The invention relates to a preparation method of a BiOCl/carbonized egg membrane composite visible light catalyst. The preparation method comprises the following steps that S1, egg membranes are driedand cut into pieces; S2, egg membrane fragments are calcined, and are grinded to particles after being calcined, and carbonized egg membranes are obtained; and S3, hydrochloric acid, deionized waterand ethanol are added to a Bi(NO3)3 solid body, then the carbonized egg membranes are added, ultrasonic treatment is carried out for 30-120 min, stirring is carried out for 30 min, a NaOH solution isadded in the stirring process, finally aging is carried out for 8-12 hours, liquid is filtered out, drying is carried out at 100 DEG C for 12-15 hours, finally the modified BiOCl/carbonized egg membrane catalyst is obtained, and the catalyst is applied to degradation of dye wastewater containing rhodamine B, antibiotic wastewater containing tetracycline hydrochloride and industrial wastewater containing organic pollutants. According to the preparation method of the BiOCl/carbonized egg membrane composite visible light catalyst, the pressure of waste treatment and environmental pollution can bereduced, waste is turned into treasure, and efficient catalytic degradation of the industrial waste water is realized.