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74 results about "Solid sphere" patented technology

The Solid Sphere Model was the first atomic model and was developed by John Dalton in the early 19th century. He hypothesized that an atom is a solid sphere that could not be divided into smaller particles. He came up with his theory as a result of his research into gases. He realized that certain gases only combined in specific proportions.

Solid sphere flux heat absorber for solar thermal power generation

The invention relates to a solid sphere flux heat absorber for solar thermal power generation, comprising a solid sphere heating absorbing device (1), a heat absorbing solid sphere (2) arranged in the solid sphere heating absorbing device (1), a lower-temperature sphere storage tank (5) arranged on the upper part of the solid sphere heating absorbing device (1), a high-temperature sphere storage tank (9) arranged on the lower part of the solid sphere heating absorbing device (1), lower-temperature sphere storage tank inlet valves (7) and (8) respectively arranged on the upper part and the lower part of the lower-temperature sphere storage tank (5), and high-temperature sphere storage tank inlet valves (11) and (12) respectively arranged on the upper part and the lower part of the high-temperature sphere storage tank (9). The solid sphere heating absorbing device (1) faces an energy flux of a radiation receiving window (4) at the throwing side of radiation energy flux (3). The lower-temperature sphere storage tank (5) is used for storing a lower-temperature solid sphere (6), and the high-temperature sphere storage tank (9) is used for storing a high-temperature solid sphere (10). The surface of the heat absorbing solid sphere (2) is black or is coated with solar selective absorption coatings.
Owner:GUANGDONG FIVESTAR SOLAR ENERGY

Zinc oxide based composite photocatalytic nano-material and preparation method thereof

The invention provides a zinc oxide based composite photocatalytic nano-material, which is a material with visible light catalytic activity. The material has a sea-urchin-shaped solid sphere shape or hollow sphere shape. The preparation method comprises the following two steps: (1) putting alcohol/water solution of zinc salt into a high-pressure reaction kettle, reacting at 140-180 DEG C for 1.5-9 hours, washing the product with ethanol, and drying at 60 DEG C for 2-6 hours to obtain a sea-urchin-shaped ZnO microsphere; (2) performing ultrasonic dispersion on the sea-urchin-shaped ZnO in a ferric salt solution by utilizing a dipping-precipitation method, dripping ammonium hydroxide to react for 1-12 hours at 40 DEG C in a stirring condition, wherein the mass ratio of ferric salt to ZnO is 0.05-0.2; collecting solid, calcining at 350 DEG C for 2 hours to obtain an alpha-Fe2O3 nano-particle modified ZnO composite photocatalytic system. The material has strong light absorption and light response in the visible light range, can be used for remarkably improving the activity of visible light catalytic degraded organic dye, and can be applied to light catalytic degradation treatment of wastewater of the dye industry.
Owner:ZHEJIANG NORMAL UNIVERSITY

Multi-layer core shell structure CeO2 nanometer hollow sphere template-free composite method

ActiveCN104925845APrecise control of the number of core shellsPrecise thickness controlMaterial nanotechnologyRare earth metal compoundsSolid sphereCerium
The invention discloses a multi-layer core shell structure CeO2 nanometer hollow sphere template-free composite method. The method includes the steps that firstly, cerous nitrate and pyridine-2,5-dicarboxylic acid are dissolved in an absolute ethyl alcohol and DMF mixed solvent; then the mixed solution is placed in a reaction kettle, reaction is conducted for 6-12 hours at the temperature of 100 DEG C to 160 DEG C, centrifugal washing is conducted after reaction is conducted, and coordination polymer nano solid spheres of cerium are obtained after the mixture is dried at 80 DEG C; finally, the obtained dried samples are placed in a muffle furnace, roasting is conducted for 1-4 hours at the temperature of 400 DEG C to 800 DEG C, and the multi-layer core shell structure CeO2 hollow spheres are obtained after the mixture is cooled to the room temperature. The method is simple in synthesis procedures and capable of conducting accurate control over the number of core shells, the thickness and the like; the average grain size of the synthetic multi-layer core shell structure CeO2 nanometer hollow spheres is 400 nm, distribution is even, most spheres are composed of three hollow sphere shells and one hollow sphere core, and the obtained material structure is stable. The method provides a new way for synthesis of ceria of a complex core-shell structure.
Owner:JIANGXI NORMAL UNIV

Double-layer compound biological filter material for aerated biological filter and method for preparing same

