This is the room temperature regeneration method of the catalyst for noble metal dehydrogenization by carbamide. Adopt 3 - 15wt% complex compound watery solution containing ammonium ion or ammonia, at 5 - 80 Deg. C, soak out the poison produced on the surface of deactivated heavy metal catalyst in carbamide dehydrogenization. The volume proportion of soaking solid and liquid is 1 : 2.5 - 5, soaking time is 4 - 8 hours, after get out the catalyst, wash over three times with distilled water or deionized water, then lay at 110 - 120 Deg. C to dry, so it can achieve the purpose of renewing activeness and reuse. Compared with the present high temperature hydrogen deoxidizing regeneration technology, the invention has following advantages: needn't hydrogen source; needn't operate at 500 - 600 Deg. C high temperature, and can be operated at room temperature of 5 - 80 Deg. C; can very remarkably save energy waste, needn't regeneration system and electric heating device; its operation is simple, has no security hidden trouble, and can save regeneration time; the regeneration expense can be saved by 90%; after regenerated, the quality of catalyst can be ensured.