140results about How to "Small residual magnetism" patented technology

The invention discloses an ultrasonic assistant hydro-thermal synthesis process for magnetic Fe3O4 nanometer super fine grain. The invention solves the problems of impure products and large grain diameter. The invention has the technical proposal that the form of Fe3O4 crystal nucleus is promoted in the cavitation effect of ultrasonic; cavitation gas bubble is produced in mediums; the pH value of strong ammonia is adjusted to 11 to 13; and the nanometer grain diameter size and the magnetic characteristics are controlled by controlling the hydro-thermal synthesis temperature within range from 140 DEG C to 160 DEG C and within time of 3 to 5 hours, and by changing the micro environment of the air bubble chamber, so as to obtain the dry product which is black magnetic Fe3O4 nanometer powder after being milled. The invention comprises no organic solvent, belonging to full green environmental protection which is a break in the field, and the invention is also the first to use the ultrasonic technology for assistant hydro-thermal synthesis. The invention has the advantages of simple technology, low cost, small powder granularity and even grain diameter. The powder not only can be used as duplicate ink powder, but also can be board used in aspects such as medical, biological technology, magnetic immunocyte separation, DNA separation, nucleic acid hybridization, and preparation for magnetic butt directional medicine carrying micron ball.

The invention discloses a heald selecting device for a solenoid valve of an electronic jacquard, which consists essentially of seven pieces of central brackets, two pieces of side brackets, modular solenoid valves, needle selecting hooks, offsetting springs, bidirectional moving hooks, a pulley module, a heald twine hanging cable and a quick coupling, wherein, the modular solenoid valves are arranged among the seven pieces of central brackets as well as between the central brackets and the side brackets; two sides of each modular solenoid valve are provided with a pair of needle selecting hooks, and a pair of offsetting springs and a pair of bidirectional moving hooks are arranged under each modular solenoid valve; and the bidirectional moving hooks, the pulley module, the heald twine hanging cable and the quick coupling are sequentially connected. The heald selecting device for the solenoid valve of the electronic jacquard has small electric power, correct and stable heald selecting and convenient maintenance.

The invention relates to a soft magnetic core used for a high-power inverter power supply, and a manufacturing method thereof. The magnetic core is made of an Fe-based amorphous nano-crystalline belt material through winding , and comprises components according to weight percentages as follows: 81%-85% of Fe, 0.01%-5% of Co, 7%-9% of Si, 1.5%-2.5% of B, 1%-2% of Cu, 4%-7% of M, and 0.001%-0.04% of M', wherein M is one or more of Nb, Mo, V, W and Ta, and M' is at least one of Al and Ti. The magnetic core is subjected to anneal in a protective atmosphere or a vacuum; when in anneal, the position of the magnetic core in a furnace is movable or rotatable, a holding temperature is 520-600 DEG C, the holding time is 1-2 hours, and a temperature rise speed is 100 DEG C per hour. The magnetic core manufactured by adopting the method has lower loss, better manufacturing technique properties, and good soft magnetic characteristics; moreover, the downstream processing after the heat treatment is applicable to various technique methods.

The invention discloses a method for preparing high-magnetic energy product high-coercive force low-cost sintered neodymium iron boron (NdFeB). The method comprises the following steps of: throwing raw materials into a rapid coagulating furnace and smelting in the protective atmosphere of inert gases or nitrogen, and pouring smelting liquid onto a copper roller at a roller speed of 2 to 4m/s to form a rapid coagulating thin strip with the mean thickness of 0.1 to 0.3mm; performing hydrogen breaking and jet milling to obtain magnetic powder with the superficial area mean particle size of 1.5 to 3 mu m, and orientating and molding the magnetic powder in a magnetic field to obtain a blank; and finally, sintering, cooling and ageing to obtain a sintered NdFeB magnet with the mean grain size of 5 to 6 mu m. Compared with the conventional preparation method, by optimizing the rapid coagulating process and combining the adjustment of raw materials, the preparation method makes NdFeB columnar crystals reduced during smelting; therefore, the superficial area mean particle size of the magnetic powder is reduced in the process of performing jet milling, the mean grain size of the sintered NdFeB magnet is reduced finally, and the coercive force of the sintered NdFeB magnet is improved. Therefore, the preparation method is suitable for preparing a high-magnetic energy product and low-cost high-coercive force magnet.

