The invention relates to the technical field of
molecular sieve, and especially relates to a regeneration method of a
nitrogen-preparation carbon
molecular sieve. The method provided by the invention sequentially comprises the steps that: screening and washing are carried out, wherein poisoned carbon
molecular sieve is screened by using a mesh, and the screened carbon molecular
sieve is washed by using water, such that impurities are removed;
nitrogen-based high-temperature
charring is carried out, wherein the temperature is increased to 850-1000 DEG C under the protection of
nitrogen gas, such that
charring is carried out;
mixed gas activation is carried out, wherein a
mixed gas of CO2 and CO is delivered into a furnace cavity, wherein the proportion of CO2 is 85-90%, such that the charred carbon molecular
sieve is activated, wherein the temperature in the furnace is 700-800 DEG C;
carbon deposition is carried out, wherein
activated carbon molecular
sieve is placed in a furnace cavity of a converter; the temperature in the converter is 800-900 DEG C;
xylene is delivered in under the protection of
nitrogen gas; the temperature of the furnace is maintained at 300-500 DEG C, such that
xylene is absorbed by the carbon molecular sieve;
xylene is cracked under the temperature of 800-900 DEG C, such that
pyrolytic carbon is deposited on the
char material; the carbon molecular sieve is subjected to pore
size adjustment, such that a regenerated finished product is obtained. With the method provided by the invention, deeply poisoned nitrogen-preparation carbon molecular sieve can be activated, and the pore sizes after activation is uniform.