The invention discloses a double-layer compound biological filter material for an aerated biological filter. The double-layer compound biological filter material is formed by combining an inner layer and an outer layer, wherein the inner layer consists of attapulgite clay and fly ash in a weight ratio of 4:6; and the outer layer consists of attapulgite clay, kieselguhr and coal dust in a weight ratio of 7-10:9-12:1. The preparation method comprises the following steps of: uniformly mixing the attapulgite clay and the fly ash, and forming inner cores of solid spheres in a granulator; uniformly mixing the attapulgite clay, the kieselguhr and the coal dust to obtain mixed powder, continuously and slowly adding the mixed powder into the granulator to coat the surfaces of the inner cores of the solid spheres for granulation to obtain the finished product spheres; and drying the finished spheres naturally for 24 hours and in a constant-temperature fan drying box at the temperature of 120 DEG C for 2 hours, taking the finished spheres out of the drying box, directly putting the finished spheres in a box-typed resistance furnace to sinter the finished spheres at the temperature of between 950 and 1.050 DEG C for 20 minutes, and naturally cooling the finished spheres to obtain the double-layer compound biological filter material. The double-layer compound biological filter material obtained by the preparation method has the advantages of rough surface, high void ratio, good wearing resistance, high strength, easy film formation and high economy and practicability.
Owner:HUAIYIN INSTITUTE OF TECHNOLOGY

Preparation method of micro-nano tin dioxide solid spheres

The invention relates to the preparation of micro-nano materials, and aims to provide a preparation method of micro-nano tin dioxide solid spheres. The method comprises the following steps: respectively preparing a SnCl4.5H2O aqueous solution and a NaOH solution, uniformly dropwise adding the NaOH solution into the SnCl4.5H2O aqueous solution, and stirring at a high speed; transferring the mixed solution to a polytetrafluoroethylene reaction kettle, and carrying out a hydrothermal reaction on the mixed solution; carrying out centrifugal separation or filtering on the obtained product, washing the obtained object until no soluble ion exists in the solution, and drying, so that white powder is obtained; and putting the powder into a chamber electric furnace or a muffle furnace to calcine, and carrying out furnace cooling on the obtained product, so that white or light yellow powder, namely, micro-nano tin dioxide solid spheres, is obtained. Products prepared according to the preparation method disclosed by the invention are good in sphericity, smooth in surface, and uniform in size; no organic solvent as well as volatile poisonous gas and the like is used in the preparation process, so that only do sodium salts exist in products, and therefore, the product has no pollution to the environment; and no template is used, so that the method is simple in process, easily controlled in reaction process, mild in reaction condition, simple in raw material and low in cost, and therefore, the method is specially suitable for large-scale industrial production.
Owner:ZHEJIANG UNIV

Mesoporous silicon dioxide material with eggshell-yolk structure and preparation method of mesoporous silicon dioxide material

The invention provides a mesoporous silicon dioxide material with an eggshell-yolk structure and a preparation method of the mesoporous silicon dioxide material. The material is in a spherical shape as a whole, and the specific surface area is 500-800 m<2>/g. The ''yolk'' is a silicon dioxide solid sphere with a diameter of 200-500 nm, the ''eggshell'' is a silicon dioxide hollow sphere with a thickness of 20-100 nm, the diameter of a cavity is 240-800 nm, the ''eggshell'' and the ''yolk'' have regular ordered mesopores, and the aperture is 2.5-3.5 nm. The material is prepared by adopting a simple one-pot method, a silicon source and a carbon source are added into a mixed solution of ethanol/deionized water/ammonia water/hexadecyl trimethyl ammonium bromide, a proper amount of silicon source is added after reaction for a period of time, and an obtained solid product is dried and roasted to obtain the mesoporous silicon dioxide with the eggshell-yolk structure. The invention has the beneficial effects that the provided material is regular in structure and large in specific surface area, and has good application prospects in the fields of catalysis, adsorption separation, drug sustained release and the like.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Porous spherical electrospinning nozzle and spinning method thereof

InactiveCN108411383AMulti-level distribution of diameter can be controlled and adjustedElectro-spinningPeristaltic pumpSolid sphere
The invention discloses a porous spherical electrospinning nozzle and a spinning method thereof. The porous spherical electrospinning nozzle is a solid sphere with a smooth surface, and a plurality ofholes are distributed in the spherical surface; the porous spherical electrospinning nozzle is connected to a first motor through a transmission shaft, and the lower portion of the porous spherical electrospinning nozzle is immersed in a spinning solution of a liquid storage tank. The spinning method includes the steps of opening a receiving device; opening a liquid supply device and injecting the spinning solution into the liquid storage tank through a peristaltic pump; opening the first motor, so that the porous spherical electrospinning nozzle rotates in the spinning solution, and the spinning solution forms two states of liquid films on the spherical surface and hole surfaces respectively; opening a high-voltage generator, so that the liquid films on the spherical surface and the holesurfaces generate jet flow different in fineness respectively, and the jet flow is stretched, solidified and deposited on the receiving device to form nanofibers. The nanofibers with two or more kinds of diameter distribution can be prepared under the conditions of not using a plurality of spinning solutions and not adjusting spinning parameters.
Owner:DONGHUA UNIV +1

