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90 results about "Saturated fatty acid ester" patented technology

Method for purifying sucrose fatty acid esters

ActiveCN103087118ASolve the problem of high acid valueIncrease content levelEsterified saccharide compoundsSugar derivativesSaturated fatty acid esterSucrose
The invention relates to a method for purifying sucrose fatty acid esters. The method comprises the following steps: dissolving crude sucrose ester products in an organic solvent which can be separated from water, thereby obtaining a crude sucrose ester product solution; dropwise adding a salt aqueous solution while stirring, so that fatty acid soap substances in the crude sucrose ester product solution generate fatty-acid alkaline-earth metal salts, wherein alkaline-earth metal salts and/or alkaline-earth metal oxides are dissolved in the salt aqueous solution, and the fatty-acid alkaline-earth metal salts are not dissolved in the organic solvent; removing generated solid fatty acid alkaline earth metal salts; adding saline water into the obtained object to carry out stirring and extraction, and sanding for separating a lower water layer; cooling liquid supernatant to 0-40 DEG C through stirring, and separating out sucrose ester crystal substances in precipitation form; removing liquid and taking solid matters; and drying the solid matters so as to obtain a sucrose ester product. According to the invention, a technological process of cooling crystallization is introduced, so that the problem that reaction raw materials such as fatty acid methyl esters and the like remain in products is solved, therefore, the content level of products is further improved, and the total ester content of products is more than 98%.
Owner:LIUZHOU GAOTONG FOOD CHEM

Method for preparing polyol from waste grease and application thereof

The invention discloses a method for preparing polyol from waste grease, comprising the following steps: a solid acid catalyst which has large hydrophobic surface and has both a sulfonic group and a carboxylic group is adopted to catalyze esterification and transesterification between waste grease and methanol so as to convert waste grease to fatty acid methyl ester and a by-product glycerin; saturated fatty acid ester in fatty acid methyl ester is separated; under the catalysis of a dual acid site solid acid and in cooperation of the dual acid site, 30% hydrogen peroxide is directly catalyzed for epoxidation of fatty acid methyl ester, an intermediate product is not separated, and the by-product glycerin is added for ring opening of alkoxylation after direct heating-up; and finally, filtration is carried out to recycle the catalyst, and reduced pressure distillation is carried out to remove water so as to obtain biological oil-based polyol. According to the method, waste grease is used as a raw material, thus turning waste into wealth. The polyol product obtained has good biodegradability; the preparation process is green; emission of three industrial wastes is low; product structure and hydroxyl value can be adjusted; the range of application is wide; and the level of effect on the environment is low.
Owner:ZHEJIANG HENGFENG NEW MATERIAL

Water-soluble phytosterol unsaturated fatty acid microcapsule and preparation method of water-soluble phytosterol unsaturated fatty acid microcapsule

The invention belongs to the technical field of food and chemical industry and particularly relates to a water-soluble phytosterol unsaturated fatty acid microcapsule and preparation method of water-soluble phytosterol unsaturated fatty acid microcapsule. The microcapsule comprises 25 to 40 percent of phytosterol unsaturated fatty acid ester, 5 percent of emulsifying agents, 6.25 to 18.75 percent of sucrose and the balance wall materials, wherein the total quantity is 100 percent, the emulsifying agents are glycerin monostearate and sucrose ester, the mass ration of the glycerin monostearate to the sucrose ester is 1:(0.33-3), the ratio of the sucrose ester to the sucrose is 1:5, and the wall materials are dextrin and soy isolate protein. The water solubility of the phytosterol unsaturated fatty acid microcapsule is good, the phytosterol unsaturated fatty acid microcapsule can be mixed and dissolved with water-soluble matters, the application of the phytosterol ester to functional food, dairy products and beverages is widened, in addition, the preparation method disclosed by the invention is simple, the equipment requirement is low, and the preparation method is suitable for large-scale industrial production.
Owner:SHAANXI HEALTHFUL BIOLOGICAL ENG