The invention provides a rare earth permanent magnetic material and a preparation method thereof. The rare earth permanent magnetic material is characterized in that the rare earth permanent magnetic material is formed in the mode that a composite-structure blank composed of a magnetic phase blank and a non-magnetic phase covering the surface of the magnetic phase blank is pressed and sintered and undergoes tempering heat treatment. During preparation, firstly the magnetic phase blank is prepared in a forming stage, then non-magnetic phase mixtures comprising heavy rare earth compounds are applied to the end face of the blank, then sintering and tempering processing are carried out, and in the heat processing process, by means of grain boundary diffusion, a sintered magnet with low heavy rare earth content and high coercivity is obtained. Compared with an existing grain boundary diffusion technique, production efficiency is improved after the technique is adopted. By means of the method, heavy rare earth elements are in grain boundary of gains in the sintered magnet, and accordingly coercivity is improved and meanwhile residual magnetism is reduced to the smallest degree. By means of the method, a large magnet can be prepared, the defect that a large magnet cannot be prepared in a traditional sintered magnet grain boundary diffusion technique is overcome, and preparation and machining cost of the magnet is reduced.

The invention discloses a double-principal-phase yttrium-contained permanent magnet, and belongs to the technical field of rare earth permanent magnetic materials. The chemical formula of the double-principal-phase yttrium-contained permanent magnet is (YetaRe1-eta)alphaFe100-alpha-beta-gammaBbetaTMgamma according to the mass percent, wherein the eta is larger than or equal to 0.05 and smaller than or equal to 0.6, the alpha is larger than or equal to 29 and smaller than or equal to 33, the beta is larger than or equal to 0.8 and smaller than or equal to 1.4, the gamma is larger than or equal to 0.5 and smaller than or equal to 3.6, the Re is one or more of elements of Nd, Pr, Dy, Tb and Ho, and the TM is one or more of elements of Ga, Co, Cu, Nb and Al. The double-principal-phase yttrium-contained permanent magnet is of the double-principal-phase structure comprising a (Y, Re)-Fe-B principal phase and a (Nd, Pr)-Fe-B principal phase. According to the double-principal-phase yttrium-contained permanent magnet prepared by a double-principal-phase alloy method, the good magnetic performance is kept, meanwhile, the Nd and the Pr can be greatly replaced by the relatively abundant Y, and the production cost of the double-principal-phase yttrium-contained permanent magnet is greatly reduced.

The invention relates to a method for preparing sintered neodymium iron boron by adding nanometre aluminium powder, belonging to the technical field of rare earth magnetic material. The method comprises the following steps of: weighting the raw materials according to the following prescription: RxMyBzFe1-x-y-z (x=29-35wt%, y=0-4wt%, z=0.9-1.1wt%), wherein R is selected from one or several of La, Ce, Pr, Nd, Gd, Ho and Dy, and M is selected from one or several of Co, Al, Cu, Nb, Zr and Ga; pouring the smelted raw materials into melt-spinning sheets; hydrogen-smashing the melt-spinning sheets to obtain the powders and airflow-milling the powders into micro powders; adding the aluminium powders with the average grading of 10-100nm into the micro powders according to a proportion of 0.1-1wt% and mixing; pressing and moulding, and isostatic pressing processing the mixed powders into blanks; sintering, tempering to obtain the sintered neodymium iron boron magnets. According to the invention, the residual magnetism fall is relatively little and the production cost is low while the coercive force of the neodymium iron boron magnet is improved.

The invention relates to a preparation method of a magnetism macromolecule hydrogel. In the forming process of the novel magnetism macromolecule hydrogel, iron ions enter a three-dimensional network structure of poly2-acrylamide-2-methylpropane sodium anionic hydrogel through the diffusion action and are adsorbed by sulfonate radicals in the anionic hydrogel through electrostatic interaction and stably to be stably and uniformly distributed in the hydrogel; then the iron ions generate octahedral Fe3O4 magnetic particles with the size of about 50nm to 100nm in situ in a special macromolecule hydrogel network microenvironment by a simple and soft coprecipitation method, thereby obtaining the magnetism macromolecule hydrogel with irregular and uniform-distributed Fe3O4 magnetic particles. The magnetism macromolecule hydrogel prepared by the method overcomes the problem of non-uniform magnetism distribution; and magnetic particles in the hydrogel have the appearance of regular octahedrons with the average size of 50nm-10nm, thereby leading the magnetism hydrogel to have very low residual magnetism.

The invention provides a magnetic abrasive material and a method for preparing the magnetic abrasive material. The magnetic abrasive material is an acicular or spherical magnetic abrasive material with the structure of a core and a film, the core is a stainless pin or a stainless steel ball, and the film is ceramics. Through the method for preparing the magnetic abrasive material provided by the invention, a magnetic abrasive material which has strong polishing or grinding capacity and can form an ideal magnetic brush is obtained.