Method for preparing CeO2 nanometer solid sphere by using CTAB (Cetyltrimethyl Ammonium Bromide) as soft template

The invention discloses a method for preparing a CeO2 nanometer solid sphere by using CTAB (Cetyltrimethyl Ammonium Bromide) as a soft template. The method comprises the following steps of: dissolving Ce(NO3)3.6H2O in deionized water to obtain a Ce(NO3)3 solution; adding KBrO3 and the CTAB (Cetyltrimethyl Ammonium Bromide) into the Ce(NO3)3 solution and obtaining a mixed solution after continuous uniform stirring; and transferring the mixed solution into a reaction kettle, placing the reaction kettle in a baking oven to carry out reaction at 160-190 DEG C for 10-20hours, carrying out centrifugal washing after the reaction is finished, and drying the washed product at 80 DEG C to obtain solid sphere-like CeO2 nanometer powder. According to the preparation method disclosed by the invention, the Ce(NO3)3.6H2O, the KBrO3 and the CTAB (Cetyltrimethyl Ammonium Bromide) are used as raw materials, the nanometer solid sphere is further synthesized by taking the CATB as the soft template and by means of hydro-thermal method, mean diameter of the sphere is 1mu m, and the nanometer solid sphere is composed of a large number of fine CeO2 particles. The method has the unique advantages of relative low cost of raw materials and simple technological operation.
Owner:SHAANXI UNIV OF SCI & TECH

Method for preparing mesoporous nano particles with special appearance based on anion surfactant

InactiveCN102659122AEliminate non-biocompatibility factorsEasy to separateSilicaNanotechnologySolid sphereRoom temperature
The invention relates to a method for preparing mesoporous nano particles with special appearance based on an anion surfactant, and belongs to a method for preparing mesoporous nano particles. The method comprises the following steps of: dissolving 1.0 millimole of Sar-Na in 30 mL of deionized water at the temperature of between 14 and 18 DEG C, dripping 2.0 mL of 0.1 M hydrochloric acid, regulating the pH value to 6.0 to 6.8 slowly, stirring for 30 minutes, dripping 1.0 mL of tetraethyl orthosilicate (TEOS) and 0.1 mL of 3-aminopropyl trimethoxysilane (APMS), stirring a mixture at room temperature for 10 minutes, putting into a kettle, standing at the temperature of 15 DEG C for 2 hours, transferring the reaction kettle into a drying oven of 80 DEG C, and crystallizing for 20 hours; cooling to the room temperature, opening the kettle, centrifuging and washing; drying at the temperature of 40 DEG C for 48 hours; and performing reaction to generate two products, wherein one product is positioned on a solution and is named AMS-U, the other product is dispersed in a substratum solution and is named AMS-R, superstratum substances are mesoporous hollow spheres, and substratum products are solid spheres with mesoporous structures. The method has the advantages that two mesoporous nano particles are prepared in one step and are distributed in two layers, the superstratum substances are the mesoporous hollow spheres, the substratum substances are the solid spheres, and the hollow spheres and the solid spheres can be separated by a physical method.
Owner:CHINA UNIV OF MINING & TECH

Filling material for sewage treatment and preparation method of filling material

The invention discloses a filling material for sewage treatment and a preparation method of the filling material. The filling material is spherical and comprises a solid sphere in the centre, a sheet-like fan-shaped expansion area and a wool area on various surfaces, wherein the sheet-like fan-shaped expansion area and the wool area on various surfaces are arranged outside the solid sphere at intervals. The preparation method comprises the steps of manufacturing a spherical basal body, forming a fan-shaped surface in the expansion area, splitting and the like. By means of the unique structure and the process thereof, the filling material disclosed by the invention is good in oxygenizing efficiency and rapid to hang; the specific surface area of the filling material is high; attachment of microorganisms is promoted through the fan-shaped wool area; an aerobic state is formed in the sphere; an anoxic state is formed even in the spherical centre; a biological membrane has multiple varieties of the microorganisms, long food chain and higher processing capacity; the filling material is simple to install and convenient to operate and manage; the basal body shape of the filling material is a sphere; under the stirring of aerated bubbles, the filling material can rotate at high speed; therefore, the filling material is low in resistance and mould releasing and updating are easy; the filling material takes synthetic fibre polyurethane, which has good hydrophilia, as a substrate material.
Owner:四川省科学城天人环保有限公司