Method for synthesizing and separating phytosterol saturated fatty acid esters and phytosterol unsaturated fatty acid esters

The invention relates to a method for synthesizing and separating phytosterol saturated fatty acid esters and phytosterol unsaturated fatty acid esters. The method comprises the following steps: reacting phytosterol and a mixture of saturated fatty acid esters and unsaturated fatty acid esters, sequentially washing the obtained products by a 70-80DEG C aqueous ethanol solution with the volume fraction of above 95% and an -10-10DEG C aqueous methanol solution with the volume fraction of above 80%, filtering, washing the obtained filter cake by the -10-10DEG C aqueous methanol solution with the volume fraction of above 80% to obtain the phytosterol saturated fatty acid esters with the purity of above 90%, carrying out reduced pressure distillation on the obtained filtrate, and carrying out film evaporation and molecular distillation to obtain the phytosterol unsaturated fatty acid esters with the purity of above 90%. According to the invention, the method is simple, conversion rates of raw materials are high, and the obtained products have the advantages of high purity and good color, and the phytosterol saturated fatty acid esters which can be used for antibiosis and anti-inflammation can be applied to the cosmetic field; and the phytosterol unsaturated fatty acid esters which have the antioxidation and cholesterol reduction effects can be applied to medicine and food fields.
Owner:XIAN HEALTHFUL BIOTECH

A kind of purification method of sucrose fatty acid ester

ActiveCN103087118BSolve the problem of high acid valueIncrease content levelEsterified saccharide compoundsSugar derivativesSaturated fatty acid esterSucrose
The invention relates to a method for purifying sucrose fatty acid esters. The method comprises the following steps: dissolving crude sucrose ester products in an organic solvent which can be separated from water, thereby obtaining a crude sucrose ester product solution; dropwise adding a salt aqueous solution while stirring, so that fatty acid soap substances in the crude sucrose ester product solution generate fatty-acid alkaline-earth metal salts, wherein alkaline-earth metal salts and / or alkaline-earth metal oxides are dissolved in the salt aqueous solution, and the fatty-acid alkaline-earth metal salts are not dissolved in the organic solvent; removing generated solid fatty acid alkaline earth metal salts; adding saline water into the obtained object to carry out stirring and extraction, and sanding for separating a lower water layer; cooling liquid supernatant to 0-40 DEG C through stirring, and separating out sucrose ester crystal substances in precipitation form; removing liquid and taking solid matters; and drying the solid matters so as to obtain a sucrose ester product. According to the invention, a technological process of cooling crystallization is introduced, so that the problem that reaction raw materials such as fatty acid methyl esters and the like remain in products is solved, therefore, the content level of products is further improved, and the total ester content of products is more than 98%.
Owner:LIUZHOU GAOTONG FOOD CHEM

Coupling process for preparing biodiesel and enriching polyunsaturated fatty acid esters

The invention relates to a coupling process for preparing biodiesel and enriching polyunsaturated fatty acid esters. The coupling process comprises the following steps: reacting grease, short-chain alcohol, water and liquid lipase in a reactor, and then dividing reaction liquid into a heavy phase and a light phase; recycling and reusing enzyme in the heavy phase; and distilling the light phase so as to separate out a C14-C18 fatty acid ester which serves as the biodiesel. A tower oil phase is applied to subsequent immobilized enzyme transformation, and meanwhile, online dehydration is introduced to a reaction course. The process, without conducting pre-treatment on the grease raw material in a previous reaction process of liquid enzyme catalysis, can achieve the effective transformation of the grease, which is C14-C18 in fatty acid carbon-chain length, into corresponding fatty acid ester, with a transformation rate reaching 90% or above; and tower liquid is applied to immobilized lipase catalysis in the second stage, and polyunsaturated fatty acid esters higher than C19 are effectively transformed into corresponding fatty acid ester, with a transformation rate reaching 98% or above. The process has the advantages of being strong in grease raw material adaptability, environment-friendly and clean in process, high in product yield and the like.
Owner:北京启迪德清生物能源科技有限公司