The present invention relates to a kind of magnetic separating column and its application in separating biological samples. The magnetic separating column has structure comprising a material holding section, a filler column, a discharge port and a pushing plug. The filler column is filled with small magnetic soft iron balls of sizes 0.01-0.1mm, 0.1-0.2mm and 0.2-1mm separately. During separation, the sample fed through the inlet in the upper end is made to flow through the filler column and the discharge port under the gravity action, and the pushing plug applies pressure to push out the blocked sample. Under the action of outer magnetic field, the magnetic separating column can generate high gradient magnetic field for effective fast separation of various kinds of cells, subcellular matters, bacteria, viruses, nucleic acids, proteins and other biological samples.

The invention relates to the technical field of high frequency inverter power supplies, in particular to a low-remanence nanocrystalline magnetic core and a preparation method thereof. The preparation method includes the following steps: performing vacuum isothermal annealing on a Fe-Ni based nanocrystalline ribbon prepared by the single roller melt rotation rapid quenching method, and water-cooling the Fe-Ni based nanocrystalline ribbon to the indoor temperature; crushing the Fe-Ni based nanocrystalline ribbon into nanocrystalline metallic powder, performing ball-milling and shaping on the nanocrystalline metallic powder, screening the powder into first powder and second powder; evenly mixing the processed first powder and the processed second powder, pressing the mixed powder into a magnetic core; putting the formed magnetic core in a vacuum annealing furnace to perform heat treatment; performing heat treatment again; and performing glue dipping and curing treatment on the nanocrystalline magnetic core. The preparation method is simple in process, and is low in production cost; the acquired magnetic core finished product has high saturation flux density, low a loss value, low coercivity, low remanence, and high temperature resistance, is excellent in comprehensive performance, will not be damaged, and is improved in reliability.

The invention provides a preparation method of a permanent magnet material. The preparation method provided by the invention comprises a coating process and a permeation process, wherein a material containing a rare-earth element coats the surfaces of sintered neodymium-iron-boron magnets; the thickness of each sintered neodymium-iron-boron magnet in one direction is at least less than 10mm; the sintered neodymium-iron-boron magnets are regularly arranged; with respective surfaces with the maximum area as contact surfaces, the sintered neodymium-iron-boron magnets tightly contact one another under the pressure action; and then the sintered neodymium-iron-boron magnets are subjected to heat treatment. By the preparation method provided by the invention, the rare-earth element can permeate evenly and the permeability is high. In addition, by the preparation method provided by the invention, the coercive force of the permanent magnet material can be greatly improved while the residual magnetism is reduced slightly.

The invention relates to a preparation method of a high-performance sintered Nd-Fe-B permanent magnet material, belonging to the field of rare earth permanent magnet material. The quaternary and abovequaternary rare earth alloy films are deposited on the surface of pretreated Nd-Fe-B magnet by magnetron sputtering. The homogenization, grain boundary diffusion and low temperature tempering are used as diffusion sources to improve the boundary structure of the magnet, so that the coercivity of the magnet is greatly increased and the remanence is kept basically unchanged. The composition of thequaternary and above quaternary rare earth alloy film is LRE 100-X-Y-ZHRExMyAlz (1 <= x <= 40, 1 <= y <= 20, 1 <= z <= 20), wherein LRE is one or more of the light rare earth elements such as Y, La, Ce, Pr, Nd, HRE is one or more of the heavy rare earth elements such as Tb, Dy, Ho, and M is one or more of the alloy elements such as Cu, Fe, Co, Ga, Zr, Zn, Mn, and Mg. The rare earth alloy thin filmprepared by the invention is uniform, compact and strong in adhesion as diffusion source, the quantity is continuously controllable, and the consistency of magnetic properties of the magnet after diffusion treatment is good; It can reduce the amount of rare earth and is suitable for industrial production.

The invention discloses an R-Fe-B type sintered magnet manufacturing method. The method mainly includes the steps that an R-Fe-B type sintered magnet is prepared as a matrix; a heavy rare earth RHX layer comprising at least one of metal dysprosium, dysprosium hydride, terbium and terbium hydride is distributed on the surface of the matrix, and an RLF layer comprising at least one of praseodymium fluoride, neodymium fluoride, praseodymium oxide and neodymium oxide is distributed on the RHX layer; heat treatment is conducted in a diffusion furnace, the heavy rare earth RHX is diffused into the magnet through the surface of the matrix. By arranging the RLF layer with praseodymium fluoride, neodymium fluoride, praseodymium oxide and neodymium oxide coatings outside the heavy rare earth RHX layer of the magnet, on one hand, magnets can be stacked in the diffusion process and the adhesion is prevented; on the other hand, the heavy rare earth RHX layer is protected against oxidation in the diffusion process, the situation that the heavy rare earth RHX layer is oxidized on the surface of the magnet and influences the diffusion effect is affected, besides, volatilization of the R element in the R-Fe-B type magnet matrix can be prevented in the diffusion process, and it is guaranteed that remanence of the magnet hardly reduces.