Double-silicon-source-oriented hollow-sandwich-hollow silicon dioxide mesoporous material and synthesizing method thereof

The invention relates to a double-silicon-source-oriented hollow-sandwich-hollow silicon dioxide mesoporous material and a synthesizing method thereof. The synthesizing method includes the steps that ethyl alcohol serves as a solvent, and under the base catalysis effect of ammonium hydroxide, 3-(2-aminoethyl)-aminopropyl trimethoxy silane (TSD) and tetraethoxysilane (TEOS) are subjected to hydrolytic polymerization to obtain solid hybridization silicon dioxide spheres; the spheres are converted into the hollow or solid sandwich-hollow silicon dioxide mesoporous material under the etching effect of hydrofluoric acid (HF), wherein in the process of preparing the solid hybridization silicon dioxide spheres, the silicon dioxide mesoporous material of different structures can be obtained by simply adjusting the volume ratio of the two silicon sources. According to the hollow silicon dioxide mesoporous material obtained with the method, the particle size ranges from 350 nm to 420 nm, the shell thickness ranges from 30 nm to 50 nm, and the hole diameter ranges from 3 nm to 4 nm; according to the obtained sandwich-hollow silicon dioxide mesoporous material, the particle size ranges from 350 nm to 420 nm, silicon dioxide solid spheres with the particle size of 100 nm to 160 nm serve as cores, the shell thickness ranges from 30 nm to 50 nm, and the hole diameter ranges from 3 nm to 4 nm. According to the silicon dioxide mesoporous material obtained with the method, a certain amount of amino exists for modification, and the application in the fields of catalysis, biological medicine and the like is greatly expanded.
Owner:SHANGHAI UNIV

Preparation method of SnO2/carbon fabric composite material for sodium ion battery negative electrode

The invention relates to a preparation method of a SnO2/carbon fabric composite material for a sodium ion battery negative electrode. The SnO2/carbon fabric composite material with a grain size being0.5-1 micrometer and a uniform solid-sphere structure is prepared by taking water as a solvent and SnCl<2>.2H2O as a tin source and by a hydrothermal method, the SnO2/carbon fabric composite materialis used as a negative electrode material to be assembled to form a sodium ion battery. Since SnO2 has relatively high theoretical capacity, the conductivity of the negative electrode material can be improved by taking a carbon fabric as a matrix; and moreover, SnO2 is directly grown on the carbon fabric, a binding agent and a conductive agent are not needed to be pasted, the active substance dutyratio is improved, the energy density is large, and thus, the SnO2/carbon fabric composite material shows relatively good electrochemical performance. The preparation process is simple in process, theSnO2/carbon fabric composite material low in reaction temperature, high in repeatability, short in period and low in energy consumption, is suitable for demand of large-scale production and has remarkable scientific significance to the application aspect of the sodium ion battery, and the production cost is reduced.
Owner:SHAANXI UNIV OF SCI & TECH

Filler for sewage treatment and preparation method thereof

The invention discloses a filling material for sewage treatment and a preparation method of the filling material. The filling material is spherical and comprises a solid sphere in the centre, a sheet-like fan-shaped expansion area and a wool area on various surfaces, wherein the sheet-like fan-shaped expansion area and the wool area on various surfaces are arranged outside the solid sphere at intervals. The preparation method comprises the steps of manufacturing a spherical basal body, forming a fan-shaped surface in the expansion area, splitting and the like. By means of the unique structure and the process thereof, the filling material disclosed by the invention is good in oxygenizing efficiency and rapid to hang; the specific surface area of the filling material is high; attachment of microorganisms is promoted through the fan-shaped wool area; an aerobic state is formed in the sphere; an anoxic state is formed even in the spherical centre; a biological membrane has multiple varieties of the microorganisms, long food chain and higher processing capacity; the filling material is simple to install and convenient to operate and manage; the basal body shape of the filling material is a sphere; under the stirring of aerated bubbles, the filling material can rotate at high speed; therefore, the filling material is low in resistance and mould releasing and updating are easy; the filling material takes synthetic fibre polyurethane, which has good hydrophilia, as a substrate material.
Owner:四川省科学城天人环保有限公司
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