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33results about How to "Proportional control" patented technology

Preparation method for Sn based composite solder sheets

InactiveCN108453414AGuaranteed liquidityIncreased strength and high temperature stabilityWelding/cutting media/materialsSoldering mediaHot pressHot pressing
The invention relates to the technical field of welding, in particular to a preparation method for Sn based composite solder sheets. The preparation method comprises the following steps that S1, trepanned foam metal is subject to surface treatment; S2, filling of molten Sn based solder is carried out, specially, an infiltration manner is adopted for filling the foam metal with the molten Sn basedsolder, then foam metal sheets obtained after surface treatment are immersed into the molten Sn based solder, and the foam metal sheets are taken out after holes are filled with the solder; and S3, alternative stacking hot pressing treatment is carried out, specially, the foam metal sheets filled with the Sn based composite solder are alternatively stacked together, the stacked sheets are subjectto repeated hot pressing treatment, and finally the Sn based composite solder sheets are obtained. The preparation method has the beneficial effects that liquidity of the Sn based solder during brazing is guaranteed; the stacking layer number of foam Cu and foam Ni is changed, and the proportion of Cu to Ni in the composite solder sheets can be effectively controlled; and the strength and the hightemperature stability of a soldered joint are effectively improved.
Owner:WUHAN UNIV OF TECH

Light/heat double crosslinked hyperbranched polycarbosilane benzocyclobutene resin and preparation method thereof

The invention discloses light/heat double crosslinked hyperbranched polycarbosilane benzocyclobutene resin as shown in a formula (IV) and a preparation method thereof. The preparation method of the hyperbranched polycarbosilane benzocyclobutene resin comprises the following steps: generating a Grignard reagent from chloromethyltrichlorosilane under the action of magnesium; then performing a coupling reaction with Si-Cl to further form a hyperbranched Si-Cl bond-containing hyperbranched polycarbosilane polymer; adding 4-bromobenzocyclobutene to react; adding p-bromostyrene to react; then adding alkyl (alkenyl) halide to react; performing cooling; adding distilled water (deionized water) into the system for a quenching reaction; and performing solvent extraction, concentration, and purification steps such as distillation or column chromatography on silica gel to obtain the light/heat double crosslinked hyperbranched polycarbosilane benzocyclobutene resin. The light/heat double crosslinked hyperbranched polycarbosilane benzocyclobutene resin prepared by the method is excellent in thermal, electrical and photosensitive properties and is suitable for being used as a high performance dielectric film material or a packaging material in the field of microelectronics industry, space flight and aviation and national defense and the like. The formula (IV) is as shown in the specification.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Method for controlling acquisition of alloy films on multi-arc ion plating machine and proportional regulator thereof

The invention discloses a method for controlling acquisition of alloy films on a multi-arc ion plating machine and a proportional regulator thereof. The proportional regulator for regulating screening cathode plasma flux is arranged in front of one of vacuum cathode target boots; the proportional regulator is a double-layer circular baffle plate with annular holes, the annular holes of the two baffle plates are the same and account for a certain proportion of the whole circular baffle plate, and the centers of the two baffle plates are provided with a guide pillar and a guide bush for rotating the baffle plates mutually; and the rotating angle of the double-layer circular baffle plate of the proportional regulator can be regulated. The flux of cathode plasma is regulated by regulating the rotating angles of the two plates of the proportional regulator so as to control the proportion of components in the plasma atmosphere; and multi-element multilayer composite films are prepared by controlling the working state of a target. The method can effectively control the proportion of the components in the plasma atmosphere, and can prepare the multi-element multilayer composite films; and high-hardness ceramic multi-element films or multi-element multilayer films can be prepared by introducing N2 and CH4 during deposition.
Owner:GUANGDONG UNIV OF TECH

Composite coating modified high-nickel NCA positive electrode material and preparation method thereof

The invention provides a composite coating modified high-nickel NCA positive electrode material and a preparation method thereof. The NCA positive electrode material takes a ternary material as a matrix, and the surface of the matrix is coated with a composite coating modified layer composed of LiCoO2 and Co2O3. The preparation method comprises the following steps of: carrying out a co-precipitation reaction on a nickel salt solution, a cobalt salt solution, a sodium hydroxide solution and an ammonia water solution to obtain a nickel-cobalt hydroxide precursor; well mixing the obtained nickel-cobalt hydroxide precursor with a lithium source and an M source, then sintering in an oxygen atmosphere, then cooling to room temperature, crushing and sieving to obtain a primary sintered matrix; and mixing the obtained primary sintered matrix with deionized water, adding a cobalt source, adjusting the pH value, then filtering, drying, placing the matrix in an oxygen atmosphere for repeated heating and cooling sintering, cooling after sintering, and sieving to obtain the composite coating modified high-nickel NCA positive electrode material. The obtained NCA positive electrode material is high in capacity and good in cycle performance.
Owner:HUNAN SHANSHAN ENERGY TECH CO LTD