The invention relates to a solid garage falling protector. The falling protector is characterized in that one end of a pull rod is flexibly connected with an armature connector in a hinged mode, a fulcrum pin is fixed on a support, and the middle of a linkage lever is rotatablely matched with the fulcrum pin; one end of the linkage lever is flexibly connected with the other end of the pull rod in the hinged mode, the other end of the linkage lever is a flexibly connected with a connecting pin of a hook connector in the hinged mode, and the other end of the linkage lever is rotatablely connected to the connecting pin on the right upper part of the hook connector; and the support arranged on the left upper side of the hook connector is provided with a signal switch, and a trigger end of the signal switch is matched above the left upper side step of the hook connector. The pull rod of the falling protector provided by the invention is formed by connecting elastisch Oxford rods through the active linkage lever, therefore, the collision of the falling protector does not deform and bend through the collision. The falling protector provided by the invention has the advantages of restoration in time, good sensitivity, safety and waterproof properties, and prolongs the service life.

The invention relates to the technical field of rare earth permanent magnets, in particular to a sintered neodymium iron boron magnet and a preparation method thereof. The sintered neodymium iron boron magnet is characterized in that according to the mass percentage composition, the general formula of the sintered neodymium iron boron magnet is ReaDybFe100-a-b-c-dBcMd; Re is one or more of Pr, Nd,La, Ce, Gd and Ho; M is one or more of Co, Cu, Al, Nb, Ga, Zr, Ti and Cr; and a is larger than or equal to 27 and smaller than or equal to 33, b is larger than or equal to 1.0 and smaller than or equal to 2.0, c is larger than or equal to 0.9 and smaller than or equal to 1.1, and d is larger than or equal to 0 and smaller than or equal to 5. Through the optimized process, smelting, single hydrogen breaking and powder making are not needed, and the using amount of heavy rare earth can be reduced to 1.5wt% or even 1.2wt%, so that rare earth is more uniformly distributed in the grain boundary, and the effective utilization ratio of the rare earth is improved; and according to the sintered neodymium iron boron magnet prepared through the process, while cost is reduced, the excellent magneticproperties are achieved.

The invention provides a preparation method of a nano-micron pyrrhotite soft magnetic material. The preparation method comprises the following steps: by using reduced iron powder (Fe) and sublimed sulfur as main raw materials, and grinding the two raw materials in a certain proportion until the two raw materials are uniformly mixed; heating for a certain time under a certain temperature condition; performing heat preservation and cooling, thereby finally obtaining the ash black pyrrhotite soft magnetic powered material with crystals developing well. The material has the characteristics of low residual magnetism and low coercivity. The basic expression of the components is Fe1-xS (x is greater than or equal to 0 but less than or equal to 0.223). By using materials which are low in price and simple and easily available, the pyrrhotite soft magnetic material which is high in purity, uniform in granular distribution and low in coercivity and residual magnetism is manually prepared by virtue of an iron-sulfur compound method and can be used for satisfying the actual demand of the magnetic material. The soft magnetic material is the magnetic material with low residual magnetism and low coercivity, has the characteristics of easiness for magnetization and easiness for demagnetization, can be widely applied to electrical equipment and electronic equipment and has actual application value.

The invention discloses a method for improving coercive force of a rare-earth permanent-magnet, which is characterized in that in the process of manufacturing the rare-earth permanent-magnet, other rare-earth oxides except DyO and TbO are added into and fully mixed with prepared powdered alloy, and then the mixture is molded in an oriented way and sintered; and the added rare-earth oxides are NdO and/or GdO, and are treated by dehydration at the temperature of over 500 DEG C, and the doping proportion is 0.8-3.2% of the weight of the prepared powdered alloy. The rare-earth oxides with lower price are added into the prepared powdered alloy, and other processes are not changed, serial tests prove that when about 0.8% of rare-earth oxides are added, the coercive force is increased by 1900-3900KOe, and the remanence of the product is reduced by 200-300Gs. When the adding proportion is more than 1.6%, the remanence of the product is reduced, and the significance is significantly lowered. The method has simple technique, lower cost and remarkable effect.