Environment-friendly solvent-free polyurethane for synthetic leather and manufacturing method of polyurethane

The invention discloses environment-friendly solvent-free polyurethane for synthetic leather. The polyurethane comprises base cloth, a water-based surface layer, a water-based adhesive layer, a foaming layer and a functional auxiliary agent, wherein the water-based surface layer comprises water-based polyurethane emulsion, a thickening agent, a water-based defoaming agent, water-based color pasteand a leveling agent; the water-based adhesive layer comprises water-based polyurethane emulsion, a water-based polyurethane crosslinking agent and water-based color paste; the foaming layer comprisesa polyol compound, white carbon black, an organometallic catalyst, hydroxyl silicone oil, fatty acid, an organic amine catalyst, a filler and toluene diisocyanate; and the functional auxiliary agentcomprises sorbitol, maltitol, oligosaccharide, glycerin saturated fatty acid ester, a coloring agent and a surfactant. The environment-friendly solvent-free polyurethane for the synthetic leather is clean and environment-friendly; the foaming layer is free of an organic solvent, so that the polyurethane is more environment-friendly and environmental protection and sustainable development are facilitated; and meanwhile, the polyurethane has the relatively good toughness.
Owner:福建成杰高分子材料有限公司 +1

Preparation method of special nanometer calcium carbonate for antifogging polyethylene films

The invention discloses a preparation method of special nanometer calcium carbonate for antifogging polyethylene films. The method concretely comprises the following steps: diluting lime milk, and conveying the diluted lime milk into a film reaction carbonizer; introducing a purified and cooled kiln gas into the above film reactor, and carrying out a carbonizing reaction to obtain a nanometer calcium carbonate slurry; adding sodium carboxymethylcellulose into the film reactor the after the completion of the reaction, performing uniform stirring, conveying the obtained slurry into a homogenization tank, and carrying out heat insulation aging; conveying the aged calcium carbonate slurry into a surface treatment tank, heating the aged slurry, adding a composite emulsion of a saturated fatty acid ester and polyphenyltrimethoxysiloxane to carry out secondary cladding modification, and performing stirring to obtain a modified nanometer calcium carbonate slurry; and carrying out pressure filtration dehydration, and drying, crushing, classifying and packaging the hydrated modified slurry to obtain the special nanometer calcium carbonate for antifogging polyethylene films. The nanometer calcium carbonate obtained in the invention can meet the requirements for the dispersibility, transparency and compatibility of a filler in the polyethylene system, and also can effectively prevent the films from fogging.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Water-soluble haematococcus pluvialis astaxanthin soft capsules and preparation method therefor

The invention discloses water-soluble haematococcus pluvialis astaxanthin soft capsules and a preparation method therefor. Capsule walls of the astaxanthin soft capsules comprise the ingredients in parts by mass: 100 parts of gelatin, 6 parts of citric acid, 20 parts of glycerine, 4 parts of sodium carboxymethyl cellulose, 10 parts of sorbitol and 11-13 parts of water; and capsule cores comprise the ingredients in percentage by mass: 10.0%-18.0% of haematococcus pluvialis astaxanthin oil, 10.0%-20.0% of polyethylene glycol-400, 20.0%-40.0% of mono-/bis-glyceryl unsaturated fatty acid ester, 2.0%-5.0% of sorbitol and 30.0%-45.0% of decapolyglyceryl monooleate. The preparation method for the astaxanthin soft capsules further comprises a step of carrying out high-pressure homogenizing mixingunder nitrogen protection so as to prepare the capsule cores. According to the water-soluble haematococcus pluvialis astaxanthin soft capsules and the preparation method therefor, all adjuvants employed are used by health-care foods according to production needs, an emulsifier is an unsaturated fatty acid processed product, the astaxanthin soft capsules are safe, non-toxic, compliant and legal, are low in health security risk and are suitable for an aqueous nutrient absorption system of the intestines and stomach of a human body, and the bioavailability of an active ingredient, i.e., astaxanthin can be improved.
Owner:YUNNAN AIERKANG BIOTECH
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