Method for analyzing short-term temperature fluctuation

The invention relates to a method for analyzing short-term temperature fluctuation, which comprises the following steps of: collecting a multi-year day-by-day temperature sequence of a certain place,respectively calculating the temperature difference between the daily temperature and the first day in the time length by taking data in the length of a research time period to form a difference group, and forming a plurality of difference sequences on the basis of data of the multi-year corresponding difference group, sorting the difference value sequences according to the size, and calculating upper and lower thresholds; and judging the size relation between the corresponding difference value group every day and the upper and lower thresholds of the corresponding difference value sequence, so that whether air temperature fluctuation occurs in the length of the research time period can be judged. According to the method, the length of the research time period and the threshold proportionof fluctuation can be freely defined, the influence of seasonal change on temperature fluctuation is eliminated, the day-by-day temperature fluctuation amplitude and the fluctuation frequency in the time period can be obtained, and the fluctuation direction can be indicated by the positive and negative of the fluctuation amplitude index.
Owner:NANJING INST OF GEOGRAPHY & LIMNOLOGY

Single metal/multi-wall carbon nano tube type composite material, preparation method and application thereof

The invention provides a single metal / multi-wall carbon nano tube type composite material, a preparation method and application thereof. According to the composite material, the single metal is uniformly loaded on the carbon nano tube, wherein the mass percentage of the carbon nano tube is 63 to 95 percent, the particle diameter of the single metal is 15 to 28 nanometers, and the diameter of the carbon nano tube is 10 to 30 nanometers. The preparation method comprises the following steps of: preparing a laminated plate containing LDH of Co, Cu and Mg activity or activity-aid species by using the micro adjustable characteristics of the composition and the structure of the LDH laminated plate, growing a carbon composite material by roasting and a chemical vapor deposition method, and meanwhile reducing mixed metal oxide into the single metal so as to obtain the single metal / multi-wall carbon nano tube type composite material. A noble platinum metal is loaded on the composite material toprepare an anode catalyst of a direct methanol fuel cell, the peak current density of the catalyst on methanol electro-catalysis oxidation is 21 to 36mA.cm<2>, and the specific activity can reach 235to 451 mA / mg. The preparation method has the advantages of simple preparation flow, low cost, environment friendliness and the like, and is suitable for industrialized application.
Owner:BEIJING UNIV OF CHEM TECH

Photo/thermal double crosslinkable hyperbranched polycarbosilane benzocyclobutene resin and preparation method thereof

The invention discloses light / heat double crosslinked hyperbranched polycarbosilane benzocyclobutene resin as shown in a formula (IV) and a preparation method thereof. The preparation method of the hyperbranched polycarbosilane benzocyclobutene resin comprises the following steps: generating a Grignard reagent from chloromethyltrichlorosilane under the action of magnesium; then performing a coupling reaction with Si-Cl to further form a hyperbranched Si-Cl bond-containing hyperbranched polycarbosilane polymer; adding 4-bromobenzocyclobutene to react; adding p-bromostyrene to react; then adding alkyl (alkenyl) halide to react; performing cooling; adding distilled water (deionized water) into the system for a quenching reaction; and performing solvent extraction, concentration, and purification steps such as distillation or column chromatography on silica gel to obtain the light / heat double crosslinked hyperbranched polycarbosilane benzocyclobutene resin. The light / heat double crosslinked hyperbranched polycarbosilane benzocyclobutene resin prepared by the method is excellent in thermal, electrical and photosensitive properties and is suitable for being used as a high performance dielectric film material or a packaging material in the field of microelectronics industry, space flight and aviation and national defense and the like. The formula (IV) is as shown in the specification.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Sealing system for sulfur dioxide fan

The invention relates to the technical field of sulfuric acid production industrial equipment sealing structures, in particular to a sealing system for a sulfur dioxide fan. The technical problems in the prior art that due to the fact that a sulfur dioxide gas leaks from a negative pressure end of a centrifugal multi-stage impeller sulfur dioxide fan, the total content of sulfur dioxide entering conversion is low, and effective compensation of the gas amount cannot be achieved are solved, and a sealing device is connected to a suction end shell of the sulfur dioxide fan to serve as a seal of a suction end rotor. A backflow pipe set is connected with the sealing device and a fan multi-stage impeller chamber and receives the negative pressure formed by guiding of the fan multi-stage impeller chamber. A control unit is used for controlling the opportunity that the backflow pipe set is guided by the fan multi-stage impeller chamber to form the negative pressure. The system has the advantages that the leakage amount of sulfur dioxide can be effectively reduced, the effective compensation total gas amount can be formed, an external medium does not need to be introduced, the impact on a production system is small when the gas amount is compensated, control over the process gas proportion is facilitated, and energy conservation and environmental protection are achieved.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY
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