between 45 and 60 DEG C and the pH of 7 to 9 for 2 to 4 hours; filtering to remove fish bones and centrifuging to remove fish oil and fish scrap; adding 0.3 to 0.5 weight percent of flavorzyme into filtrate and performing enzymolysis at the temperature of between 45 and 60 DEG C and the pH of 6 to 8 for 2 to 4 hours; heating to 100 DEG C after the enzymolysis is finished, and inactivating for 5 minutes; regulating the pH of enzymolysis liquid to 5 to 6.5 by using citric acid, adding 1 to 3 weight percent of activated carbon, stirring at the temperature of between 60 and 75 DEG C for 2 to 3 hours, centrifuging and filtering; removing impurities from filtrate by using an ultrafiltration membrane of about 2,000Dal and concentrating the filtrate by using a nanofiltration membrane of about 400Dal in turn; and adding 0.1 to 0.3 weight percent of flavor substances and 0.2 to 0.5 weight percent of truffle into concentrated solution, dissolving, uniformly mixing and performing spray drying. The low-value marine fishes are reasonably utilized, the process is simple, secondary pollution is avoided and a large amount of waste water cannot be generated.
Owner:WUHAN AIMIN PHARMA

Comprehensive utilization method of pumpkin

The invention relates to a comprehensive utilization method of a pumpkin. In the method, added amount of substances is based on weight of the pumpkin; and the pumpkin is taken as a raw material for step-by-step extraction to respectively obtain pumpkin polysaccharide, pectin and pumpkin powder by utilizing a biotechnology and a membrane separation technology. The method comprises the following steps: firstly washing and cutting the pumpkin into blocks, removing seeds, pulping, carrying out water extraction at moderate temperature and centrifugal separation, carrying out acid precipitation on the obtained water extract, concentrating the obtained supernate through a nanofiltration membrane, and spray-drying to obtain the polysaccharide; extracting residues after water extraction by utilizing acid water, carrying out centrifugal separation, removing impurities from the obtained supernate through a microfiltration membrane, concentrating the supernate through a nanofiltration membrane, carrying out acid precipitation on the obtained concentrated solution, carrying out centrifugal separation, and freeze-drying the obtained precipitate to obtain the pectin; spray-drying the supernate to obtain the polysaccharide; and mixing the remaining residues and filtered liquor, grinding by a colloid mill and spray-drying to obtain the pumpkin powder. The comprehensive utilization method has the advantages that effective substances of the pumpkin are fully utilized, and process is simple and feasible, thus being applicable to industrialized production.
Owner:武汉普赛特膜技术循环利用有限公司

Warm isostatic pressing machine

The invention relates to an isostatic pressing machine, particularly relates to a warm isostatic pressing machine, and solves the problems that an existing warm isostatic pressing machine is complex in structure, low in efficiency, large in energy consumption and poor in working condition. The warm isostatic pressing machine comprises a rack, wherein a pressurizing oil cylinder is installed on an upper beam of the rack, a high-pressure cavity located under the pressurizing oil cylinder is installed on a lower beam of the rack, a piston rod of the pressurizing oil cylinder can be inserted into the high-pressure cavity in a sealed mode, a heat conduction tank is also included and filled with heat conduction oil, an electric heater is arranged in the heat conduction tank, an oil injection hole is formed in the bottom of the high-pressure cavity, an oil return hole is formed in the top of the high-pressure cavity, and the heat conduction tank communicates with the high-pressure cavity through a heat conduction pump, a one-way valve and the oil injection hole by means of a pipeline and further communicates with the high-pressure cavity through an oil return pipe and the oil return hole. The warm isostatic pressing machine is technically characterized in that the mode that the high-pressure cavity of the isostatic pressing machine obtains high pressure is changed into a direct pressurization mode from an injection mode, and defects of an existing warm isostatic pressing machine are overcome.
Owner:TAIYUAN UNIVERSITY OF SCIENCE AND TECHNOLOGY +1

Method for extracting lithium from high-calcium lithium-containing raw material

The invention relates to a method for extracting lithium from a high-calcium lithium-containing raw material, which comprises the following steps: (1) calcium precipitation: adding the calcium-containing lithium-containing raw material into a reaction container, adding a calcium precipitator, stirring to generate calcium sulfate crystals, and carrying out solid-liquid separation to obtain a decalcified lithium-containing mother solution; (2) nanofiltration: carrying out nanofiltration on the decalcified lithium-containing mother liquor obtained in the step (1) through a nanofiltration system to further decalcify and remove other ions greater than or equal to 2 so as to obtain lithium-containing filtrate; and (3) evaporating and concentrating: evaporating and concentrating the lithium-containing filtrate obtained in the step (2) to obtain a lithium-rich concentrated solution. The method has the advantages of simple operation steps, mild working conditions, low energy consumption, safe operation and less environmental pollution; and the whole operation process is carried out according to safe, energy-saving and environment-friendly conditions. The method is suitable for extracting lithium from various calcium-containing and lithium-containing raw materials, is low in production cost, and is particularly suitable for extracting lithium from high-calcium and lithium-containing raw materials.
Owner:CHANGSHA DESIGN & RES INST OF CHEM IND MIN

