The invention discloses a Ni-Mo-Ti
alloy reinforced by an ordered D0a / disordered HCP
composite structure, which is characterized in that the element percentage composition expression of the Ni-Mo-Ti
alloy is (Ni80 + yMo20-y) 100-xTix, x is greater than or equal to 1 and less than or equal to 10, y is greater than or equal to-5 and less than or equal to 5; the
microstructure of the Ni-Mo-Ti
alloy comprises a face-centered cubic FCC matrix and a strengthening phase embedded in the face-centered cubic FCC matrix, and the strengthening phase is a layered phase formed by compounding an ordered D0a area and a disordered HCP area. The invention further provides a preparation method of the Ni-Mo-Ti alloy reinforced by the ordered D0a / disordered HCP
composite structure. The preparation method comprises the following steps of vacuum melting and
vacuum casting; carrying out homogenization treatment; multi-pass rolling is conducted at the
room temperature, the pass rolling amount is 2%-6%, and the total rolling amount is 60%-90%; and annealing heat treatment is conducted, specifically, the temperature of annealing heat treatment ranges from 910 DEG C to 1150 DEG C, and the time ranges from 1.5 min to 120 min. According to the Ni-Mo-Ti alloy strengthened by the ordered D0a / disordered HCP
composite structure and the preparation method of the Ni-Mo-Ti alloy, through the strengthening effect of the ordered D0a and disordered HCP composite layer, the alloy material has ultrahigh strength and high
plasticity at the same time, and the comprehensive
mechanical property of the alloy material is improved.