A kind of solar semiconductor refrigeration type water collector

The invention discloses a solar semiconductor refrigeration type water collector. The solar semiconductor refrigeration type water collector comprises a solar power generation panel, a voltage regulation module, a storage battery and a water collection device, wherein the solar power generation panel is connected with the storage battery through the voltage regulation module; the storage battery is connected with the water collection device; the water collection device comprises a heat radiator, a heat pipe, a semiconductor refrigeration assembly, a cylindrical water collection tank and a water storage tank; a water inlet of the water storage tank is connected with a water outlet of the water collection tank; the water collection tank is internally provided with an annular cold air channel; the cold air channel is internally provided with a separation plate; an air inlet and an air outlet, which are communicated with the cold air channel, are formed in the upper end of the water collection tank; the air inlet and the air outlet are located on the two sides of the separation plate respectively; the air inlet is provided with an air blowing fan; one end of the semiconductor refrigeration assembly is inserted into the cold air channel; and the other end of the semiconductor refrigeration assembly is connected with the heat radiator through the heat pipe. The solar semiconductor refrigeration type water collector has the advantages of simple structure, convenience for installation, low environment requirements and high water collection efficiency.
Owner:SOUTH CHINA UNIV OF TECH

Rotary-type bioreactor

The invention discloses a rotary-type bioreactor, comprising a reaction tank, wherein bacterium solution is filled in the reaction tank; a first water inlet and a first water outlet are formed at the left end of the reaction tank; a second water outlet is formed at the right end of the reaction tank; a drum is arranged in the reaction tank; the drum sinks in the bacterium solution, and the interior of the drum is hollow; a hole is formed on the drum, and the aperture of the hole is less than the aperture of a reaction material; and a backflow tube is arranged in the drum; and a hole is formed on the backflow tube. Via the mode aforementioned, the rotary-type bioreactor adopting the scheme has the advantages of being less in pollution, temperate in working condition, short in flow, low in cost, less in investment and the like, and has the characteristic of being wide in mineral applicability in case of being applied to mining metallurgical engineering; oxygen is provided for the bacterium solution via the rotation of the drum so as to directly culture the bacterium solution, and the operation is convenient and fast; the rotary-type reactor performs reaction by means of injecting the bacterium solution, thus avoiding the damages of a shearing force in the normally-used stirring mode on the cells of bacteria, and contributing to the survival of the bacteria; and the reaction of the rotary-type reactor during a rotation process is uniform.
Owner:CHANGZHOU TEXTILE GARMENT INST

Comprehensive utilization method of pumpkin

The invention relates to a comprehensive utilization method of a pumpkin. In the method, added amount of substances is based on weight of the pumpkin; and the pumpkin is taken as a raw material for step-by-step extraction to respectively obtain pumpkin polysaccharide, pectin and pumpkin powder by utilizing a biotechnology and a membrane separation technology. The method comprises the following steps: firstly washing and cutting the pumpkin into blocks, removing seeds, pulping, carrying out water extraction at moderate temperature and centrifugal separation, carrying out acid precipitation on the obtained water extract, concentrating the obtained supernate through a nanofiltration membrane, and spray-drying to obtain the polysaccharide; extracting residues after water extraction by utilizing acid water, carrying out centrifugal separation, removing impurities from the obtained supernate through a microfiltration membrane, concentrating the supernate through a nanofiltration membrane, carrying out acid precipitation on the obtained concentrated solution, carrying out centrifugal separation, and freeze-drying the obtained precipitate to obtain the pectin; spray-drying the supernate to obtain the polysaccharide; and mixing the remaining residues and filtered liquor, grinding by a colloid mill and spray-drying to obtain the pumpkin powder. The comprehensive utilization method has the advantages that effective substances of the pumpkin are fully utilized, and process is simple and feasible, thus being applicable to industrialized production.
Owner:武汉普赛特膜技术循环利用有限公司

Preparation method of titanium dioxide nanotube array photoelectrochemical oxygen evolution electrode co-modified with polyacid and nine cobalt octasulfide

InactiveCN107012480BPhotoelectrochemical water splitting performance promotionMild working conditionsSurface reaction electrolytic coatingEnergy inputComposite filmDecomposition
The invention provides a preparation method of a polyacid and enneacobalt octasulfide co-modified titanium dioxide nanotube array photoelectrochemical oxygen evolution electrode. The prepared polyacid and enneacobalt octasulfide co-modified titanium dioxide nanotube array composite film photo anode can be used for photoelectrochemical water decomposition and oxygen evolution. The composite film photo anode is the titanium dioxide-enneacobalt octasulfide-polyacid composite film photo anode which is formed by using a titanium dioxide nanotube array as a main body and co-modified by enneacobalt octasulfide and Keggin type phosphotungstic acid. Under indoor temperature environment and irradiation of a xenon lamp, the composite film photo anode has good photoelectrochemical water decomposition performance. The preparation method of the titanium dioxide-enneacobalt octasulfide-polyacid composite film electrode is simple, quite low in cost, capable of achieving efficient and stable photoelectric water decomposition without sacrificing a reagent, a protective layer and a buffer solution, capable of achieving high-efficiency conversion from optical energy to chemical energy and applicable to development and production of the novel photoelectrochemical water decomposition and oxygen evolution electrode.
Owner:NORTHEAST NORMAL UNIVERSITY
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